CN110643243A - Scraping sand wall texture coating and preparation method thereof - Google Patents

Scraping sand wall texture coating and preparation method thereof Download PDF

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Publication number
CN110643243A
CN110643243A CN201910955203.9A CN201910955203A CN110643243A CN 110643243 A CN110643243 A CN 110643243A CN 201910955203 A CN201910955203 A CN 201910955203A CN 110643243 A CN110643243 A CN 110643243A
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parts
coating
agent
batch
cellulose
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王四九
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Jiangsu Jiunuo Building Materials Polytron Technologies Inc
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Jiangsu Jiunuo Building Materials Polytron Technologies Inc
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04Homopolymers or copolymers of esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/28Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for wrinkle, crackle, orange-peel, or similar decorative effects
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/43Thickening agents
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/47Levelling agents
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/32Phosphorus-containing compounds
    • C08K2003/321Phosphates
    • C08K2003/324Alkali metal phosphate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Engineering & Computer Science (AREA)
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  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention relates to the technical field of decorative coatings, in particular to a batch scraping type sand wall texture coating and a preparation method thereof, wherein the batch scraping type sand wall texture coating comprises the following components in parts by mass: 200 parts of water 180-type organic silicon-containing powder, 2-2.4 parts of modified cellulose, 2-3 parts of dispersing agent, 1.5-2.1 parts of defoaming agent, 25-30 parts of titanium dioxide, 12-15 parts of propylene glycol methyl ether acetate film-forming assistant, 16-20 parts of glycerol, 30-50 parts of river midstream gravel, 180 parts of pure acrylic emulsion 150-type organic silicon-containing powder, 2-6 parts of gas-phase silicon dioxide, 2.1-3.6 parts of dibutyl phthalate, 1.2-3.2 parts of flatting agent, 5-8 parts of inorganic thixotropic thickener, 1.2-2.4 parts of composite dispersing agent, 20-30 parts of calcined kaolin, 21-25 parts of redispersible rubber powder and 1.5-1.8 parts of mildew-proof bactericide; according to the invention, the midstream gravel of the river is adopted, the surface of the midstream gravel is usually arc-shaped after being washed by flowing water, so that the resistance in the construction process is reduced, the construction efficiency is improved, and meanwhile, the leveling agent is added, so that the flatness of the coating can be improved, including the phenomena of shrinkage prevention, orange peel prevention, sagging prevention and the like, and the batch scraping effect of batch scraping of the coating with the gravel feeling is improved.

Description

Scraping sand wall texture coating and preparation method thereof
Technical Field
The invention relates to the technical field of decorative coatings, in particular to a batch scraping type sand wall texture coating and a preparation method thereof.
Background
The texture coating shows a unique space visual angle by the infinite three-dimensional texture and the multiple-choice individual matching, is rich and vivid, and is novel. And the overall decoration style is satisfied by individual creation, so that the texture paint shows the unique style thereof in decoration! The novel artistic paint brings the smooth times of wall paint into the brand new times of natural environment-friendly concave-convex paint. Can replace wallpaper, and is more environment-friendly, economical and personalized. The texture coating has no radiation, light dead weight and vivid effect, and creates infinite special decorative effect through different construction processes, techniques and skills. This is a new decorative material, texture paint, which is popular in the market.
The batch scraping type sand wall texture coating has high construction requirements, but the existing batch scraping type sand wall texture coating usually adopts angular gravels, so that the construction difficulty is increased.
Disclosure of Invention
The purpose of the invention is: overcomes the defects in the prior art and provides the batch scraping sand wall texture coating with low construction requirements and the preparation method thereof.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows:
a batch scraping type sand wall texture coating comprises the following components in parts by mass: 200 parts of water 180-type organic silicon-containing powder, 2-2.4 parts of modified cellulose, 2-3 parts of dispersing agent, 1.5-2.1 parts of defoaming agent, 25-30 parts of titanium dioxide, 12-15 parts of propylene glycol methyl ether acetate film-forming assistant, 16-20 parts of glycerol, 30-50 parts of river midstream gravel, 180 parts of pure acrylic emulsion 150-type organic silicon-containing powder, 2-6 parts of gas-phase silicon dioxide, 2.1-3.6 parts of dibutyl phthalate, 1.2-3.2 parts of flatting agent, 5-8 parts of inorganic thixotropic thickener, 1.2-2.4 parts of composite dispersing agent, 20-30 parts of calcined kaolin, 21-25 parts of redispersible rubber powder and 1.5-1.8 parts of mildew-proof bactericide.
