CN102850862A - Golden color paint and preparation process thereof - Google Patents
Golden color paint and preparation process thereof Download PDFInfo
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- CN102850862A CN102850862A CN2012103195375A CN201210319537A CN102850862A CN 102850862 A CN102850862 A CN 102850862A CN 2012103195375 A CN2012103195375 A CN 2012103195375A CN 201210319537 A CN201210319537 A CN 201210319537A CN 102850862 A CN102850862 A CN 102850862A
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Abstract
The invention relates to a golden color paint which comprises the following components expressed in weight parts: 300 to 500 of water, 0.2 to 8 of cellulose, 0.1 to 4 of a pH conditioning agent, 1 to 15 of a dispersant, 0.5 to 12 of a wetting agent, 0.1 to 10 of an antiseptic, 0.1 to 10 of an antifoaming agent, 5 to 35 of an antifreezing agent, 8 to 40 of a film forming auxiliary agent, 0.5 to 15 of a mildew inhibitor, 0.1 to 12 of a leveling agent, 60 to 250 of aqueous gold powder, 250 to 500 of emulsion and 0.1 to 15 of a thickening agent. A preparation process for the golden color paint is to uniformly mix all the above-mentioned components at a temperature lower than 45 DEG C. The golden color paint has the advantages of strong weatherability and contamination resistance, a good droplet hanging effect and good adhesion during water sprinkling, no odor, no toxicity, a water-based property, environment friendliness, waterproofness, air permeability, mildew resistance, alkali resistance and easy and convenient construction; a paint film has high toughness and adhesion, strong ultraviolet resistance and corrosion resistance and high fullness and can comprehensively improve the service life and self-cleaning performance of a coating.
Description
Technical field
The present invention relates to paint field, particularly, the present invention relates to a kind of imitative metallic paint.
Background technology
At present needs to board, sculpture, artwork, brick, watt, the finishing material such as glasswork and other article carry out gold and decorate when processing, what mostly adopt is the treatment process of gilding, gold bar is processed into goldleaf, again goldleaf is attached to the surface of locating that to carry out article that gold decorate to process.Adopt the goldleaf treatment process of gilding, the seam that exists between adjacent two goldleaf is obvious, and the goldleaf outside surface is not wear-resisting, particularly is difficult to the problems such as stickup at rough local goldleaf, the more important thing is, such trimming cost is high, and is impracticable.
Progressively occur on the market replacing gilding treatment process with gold lacquer, carry out the brushing ormolu varnish at the golden article surface of processing of needs, now on the market ormolu varnish exists ultraviolet resistance and weather resistance poor mostly, and color and luster is darker, the metal sense is poor, complete rear 2 months color relations of general construction can be dimmed, become ash, the sense of forfeiture metal, the ormolu varnish of traditional double component need to add another kind of solidifying agent and be used in conjunction with paint during use in addition, causes the complicacy of construction, and the paint that adds solidifying agent must be finished in 4 hours, otherwise the gel phenomenon can occur and cause scrapping, thereby cause waste of material, generally painting surface drying time is 30 minutes, the time of doing solid work is 48 hours, sometimes reach a week, this has just prolonged construction period greatly, the waste labour resources.
CN 101033356A discloses a kind of gold paint, and its prescription is: resin 50 ~ 60%, metal powder or pearlescence 4 ~ 6%, yellow complex dyestuff 1 ~ 2%, tangerine look complex dyestuff 1 ~ 3%, gold powder 0.5 ~ 1.5%, UV light absorber 1 ~ 2%, thinner 25 ~ 33%, metal powder or pearlescence directing agent 0.3 ~ 0.6%, anti-settling agent 0.3 ~ 0.6%, butylacetate Mierocrystalline cellulose 2 ~ 3%.Manufacture craft may further comprise the steps: thinner and metal powder or pearlescence were soaked 30 ~ 50 minutes; Itself and 1/2nd resin are disperseed under 500 ~ 800 rpms rotating speed at leisure; The slurry that adding is made by 2/3rds resin and metal powder or pearlescence directing agent, anti-settling agent, gold powder high speed dispersion and the slurry of being made by 1-Methoxy-2-propyl acetate and butylacetate Mierocrystalline cellulose high speed dispersion; Add again yellow complex dyestuff, tangerine look complex dyestuff, UV light absorber.This gold paint and the goldleaf technique of gilding is compared more easy handling, but ultraviolet resistance and weather resistance are poor, and contains very gold in its raw material, and cost is higher, is unsuitable for using on a large scale.
CN 101372597A discloses a kind of flash gold lacquer and manufacture craft thereof, formed thermoplastic acrylic resin 45 ~ 55wt%, flash of light bronze 10 ~ 20wt%, thinner 18 ~ 25wt%, anti-settling agent 1 ~ 5wt%, flow agent 0.1 ~ 0.5wt%, synergistic agent 2 ~ 5wt%, ultraviolet absorbers 0 ~ 2wt% by thermoplastic acrylic resin, flash of light bronze, thinner, anti-settling agent, flow agent, synergistic agent and ultraviolet absorbers.This gold lacquer drying is comparatively rapid, but its weathering resistance, contamination resistance, sticking power are relatively poor, needs further to improve.
Therefore, develop a kind of weathering resistance, contamination resistance, sticking power excellence, and lower-cost gold lacquer is the metal difficult problem in affiliated field.
Summary of the invention
For the deficiencies in the prior art, one of purpose of the present invention is to provide the flammule lacquer.Flammule lacquer of the present invention refers to the general gold lacquer that is used for applying the figure of buddha, and the gold that also can be used for indoor and outdoor decoration or toy, artwork, furniture etc. is covered with paint, lacquer, colour wash, etc.
Described flammule lacquer comprises according to parts by weight:
Wherein, described water can be 300.1 parts, 300.2 parts, 301 parts, 305 parts, 360 parts, 390 parts, 430 parts, 480 parts, 495 parts, 498 parts, 499 parts, 499.7 parts, 499.8 parts, 499.9 parts etc.
Described Mierocrystalline cellulose can be 0.21 part, 0.22 part, 0.3 part, 0.5 part, 0.9 part, 1.3 parts, 1.9 parts, 3.8 parts, 4.9 parts, 6.4 parts, 7.7 parts, 7.8 parts, 7.9 parts, 7.98 parts, 7.99 parts etc.
Described pH adjusting agent can be 0.11 part, 0.12 part, 0.2 part, 0.8 part, 1.6 parts, 1.9 parts, 2.7 parts, 3.6 parts, 3.8 parts, 3.9 parts etc.
Described dispersion agent can be 1.1 parts, 1.2 parts, 1.6 parts, 2.1 parts, 3.6 parts, 5.7 parts, 8.2 parts, 10.1 parts, 13.7 parts, 14.7 parts, 14.8 parts, 14.9 parts etc.
Described wetting agent can be 0.51 part, 0.52 part, 0.53 part, 0.6 part, 0.9 part, 1.8 parts, 2.9 parts, 5.7 parts, 8.2 parts, 10.1 parts, 11.7 parts, 11.8 parts, 11.9 parts etc.
Described sanitas can be 0.11 part, 0.12 part, 0.2 part, 0.8 part, 1.6 parts, 3.4 parts, 6.8 parts, 8.1 parts, 9.5 parts, 9.7 parts, 9.8 parts, 9.9 parts etc.
Described defoamer can be 0.11 part, 0.12 part, 0.2 part, 0.8 part, 1.6 parts, 3.4 parts, 6.8 parts, 8.1 parts, 9.5 parts, 9.7 parts, 9.8 parts, 9.9 parts etc.
Described frostproofer can be 5.1 parts, 5.2 parts, 6 parts, 7.4 parts, 10.1 parts, 14.8 parts, 19.2 parts, 24.3 parts, 28.6 parts, 31.2 parts, 34.5 parts, 34.7 parts, 34.8 parts, 34.9 parts etc.
Described film coalescence aid can be 8.1 parts, 8.2 parts, 9 parts, 11.3 parts, 16.7 parts, 21.6 parts, 26.2 parts, 29.3 parts, 36.1 parts, 38 parts, 39 parts, 39.5 parts, 39.8 parts, 39.9 parts etc.