Further, the modified cellulose is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio of the cellulose inorganic acid ester to the carboxymethyl cellulose to the hydroxypropyl methyl cellulose is 1:1.2-1.8: 2.
Further, the compound dispersing agent is a mixture of sodium phosphate and sodium tripolyphosphate, and the mass ratio of the compound dispersing agent to the sodium tripolyphosphate is 2-3: 1.
Further, the particle size of the gravel at the midstream of the river is 40-100 meshes, wherein the proportion of 60 meshes or less accounts for 80%.
Furthermore, the inorganic thixotropic thickener is one of ATT-50, AT-33 and FDSS-5.
Furthermore, the redispersible rubber powder is a mixture of a lauric acid ethylene grafted tertiary carbonate ethylene copolymer and an organic silicon grafted ethylene-acetic acid copolymer, and the mass ratio of the lauric acid ethylene grafted tertiary carbonate ethylene copolymer to the organic silicon grafted ethylene-acetic acid copolymer is 1-3: 1.
Further, the flatting agent is one or more of a pure acrylic flatting agent, a fluorine modified acrylic flatting agent, a phosphate modified acrylic flatting agent and organic modified polysiloxane.
Furthermore, the leveling agent is a mixture of a phosphate modified acrylic leveling agent and organic modified polysiloxane, and the mass ratio of the phosphate modified acrylic leveling agent to the organic modified polysiloxane is 1: 2-3.
Furthermore, the mildew-proof bactericide selects one of JF-90, poly 2-methyl-4-isothiazoline-3-ketone compounds and poly 5-chloro-2-methyl-4-isothiazoline-3-ketone compounds.
A preparation method of a batch scraping type sand wall texture coating comprises the following steps:
(1) adjusting the stirring speed to 200-one-step stirring at 500r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into a reaction kettle, adjusting the rotation speed to 800-one-step stirring at 1000r/min, and continuously stirring for 20-30 min;
(2) adjusting the stirring speed to 300-; and continuously stirring for 20-30min to obtain the batch scraped sand textured coating.
The technical scheme adopted by the invention has the beneficial effects that:
the river midstream gravel is adopted, the surface of the river midstream gravel is usually in an arc shape after being washed by flowing water, and after edges and corners do not exist, the resistance in the construction process is reduced, the construction efficiency is improved, in addition, the raw materials of the river midstream gravel are easy to obtain, the cost is low, the production cost is obviously reduced, meanwhile, the leveling agent is also added, the flatness of the coating can be improved, the phenomena of shrinkage prevention, orange peel prevention, sagging prevention and the like are included, the surface tension between the coating and the substrate can be reduced, and the coating has good wettability to the substrate; the volatilization speed of the solvent is adjusted, the viscosity is reduced, the fluidity of the coating is improved, and the leveling time is prolonged; a very thin monolayer is formed on the surface of the coating film to provide uniform surface tension, thereby improving the batch effect of batch-scraping the gritty feel coating.
The plasticizer dibutyl phthalate is added in the invention, so that the strength of the coating film layer can be improved, and the spraying effect of the coating can be improved.
The composite dispersant in the invention adopts the mixture of sodium pyrophosphate and sodium tripolyphosphate, which can improve the system stability of the coating, and the sodium pyrophosphate can be used as a water softener, because the common water used for producing the water-based coating is usually high in hardness, and the addition of the sodium pyrophosphate can reduce the hardness of the water, and can be used as a dispersant and an emulsifier: sodium pyrophosphate has a deflocculation effect and plays an emulsification effect with the coating to improve the stability of the water-based coating; the aqueous solution of sodium tripolyphosphate is alkalescent (the pH value of 1% aqueous solution is about 9.7), and the aqueous solution of sodium tripolyphosphate forms suspension (similar to emulsion) in water with the pH value of 4.3-14, and the sodium tripolyphosphate can also make liquid and solid particles better dissolved in a liquid (such as water) medium, so that the sodium tripolyphosphate and the solid particles are mixed to be used as a dispersing agent, the system stability of the coating is improved, and the coating effect of the coating is improved.
According to the invention, by adding the inorganic thixotropic thickener, the addition amount of cellulose can be reduced, a paint film can be prevented from sagging, paint splashing in the coating process of the paint can be prevented, pigment deposition in the storage process of the paint can be prevented, liquid layering of the paint can be improved, and the appearance of the paint is uniform and consistent.
Detailed Description
The present invention will be described in further detail with reference to specific embodiments in order to make the above objects, features and advantages more apparent and understandable.
A batch scraping type sand wall texture coating comprises the following components in parts by mass: 200 parts of water 180-type organic silicon-containing powder, 2-2.4 parts of modified cellulose, 2-3 parts of dispersing agent, 1.5-2.1 parts of defoaming agent, 25-30 parts of titanium dioxide, 12-15 parts of propylene glycol methyl ether acetate film-forming assistant, 16-20 parts of glycerol, 30-50 parts of river midstream gravel, 180 parts of pure acrylic emulsion 150-type organic silicon-containing powder, 2-6 parts of gas-phase silicon dioxide, 2.1-3.6 parts of dibutyl phthalate, 1.2-3.2 parts of flatting agent, 5-8 parts of inorganic thixotropic thickener, 1.2-2.4 parts of composite dispersing agent, 20-30 parts of calcined kaolin, 21-25 parts of redispersible rubber powder and 1.5-1.8 parts of mildew-proof bactericide. The river midstream gravel is adopted, the surface of the river midstream gravel is usually in an arc shape after being washed by flowing water, and after edges and corners do not exist, the resistance in the construction process is reduced, the construction efficiency is improved, in addition, the raw materials of the river midstream gravel are easy to obtain, the cost is low, the production cost is obviously reduced, meanwhile, the leveling agent is also added, the flatness of the coating can be improved, the phenomena of shrinkage prevention, orange peel prevention, sagging prevention and the like are included, the surface tension between the coating and the substrate can be reduced, and the coating has good wettability to the substrate; the volatilization speed of the solvent is adjusted, the viscosity is reduced, the fluidity of the coating is improved, and the leveling time is prolonged; a very thin monolayer is formed on the surface of the coating film to provide uniform surface tension, thereby improving the batch effect of batch-scraping the gritty feel coating.
The plasticizer dibutyl phthalate is added in the invention, so that the strength of the coating film layer can be improved, and the spraying effect of the coating can be improved. According to the invention, by adding the inorganic thixotropic thickener, the addition amount of cellulose can be reduced, a paint film can be prevented from sagging, paint splashing in the coating process of the paint can be prevented, pigment deposition in the storage process of the paint can be prevented, liquid layering of the paint can be improved, and the appearance of the paint is uniform and consistent.
As a preferred embodiment, the modified cellulose in this example is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio is 1:1.2-1.8: 2.
As a preferred embodiment, the compound dispersant in the embodiment is a mixture of sodium orthophosphate and sodium tripolyphosphate, and the mass ratio of the mixture is 2-3: 1. The composite dispersant in the invention adopts the mixture of sodium pyrophosphate and sodium tripolyphosphate, which can improve the system stability of the coating, and the sodium pyrophosphate can be used as a water softener, because the common water used for producing the water-based coating is usually high in hardness, and the addition of the sodium pyrophosphate can reduce the hardness of the water, and can be used as a dispersant and an emulsifier: sodium pyrophosphate has a deflocculation effect and plays an emulsification effect with the coating to improve the stability of the water-based coating; the aqueous solution of sodium tripolyphosphate is alkalescent (the pH value of 1% aqueous solution is about 9.7), and the aqueous solution of sodium tripolyphosphate forms suspension (similar to emulsion) in water with the pH value of 4.3-14, and the sodium tripolyphosphate can also make liquid and solid particles better dissolved in a liquid (such as water) medium, so that the sodium tripolyphosphate and the solid particles are mixed to be used as a dispersing agent, the system stability of the coating is improved, and the coating effect of the coating is improved.
As a preferable embodiment, the particle size of the river midstream gravel in this example is 40 to 100 mesh, wherein 80% is the proportion of 60 mesh or less.
As a preferred embodiment, the inorganic thixotropic thickener in this example is one selected from ATT-50, AT-33 and FDSS-5.
As a preferred embodiment, the redispersible rubber powder in the embodiment is a mixture of vinyl laurate-grafted vinyl versatate copolymer and silicone-grafted ethylene-acetic acid copolymer, and the mass ratio of the mixture is 1-3: 1.