Described mould inhibitor can be 0.51 part, 0.52 part, 0.6 part, 1.1 parts, 1.8 parts, 3.2 parts, 5.6 parts, 8.2 parts, 10.1 parts, 13.2 parts, 14.6 parts, 14.7 parts, 14.8 parts, 14.9 parts etc.
Described flow agent can be 0.11 part, 0.12 part, 0.2 part, 0.8 part, 2.4 parts, 4.1 parts, 5.7 parts, 6.1 parts, 7.5 parts, 8.9 parts, 11.6 parts, 11.7 parts, 11.8 parts, 11.9 parts etc.
Described water-based bronze can be 60.1 parts, 60.2 parts, 65 parts, 76 parts, 94 parts, 115 parts, 162 parts, 184 parts, 207 parts, 229 parts, 243 parts, 247 parts, 248 parts, 249 parts etc.
Described emulsion can be 250.1 parts, 250.2 parts, 251 parts, 252 parts, 264 parts, 287 parts, 299 parts, 316 parts, 345 parts, 382 parts, 401 parts, 428 parts, 439 parts, 474 parts, 495 parts, 497 parts, 498 parts, 499 parts etc.
Described thickening material can be 0.11 part, 0.12 part, 0.2 part, 2.4 parts, 4.1 parts, 5.7 parts, 6.1 parts, 7.5 parts, 8.9 parts, 10.3 parts, 11.4 parts, 11.7 parts, 11.8 parts, 11.9 parts etc.
Preferably, described flammule lacquer comprises according to parts by weight:
Further preferred, described flammule lacquer comprises according to parts by weight:
Particularly preferably, described flammule lacquer is composed of the following components according to parts by weight:
Preferably, described water is deionized water.
Mierocrystalline cellulose among the present invention is the compound that contains the cellulosic structure unit, can comprise, for example, use acid, hydroxyl in the esterified celluloses such as lipid acid, nitric acid and the Mierocrystalline cellulose esterification product for preparing, by making the Mierocrystalline cellulose esterification product that contains the polymerizable unsaturated group and the multipolymer of polymerizable unsaturated monomer reaction preparation etc., the Mierocrystalline cellulose esterification product that wherein contains the polymerizable unsaturated group obtains by introduce the polymerizable unsaturated group in Mierocrystalline cellulose esterification product.
Preferably, described Mierocrystalline cellulose is a kind or at least 2 kinds combination in soluble cotton, butyric acid rhodia, rhodia, propionic acid rhodia, Natvosol, carboxymethyl cellulose, the ether of cellulose, particularly preferably butyric acid rhodia and/or Natvosol.
Mierocrystalline cellulose and filmogen have good consistency, and can improve resulting drying property of filming and adhesivity.
Preferably, described pH adjusting agent is selected from organic such as the AMP-95(2-amino-2-methyl-1-propyl alcohol of U.S.'s Angus (ANGUS) company) and/or mineral-type such as ammoniacal liquor, particularly preferably AMP-95.
Preferably, described dispersion agent is sodium salt dispersion agent and/or ammonium salt dispersion agent, is particularly preferably polycarboxylate sodium and/or poly carboxylic acid ammonium salt.
Preferably, described wetting agent is tensio-active agent, for example nonionogenic tenside.
Preferably, described sanitas is benzoglyoxaline ester class (Nordes EPW), Dao Weixier-75,1,1 kind or at least 2 kinds combination in 2-benzisothiazole-3-ketone (BIT), Kathon CG class (MIT and (B) CMIT) or the phenylformic acid are particularly preferably Kathon CG class and/or phenylformic acid.
Preferably, described defoamer is mineral oil antifoam agent or silicone antifoam agent.
Preferably, described frostproofer is ethylene glycol and/or propylene glycol, is particularly preferably ethylene glycol.
Preferably, described film coalescence aid is 2,2,4-trimethylammonium-1, a kind or at least 2 kinds combination in 3-pentanediol-mono isobutyrate, propylene glycol monomethyl ether, propandiol butyl ether, Diethylene Glycol butyl ether or the phenylcarbinol.