As a preferred embodiment, the leveling agent in this embodiment is one or more of a pure acrylic leveling agent, a fluorine-modified acrylic leveling agent, a phosphate-modified acrylic leveling agent, and an organic modified polysiloxane.
As a preferred embodiment, the mixture of the phosphate modified acrylic leveling agent and the organic modified polysiloxane is used as the leveling agent in the embodiment, and the mass ratio of the phosphate modified acrylic leveling agent to the organic modified polysiloxane is 1: 2-3.
As a preferred embodiment, the mildew-proof bactericide in this embodiment is one selected from JF-90, poly-2-methyl-4-isothiazolin-3-one compounds and poly-5-chloro-2-methyl-4-isothiazolin-3-one compounds.
A preparation method of a batch scraping type sand wall texture coating comprises the following steps:
(1) adjusting the stirring speed to 200-one-step stirring at 500r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into a reaction kettle, adjusting the rotation speed to 800-one-step stirring at 1000r/min, and continuously stirring for 20-30 min;
(2) adjusting the stirring speed to 300-; and continuously stirring for 20-30min to obtain the batch scraped sand textured coating.
Example 1
A batch scraping type sand wall texture coating comprises the following components in parts by mass: 180 parts of water, 2 parts of modified cellulose, 2 parts of a dispersing agent, 1.5 parts of a defoaming agent, 25 parts of titanium dioxide, 12 parts of a propylene glycol methyl ether acetate film-forming aid, 16 parts of glycerol, 30 parts of river midstream gravel, 150 parts of a pure acrylic emulsion, 2 parts of fumed silica, 2.1 parts of dibutyl phthalate, 1.2 parts of a leveling agent, 5 parts of an inorganic thixotropic thickening agent, 1.2 parts of a composite dispersing agent, 20 parts of calcined kaolin, 21 parts of redispersible rubber powder and 1.5 parts of a mildew-proof bactericide.
Wherein the modified cellulose is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio of the cellulose inorganic acid ester to the carboxymethyl cellulose to the hydroxypropyl methyl cellulose is 1:1.2: 2.
Wherein the composite dispersant is a mixture of sodium orthophosphate and sodium tripolyphosphate with the mass ratio of 2: 1.
The particle size of the river midstream gravel is 40-100 meshes, wherein the proportion of the gravel below 60 meshes accounts for 80%.
Wherein, the inorganic thixotropic thickener is ATT-50.
Wherein the redispersible rubber powder is a mixture of a lauric acid ethylene grafted tertiary carbonate ethylene copolymer and an organic silicon grafted ethylene-acetic acid copolymer, and the mass ratio of the redispersible rubber powder to the organic silicon grafted ethylene-acetic acid copolymer is 1.
Wherein, the flatting agent is a pure acrylic flatting agent.
Wherein, JF-90 is selected as the mildew-proof bactericide.
The preparation method of the batch scraping type sand wall texture coating comprises the following steps:
(1) adjusting the stirring speed to 200r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into a reaction kettle, adjusting the rotation speed to 800r/min, and continuously stirring for 30 min;
(2) adjusting the stirring speed to 300r/min, adding river midstream gravel and calcined kaolin into the reaction kettle, adjusting the rotation speed to 800r/min, and adjusting the pH value to be below 10 by using ammonia water; and continuously stirring for 30min to obtain the batch scraped sand textured coating.
Example 2
A batch scraping type sand wall texture coating comprises the following components in parts by mass: 180 parts of water, 2.1 parts of modified cellulose, 2.1 parts of a dispersing agent, 1.6 parts of a defoaming agent, 26 parts of titanium dioxide, 12 parts of a propylene glycol methyl ether acetate film-forming aid, 17 parts of glycerol, 35 parts of river midstream gravel, 160 parts of a pure acrylic emulsion, 3 parts of fumed silica, 2.4 parts of dibutyl phthalate, 1.5 parts of a leveling agent, 6 parts of an inorganic thixotropic thickening agent, 1.5 parts of a composite dispersing agent, 21 parts of calcined kaolin, 22 parts of redispersible rubber powder and 1.6 parts of a mildew-proof bactericide.
Wherein the modified cellulose is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio of the cellulose inorganic acid ester to the carboxymethyl cellulose to the hydroxypropyl methyl cellulose is 1:1.3: 2.