Preferably, described mould inhibitor is a kind or at least 2 kinds combination in isothiazolinone, nano-inorganic substance such as T200, organic zinc, organic Arylurea derivatives, derosal, the organic iodine, is particularly preferably derosal and/or organic iodine.
Preferably, described flow agent is urethane, particularly preferably aqueous polyurethane.
Described bronze is golden powder, is preferably a kind or at least 2 kinds combination in copper bronze, gold powder, blue or green bronze, the red bronze, is particularly preferably copper bronze and/or gold powder; Described water-based bronze refers to can be used for the bronze of water-borne coatings.
Preferably, described emulsion is styrene-acrylic resin emulsion and/or Emulsion acrylic resin, and one of ordinary skill in the art can be by commercial or utilize prior art/new technology to prepare.
Described flammule lacquer also can contain other material, such as sterilant, anti-settling agent, thinner, photostabilizer etc., and one of ordinary skill in the art can add as required.
One of purpose of the present invention also is to provide a kind of production technique of described flammule lacquer.
Described technique may further comprise the steps:
(1) add entry, add Mierocrystalline cellulose and pH adjusting agent under 300 ~ 500r/min stir speed (S.S.), improve stir speed (S.S.) to 700 ~ 900r/min, stir, temperature is controlled at below 45 ℃;
(2) add defoamer, frostproofer, film coalescence aid, wetting agent, reduce stir speed (S.S.) to 500 ~ 700r/min, temperature is controlled at below 45 ℃, is uniformly dispersed;
(3) add the water-based bronze, improve stir speed (S.S.) to 900 ~ 1100r/min, disperseed at least 15 minutes, temperature is controlled at below 45 ℃, is uniformly dispersed;
(4) reduce stir speed (S.S.) to 500 ~ 700r/min, add sanitas, mould inhibitor, stir, add emulsion, be uniformly dispersed, add flow agent, then stirred at least 5 minutes.
Preferably, step (4) is carried out afterwards step (5) and is added the thickening material adjusting viscosity, obtains the flammule lacquer.
Preferably, stir speed (S.S.) is 350 ~ 450r/min before step (1) middle adding Mierocrystalline cellulose and the pH adjusting agent, is particularly preferably 400r/min.
Preferably, stir speed (S.S.) is 750 ~ 850r/min after step (1) middle adding Mierocrystalline cellulose and the pH adjusting agent, is particularly preferably 800r/min.
Preferably, temperature is below 40 ℃ in the step (1).
Preferably, stir speed (S.S.) is 550 ~ 650r/min after the middle adding of step (2) defoamer, frostproofer, film coalescence aid, the wetting agent, is particularly preferably 600r/min.
Preferably, temperature is below 40 ℃ in the step (2).
Preferably, stir speed (S.S.) is 950 ~ 1050r/min after the middle adding of step (3) the water-based bronze, is particularly preferably 1000r/min.
Preferably, churning time is at least 20 minutes after the middle adding of step (3) the water-based bronze, particularly preferably stirs 30 minutes.
Preferably, temperature is below 40 ℃ in the step (3).
Preferably, stir speed (S.S.) is 550 ~ 650r/min in the step (4), is particularly preferably 600r/min.
Preferably, churning time is at least 8 minutes after the middle adding of step (4) flow agent, particularly preferably stirs 10 minutes.
Of the present invention part is parts by weight.
Parts by weight unit of the present invention is identical.
Weathering resistance, contamination resistance that the flammule that adopts the inventive method to prepare coats with lacquer are extremely strong, and water-sprinkling is hung the pearl effect, sticking power is good, tasteless nontoxic, aqueous, environmental protective, and waterproof and breathable, the mildew-resistant alkali resistant is constructed simple and convenient; Paint film is tough and tensile, strong adhesion, has extremely strong uvioresistant, erosion resistance, and high fullness ratio can improve work-ing life and the self-cleaning of coating comprehensively.
Embodiment
For ease of understanding the present invention, it is as follows that the present invention enumerates embodiment.Those skilled in the art should understand, described embodiment helps to understand the present invention, should not be considered as concrete restriction of the present invention.
Embodiment 1
(1) add 400 parts of deionized waters in reactor, start high speed dispersor, add 2 parts of Mierocrystalline celluloses and 1.5 parts of AMP-95 under the 400r/min stir speed (S.S.), improve stir speed (S.S.) to 800r/min, stir, temperature is controlled at below 40 ℃;
(2) add 2 parts of mineral oil antifoam agents, 10 parts of ethylene glycol, 30 parts of alcohol esters 12,6 parts of tensio-active agents, reduce stir speed (S.S.) to 600r/min, temperature is controlled at below 40 ℃, is uniformly dispersed;
(3) add 80 parts of water-based bronzes, improve stir speed (S.S.) to 1000r/min, disperseed 30 minutes, temperature is controlled at below 40 ℃, is uniformly dispersed;
(4) reduce stir speed (S.S.) to 600r/min, add 2 portions of sanitass, 8 parts of mould inhibitors, stir, add 400 parts of styrene-acrylic resin emulsions, be uniformly dispersed, add 2 parts of flow agents, then stirred 10 minutes.
(5) add 2 parts of thickening material adjusting viscosities, mix, obtain the flammule lacquer.
Embodiment 2
(1) add 500 parts of deionized waters in reactor, start high speed dispersor, add 8 parts of Mierocrystalline celluloses and 4 parts of AMP-95 under the 300r/min stir speed (S.S.), improve stir speed (S.S.) to 700r/min, stir, temperature is controlled at below 45 ℃;
(2) add 0.1 part of silicone antifoam agent, 5 parts of propylene glycol, 8 parts of propylene glycol monomethyl ethers, 0.5 part of tensio-active agent, reduce stir speed (S.S.) to 500r/min, temperature is controlled at below 45 ℃, is uniformly dispersed;
(3) add 60 parts of water-based bronzes, improve stir speed (S.S.) to 900r/min, disperseed 15 minutes, temperature is controlled at below 45 ℃, is uniformly dispersed;
(4) reduce stir speed (S.S.) to 700r/min, add 0.1 portion of sanitas, 15 parts of mould inhibitors, stir, add 500 parts of Emulsion acrylic resins, be uniformly dispersed, add 0.1 part of flow agent, then stirred 20 minutes.
(5) add 15 parts of thickening material adjusting viscosities, mix, obtain the flammule lacquer.
Embodiment 3
(1) add 300 parts of deionized waters in reactor, start high speed dispersor, add 0.2 part of Mierocrystalline cellulose and 0.1 part of ammoniacal liquor under the 500r/min stir speed (S.S.), improve stir speed (S.S.) to 900r/min, stir, temperature is controlled at below 38 ℃;
(2) add 10 parts of silicone antifoam agents, 35 parts of propylene glycol, 40 parts of phenylcarbinols, 12 parts of tensio-active agents, reduce stir speed (S.S.) to 700r/min, temperature is controlled at below 38 ℃, is uniformly dispersed;
(3) add 250 parts of water-based bronzes, improve stir speed (S.S.) to 1100r/min, disperseed 18 minutes, temperature is controlled at below 38 ℃, is uniformly dispersed;
(4) reduce stir speed (S.S.) to 500r/min, add 10 portions of sanitass, 0.5 part of mould inhibitor, stir, add 250 parts of Emulsion acrylic resins, be uniformly dispersed, add 12 parts of flow agents, then stirred 5 minutes.
(5) add 15 parts of thickening material adjusting viscosities, mix, obtain the flammule lacquer.
Embodiment 4
(1) add 350 parts of deionized waters in reactor, start high speed dispersor, add 1.4 parts of Mierocrystalline celluloses and 1 part of AMP-95 under the 350r/min stir speed (S.S.), improve stir speed (S.S.) to 750r/min, stir, temperature is controlled at below 41 ℃;
(2) add 3 parts of silicone antifoam agents, 8 parts of ethylene glycol, 16 parts of phenylcarbinols, 3 parts of tensio-active agents, reduce stir speed (S.S.) to 630r/min, temperature is controlled at below 41 ℃, is uniformly dispersed;
(3) add 210 parts of water-based bronzes, improve stir speed (S.S.) to 1050r/min, disperseed 21 minutes, temperature is controlled at below 41 ℃, is uniformly dispersed;
(4) reduce stir speed (S.S.) to 680r/min, add 8 portions of sanitass, 7 parts of mould inhibitors, stir, add 320 parts of Emulsion acrylic resins, be uniformly dispersed, add 4 parts of flow agents, then stirred 8 minutes.