Wherein the composite dispersant is a mixture of sodium orthophosphate and sodium tripolyphosphate with the mass ratio of 2.1: 1.
The particle size of the river midstream gravel is 40-100 meshes, wherein the proportion of the gravel below 60 meshes accounts for 80%.
Wherein, the inorganic thixotropic thickener is ATT-50.
Wherein the redispersible rubber powder is a mixture of a lauric acid ethylene grafted tertiary carbonate ethylene copolymer and an organic silicon grafted ethylene-acetic acid copolymer, and the mass ratio of the two is 1.2: 1.
Wherein the leveling agent is a mixture of a phosphate modified acrylic leveling agent and organic modified polysiloxane, and the mass ratio of the phosphate modified acrylic leveling agent to the organic modified polysiloxane is 1: 2.1.
Wherein, JF-90 is selected as the mildew-proof bactericide.
The preparation method of the batch scraping type sand wall texture coating comprises the following steps:
(1) adjusting the stirring speed to 300r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into the reaction kettle, adjusting the rotation speed to 800r/min, and continuously stirring for 25 min;
(2) adjusting the stirring speed to 400r/min, adding river midstream gravel and calcined kaolin into the reaction kettle, adjusting the rotation speed to 800r/min, and adjusting the pH value to be below 10 by using ammonia water; and stirring for 25min to obtain the batch scraped sand textured coating.
Example 3
A batch scraping type sand wall texture coating comprises the following components in parts by mass: 200 parts of water, 2.2 parts of modified cellulose, 2.5 parts of a dispersing agent, 1.8 parts of a defoaming agent, 28 parts of titanium dioxide, 14 parts of a propylene glycol methyl ether acetate film-forming aid, 18 parts of glycerol, 40 parts of river midstream gravel, 160 parts of a pure acrylic emulsion, 4 parts of fumed silica, 3 parts of dibutyl phthalate, 1.8 parts of a leveling agent, 6 parts of an inorganic thixotropic thickener, 1.8 parts of a composite dispersing agent, 25 parts of calcined kaolin, 24 parts of redispersible rubber powder and 1.6 parts of a mildew-proof bactericide.
Wherein the modified cellulose is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio of the cellulose inorganic acid ester to the carboxymethyl cellulose to the hydroxypropyl methyl cellulose is 1:1.5: 2.
Wherein the composite dispersant is a mixture of sodium orthophosphate and sodium tripolyphosphate with the mass ratio of 2.5: 1.
The particle size of the river midstream gravel is 40-100 meshes, wherein the proportion of the gravel below 60 meshes accounts for 80%.
Wherein the inorganic thixotropic thickener is FDSS-5.
Wherein the redispersible rubber powder is a mixture of a lauric acid ethylene grafted tertiary carbonate ethylene copolymer and an organic silicon grafted ethylene-acetic acid copolymer, and the mass ratio of the two is 2: 1.
Wherein the leveling agent is a mixture of a phosphate modified acrylic leveling agent and organic modified polysiloxane, and the mass ratio of the phosphate modified acrylic leveling agent to the organic modified polysiloxane is 1: 2.5.
Wherein, the mildew-proof bactericide adopts a poly 2-methyl-4-isothiazoline-3-ketone compound.
The preparation method of the batch scraping type sand wall texture coating comprises the following steps:
(1) adjusting the stirring speed to 400r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into the reaction kettle, adjusting the rotation speed to 1000r/min, and continuously stirring for 25 min;
(2) adjusting the stirring speed to 500r/min, adding river midstream gravel and calcined kaolin into the reaction kettle, adjusting the rotation speed to 1000r/min, and adjusting the pH value to be below 10 by using ammonia water; and stirring for 25min to obtain the batch scraped sand textured coating.
Example 4
A batch scraping type sand wall texture coating comprises the following components in parts by mass: 200 parts of water, 2.3 parts of modified cellulose, 2.8 parts of a dispersing agent, 2 parts of a defoaming agent, 28 parts of titanium dioxide, 14 parts of a propylene glycol methyl ether acetate film-forming aid, 18 parts of glycerol, 45 parts of river midstream gravel, 170 parts of a pure acrylic emulsion, 5 parts of fumed silica, 3.2 parts of dibutyl phthalate, 3 parts of a leveling agent, 7 parts of an inorganic thixotropic thickener, 2.1 parts of a composite dispersing agent, 28 parts of calcined kaolin, 24 parts of redispersible rubber powder and 1.6 parts of a mildew-proof bactericide.