(5) add 1.4 parts of thickening material adjusting viscosities, mix, obtain the flammule lacquer.
Comparative Examples 1
Take the disclosed flash gold lacquer of CN 101372597A as Comparative Examples.
Adopt GB/T9755-2001 that embodiment 1-4 and Comparative Examples 1 are tested, test result is as shown in table 1.
Table 1
Shown in upper table 1, it is reasonable that flammule of the present invention coats with lacquer each component concentration, cooperatively interacts, and makes it have excellent scrub resistance, water tolerance, artificial ageing resistance, resistance to soiling, alkali resistance and hydrophobicity.Simultaneously, can spray, brushing or roller coat be to matrix surface, has excellent decorative effect.
Applicant's statement, the present invention illustrates detailed process equipment and process flow process of the present invention by above-described embodiment, but the present invention is not limited to above-mentioned detailed process equipment and process flow process, does not mean that namely the present invention must rely on above-mentioned detailed process equipment and process flow process and could implement.The person of ordinary skill in the field should understand, any improvement in the present invention to the interpolation of the equivalence replacement of each raw material of product of the present invention and ancillary component, the selection of concrete mode etc., all drops within protection scope of the present invention and the open scope.
Claims (10)
1. a flammule coats with lacquer, and comprises according to parts by weight:
2. flammule lacquer as claimed in claim 1 is characterized in that, described flammule lacquer comprises according to parts by weight:
3. flammule lacquer as claimed in claim 1 is characterized in that, described flammule lacquer comprises according to parts by weight:
4. flammule lacquer as claimed in claim 1 is characterized in that, described flammule lacquer is composed of the following components according to parts by weight:
5. such as each described flammule lacquer of claim 1-4, it is characterized in that, described water is deionized water;
Preferably, described Mierocrystalline cellulose is a kind or at least 2 kinds combination in soluble cotton, butyric acid rhodia, rhodia, propionic acid rhodia, Natvosol, carboxymethyl cellulose, the ether of cellulose, particularly preferably butyric acid rhodia and/or Natvosol;
Preferably, described pH adjusting agent is AMP-95 and/or ammoniacal liquor, particularly preferably AMP-95;
Preferably, described dispersion agent is sodium salt dispersion agent and/or ammonium salt dispersion agent, is particularly preferably polycarboxylate sodium and/or poly carboxylic acid ammonium salt.
6. such as each described flammule lacquer of claim 1-5, it is characterized in that, described wetting agent is tensio-active agent, for example nonionogenic tenside;
Preferably, described sanitas is a kind or at least 2 kinds combination in benzoglyoxaline ester class, Dao Weixier-75, BIT, Kathon CG class or the phenylformic acid, is particularly preferably Kathon CG class and/or phenylformic acid;
Preferably, described defoamer is mineral oil antifoam agent or silicone antifoam agent;
Preferably, described frostproofer is ethylene glycol and/or propylene glycol, is particularly preferably ethylene glycol.
7. such as each described flammule lacquer of claim 1-6, it is characterized in that, described film coalescence aid is 2,2,4-trimethylammonium-1, a kind or at least 2 kinds combination in 3-pentanediol-mono isobutyrate, propylene glycol monomethyl ether, propandiol butyl ether, Diethylene Glycol butyl ether or the phenylcarbinol;
Preferably, described mould inhibitor is a kind or at least 2 kinds combination in isothiazolinone, nano-inorganic substance, organic zinc, organic Arylurea derivatives, derosal, the organic iodine, is particularly preferably derosal and/or organic iodine;
Preferably, described flow agent is urethane, particularly preferably aqueous polyurethane;
Preferably, described bronze is a kind or at least 2 kinds combination in copper bronze, gold powder, blue or green bronze, the red bronze, is particularly preferably copper bronze and/or gold powder;
Preferably, described emulsion is styrene-acrylic resin emulsion and/or Emulsion acrylic resin.
8. such as the production technique of each described flammule lacquer of claim 1-7, may further comprise the steps:
(1) add entry, add Mierocrystalline cellulose and pH adjusting agent under 300 ~ 500r/min stir speed (S.S.), improve stir speed (S.S.) to 700 ~ 900r/min, stir, temperature is controlled at below 45 ℃;
(2) add defoamer, frostproofer, film coalescence aid, wetting agent, reduce stir speed (S.S.) to 500 ~ 700r/min, temperature is controlled at below 45 ℃, is uniformly dispersed;
(3) add the water-based bronze, improve stir speed (S.S.) to 900 ~ 1100r/min, disperseed at least 15 minutes, temperature is controlled at below 45 ℃, is uniformly dispersed;
(4) reduce stir speed (S.S.) to 500 ~ 700r/min, add sanitas, mould inhibitor, stir, add emulsion, be uniformly dispersed, add flow agent, then stirred at least 5 minutes.
9. technique as claimed in claim 8 is characterized in that, step (4) is carried out afterwards step (5) and added the thickening material adjusting viscosity, obtains the flammule lacquer;
Preferably, stir speed (S.S.) is 350 ~ 450r/min before step (1) middle adding Mierocrystalline cellulose and the pH adjusting agent, is particularly preferably 400r/min;
Preferably, stir speed (S.S.) is 750 ~ 850r/min after step (1) middle adding Mierocrystalline cellulose and the pH adjusting agent, is particularly preferably 800r/min;
Preferably, temperature is below 40 ℃ in the step (1);
Preferably, stir speed (S.S.) is 550 ~ 650r/min after the middle adding of step (2) defoamer, frostproofer, film coalescence aid, the wetting agent, is particularly preferably 600r/min;
Preferably, temperature is below 40 ℃ in the step (2).
10. technique as claimed in claim 8 or 9 is characterized in that, adds in the step (3) that stir speed (S.S.) is 950 ~ 1050r/min after the water-based bronze, is particularly preferably 1000r/min;
Preferably, churning time is at least 20 minutes after the middle adding of step (3) the water-based bronze, particularly preferably stirs 30 minutes;
Preferably, temperature is below 40 ℃ in the step (3);
Preferably, stir speed (S.S.) is 550 ~ 650r/min in the step (4), is particularly preferably 600r/min;
Preferably, churning time is at least 8 minutes after the middle adding of step (4) flow agent, particularly preferably stirs 10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103195375A CN102850862A (en) | 2012-08-31 | 2012-08-31 | Golden color paint and preparation process thereof |
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| CN2012103195375A CN102850862A (en) | 2012-08-31 | 2012-08-31 | Golden color paint and preparation process thereof |
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Cited By (5)
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| CN104481106A (en) * | 2014-12-15 | 2015-04-01 | 广东玉兰装饰材料有限公司 | Wallpaper and preparation process of wallpaper |
| CN105176268A (en) * | 2015-10-19 | 2015-12-23 | 佛山市高明阳光逸采涂料有限公司 | Waterborne UV coloring agent and preparation method thereof |
| CN104119730B (en) * | 2014-08-06 | 2016-11-30 | 顾玉奎 | A kind of alkaline-resisting water-soluble colorful coating |
| CN109913061A (en) * | 2019-01-11 | 2019-06-21 | 河北晨阳工贸集团有限公司 | A kind of imitative copper ring water conservation paint and preparation method thereof |
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| CN104119730A (en) * | 2014-08-06 | 2014-10-29 | 吴江华诚复合材料科技有限公司 | Alkali-resisting water-based colorful coating |
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| CN105176268A (en) * | 2015-10-19 | 2015-12-23 | 佛山市高明阳光逸采涂料有限公司 | Waterborne UV coloring agent and preparation method thereof |
| CN109913061A (en) * | 2019-01-11 | 2019-06-21 | 河北晨阳工贸集团有限公司 | A kind of imitative copper ring water conservation paint and preparation method thereof |
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Application publication date: 20130102 |