Wherein the modified cellulose is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio of the cellulose inorganic acid ester to the carboxymethyl cellulose to the hydroxypropyl methyl cellulose is 1:1.6: 2.
Wherein the composite dispersant is a mixture of sodium orthophosphate and sodium tripolyphosphate with the mass ratio of 2.8: 1.
The particle size of the river midstream gravel is 40-100 meshes, wherein the proportion of the gravel below 60 meshes accounts for 80%.
Wherein the inorganic thixotropic thickener is AT-33.
Wherein the redispersible rubber powder is a mixture of a lauric acid ethylene grafted tertiary carbonate ethylene copolymer and an organic silicon grafted ethylene-acetic acid copolymer, and the mass ratio of the two is 2.8: 1.
Wherein the leveling agent is a mixture of a phosphate modified acrylic leveling agent and organic modified polysiloxane, and the mass ratio of the phosphate modified acrylic leveling agent to the organic modified polysiloxane is 1: 2.8.
Wherein, the mildew-proof bactericide adopts a poly 2-methyl-4-isothiazoline-3-ketone compound.
The preparation method of the batch scraping type sand wall texture coating comprises the following steps:
(1) adjusting the stirring speed to 500r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into a reaction kettle, adjusting the rotating speed to 1000r/min, and continuously stirring for 20 min;
(2) adjusting the stirring speed to 600r/min, adding river midstream gravel and calcined kaolin into the reaction kettle, adjusting the rotation speed to 1000r/min, and adjusting the pH value to be below 10 by using ammonia water; and continuously stirring for 20min to obtain the batch scraped sand textured coating.
Example 5
A batch scraping type sand wall texture coating comprises the following components in parts by mass: 200 parts of water, 2.4 parts of modified cellulose, 3 parts of dispersion, 2.1 parts of defoaming agent, 30 parts of titanium dioxide, 15 parts of propylene glycol methyl ether acetate film-forming aid, 20 parts of glycerol, 50 parts of river midstream gravel, 180 parts of pure acrylic emulsion, 6 parts of fumed silica, 3.6 parts of dibutyl phthalate, 3.2 parts of flatting agent, 8 parts of inorganic thixotropic thickener, 2.4 parts of composite dispersant, 30 parts of calcined kaolin, 25 parts of redispersible rubber powder and 1.8 parts of mildew-proof bactericide.
Wherein the modified cellulose is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio of the cellulose inorganic acid ester to the carboxymethyl cellulose to the hydroxypropyl methyl cellulose is 1: 1.8: 2.
Wherein the composite dispersant is a mixture of sodium orthophosphate and sodium tripolyphosphate with the mass ratio of 3: 1.
The particle size of the river midstream gravel is 40-100 meshes, wherein the proportion of the gravel below 60 meshes accounts for 80%.
Wherein, the inorganic thixotropic thickener is ATT-50.
Wherein the redispersible rubber powder is a mixture of a lauric acid ethylene grafted tertiary carbonate ethylene copolymer and an organic silicon grafted ethylene-acetic acid copolymer, and the mass ratio of the two is 3: 1.
Wherein the leveling agent is a mixture of a phosphate modified acrylic leveling agent and organic modified polysiloxane, and the mass ratio of the phosphate modified acrylic leveling agent to the organic modified polysiloxane is 1: 3.
Wherein, the mildew-proof bactericide selects poly 5-chlorine-2-methyl-4-isothiazoline-3-ketone compound.
The preparation method of the batch scraping type sand wall texture coating comprises the following steps:
(1) adjusting the stirring speed to 500r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into a reaction kettle, adjusting the rotating speed to 1000r/min, and continuously stirring for 20 min;
(2) adjusting the stirring speed to 600r/min, adding river midstream gravel and calcined kaolin into the reaction kettle, adjusting the rotation speed to 1000r/min, and adjusting the pH value to be below 10 by using ammonia water; and continuously stirring for 30min to obtain the batch scraped sand textured coating.
The construction time of the texture coating materials prepared in examples 1 to 5 was measured, and the texture coating materials were prepared in the same plane and coated by a texture coating material spray gun for 0.5m2The batch scraping time in examples 1-5 was 10-20min shorter than that of the normal commercial textured coating.
In light of the foregoing description of the preferred embodiment of the present invention, it is to be understood that numerous changes and modifications may be made without departing from the spirit and scope of the invention as defined by the appended claims. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention. The technical scope of the present invention is not limited to the content of the specification, and must be determined according to the scope of the claims.

Claims (10)

1. The utility model provides a batch type sand wall feel coating which characterized in that: the composition comprises the following components in parts by mass: 200 parts of water 180-type organic silicon-containing powder, 2-2.4 parts of modified cellulose, 2-3 parts of dispersing agent, 1.5-2.1 parts of defoaming agent, 25-30 parts of titanium dioxide, 12-15 parts of propylene glycol methyl ether acetate film-forming assistant, 16-20 parts of glycerol, 30-50 parts of river midstream gravel, 180 parts of pure acrylic emulsion 150-type organic silicon-containing powder, 2-6 parts of gas-phase silicon dioxide, 2.1-3.6 parts of dibutyl phthalate, 1.2-3.2 parts of flatting agent, 5-8 parts of inorganic thixotropic thickener, 1.2-2.4 parts of composite dispersing agent, 20-30 parts of calcined kaolin, 21-25 parts of redispersible rubber powder and 1.5-1.8 parts of mildew-proof bactericide.
2. A batch-type gritty wall-like coating as claimed in claim 1, wherein: the modified cellulose is a mixture of cellulose inorganic acid ester, carboxymethyl cellulose and hydroxypropyl methyl cellulose, and the mass ratio of the cellulose inorganic acid ester to the carboxymethyl cellulose to the hydroxypropyl methyl cellulose is 1:1.2-1.8: 2.
3. A batch-type gritty wall-like coating as claimed in claim 1, wherein: the composite dispersing agent is a mixture of sodium orthophosphate and sodium tripolyphosphate with the mass ratio of 2-3: 1.
4. A batch-type gritty wall-like coating as claimed in claim 1, wherein: the particle size of the river midstream gravel is 40-100 meshes, wherein the proportion of below 60 meshes accounts for 80%.
5. A batch-type gritty wall-like coating as claimed in claim 1, wherein: the inorganic thixotropic thickener is one of ATT-50, AT-33 and FDSS-5.
6. A batch-type gritty wall-like coating as claimed in claim 1, wherein: the redispersible rubber powder is a mixture of a lauric acid ethylene grafted tertiary carbonate ethylene copolymer and an organic silicon grafted ethylene-acetic acid copolymer, and the mass ratio of the materials is 1-3: 1.
7. A batch-type gritty wall-like coating as claimed in claim 1, wherein: the flatting agent is one or more of a pure acrylic flatting agent, a fluorine modified acrylic flatting agent, a phosphate modified acrylic flatting agent and organic modified polysiloxane.
8. A batch-type gritty wall texture coating as claimed in claim 7, wherein: the leveling agent is a mixture of a phosphate modified acrylic leveling agent and organic modified polysiloxane, and the mass ratio of the phosphate modified acrylic leveling agent to the organic modified polysiloxane is 1: 2-3.
9. A batch-type gritty wall-like coating as claimed in claim 1, wherein: the mildew-proof bactericide is one of JF-90, poly 2-methyl-4-isothiazoline-3-one compounds and poly 5-chloro-2-methyl-4-isothiazoline-3-one compounds.
10. A method of preparing a batch sand textured coating as claimed in any one of claims 1 to 9, wherein: the preparation method comprises the following steps:
(1) adjusting the stirring speed to 200-one-step stirring at 500r/min, adding water, modified cellulose, a dispersing agent, a defoaming agent, titanium dioxide, a propylene glycol methyl ether acetate film-forming aid, glycerol, a pure acrylic emulsion, fumed silica, dibutyl phthalate, a leveling agent, an inorganic thixotropic thickener, a composite dispersing agent, redispersible rubber powder and a mildew-proof bactericide into a reaction kettle, adjusting the rotation speed to 800-one-step stirring at 1000r/min, and continuously stirring for 20-30 min;
(2) adjusting the stirring speed to 300-; and continuously stirring for 20-30min to obtain the batch scraped sand textured coating.
CN201910955203.9A 2019-10-09 2019-10-09 Scraping sand wall texture coating and preparation method thereof Pending CN110643243A (en)

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