CN104151975A - Aqueous reflection heat-insulation stone-imitation paint and preparation method thereof - Google Patents
Aqueous reflection heat-insulation stone-imitation paint and preparation method thereof Download PDFInfo
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- CN104151975A CN104151975A CN201410390537.3A CN201410390537A CN104151975A CN 104151975 A CN104151975 A CN 104151975A CN 201410390537 A CN201410390537 A CN 201410390537A CN 104151975 A CN104151975 A CN 104151975A
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Abstract
The invention discloses aqueous reflection heat-insulation stone-imitation paint and a preparation method thereof. The aqueous reflection heat-insulation stone-imitation paint comprises, by weight, 30-50% of base paint as an ingredient A, 12-25% of a protection colloidal solution as an ingredient B and 30-60% of varnish as an ingredient C. Through use of the above ingredients according to the above ratio and treatment on the base paint by a reflection heat-insulation technology, the aqueous reflection heat-insulation stone-imitation paint is obtained. The aqueous reflection heat-insulation stone-imitation paint has reflection heat-insulation effects, solves the problem that the existing aqueous multi-color paint has stone-imitation effects but heat-insulation and energy-saving effects, has strong decorative effects, is environmentally friendly, saves energy, is convenient for construction, can be operated easily and has a wide application prospect.
Description
Technical field
The present invention relates to building coating field, particularly a kind of water-based reflective insulation stone-like coating and preparation method thereof.
Background technology
Water bag water multicolor finish is very popular product innovation type in building coating industry in recent years, and product is taking physicochemical colloid technology and process for treating surface as theoretical basis; By the multiple gluey hydrate colour particle that varies in size, varies in color, in the external phase aqueous emulsion paint that even stable suspension disperses to be, through a construction molding, and the effect of decorative patterns of the artificial granite stone material of finished product can reach the degree of mixing the spurious with the genuine.
As disclosed in China Patent Publication No. CN103849280A " preparation method of the weather-proof water-in-water type artificial granite of a kind of overstable height multicolor finish "; China Patent Publication No. CN103319969A disclosed " a kind of environment-friendly type water type multicolor paint for water drum and preparation method thereof ".
Day by day ripe in the technical research of water bag water multi-color lacquer and application, but aspect energy-conservation or as common latex, there is no reflective insulation function, still could not meet the requirement of national energy-saving environmental protection.
Also there is the research about reflective heat-insulation paint both at home and abroad, utilize the reflective insulation principle of hollow glass micropearl to carry out heat preservation energy-saving to buildings.As disclosed in Chinese patent notification number CN102311690B " a kind of Waterborne exterior elastic reflective heat insulation coating and production method thereof ", but its color is single, is main greatly mainly with light color or white, can not meet the ornamental requirement of client's External Wall.
Summary of the invention
One of object of the present invention is just to provide a kind of water-based reflective insulation stone-like coating, this water-based reflective insulation stone-like coating is to be mainly applied to building wall, the coating of a aesthetic effect with high imitative degree grouan stone, base paint is given the effect with the external light and heat of reflection simultaneously, thereby make the color particle of paint reach reflective insulation function, meet the requirement of national environmental protection heat preservation energy-saving, accord with the demands of the market.
Two of the object of the invention is just to provide the preparation method of above-mentioned water-based reflective insulation stone-like coating.The object of the present invention is achieved like this:
A kind of water-based reflective insulation stone-like coating, is prepared from by the component of following weight percent:
A component as base paint: 30%～50%;
B component as protective colloid solution: 12%～25%;
C component as varnish: 30%～60%;
The wherein said A component as base paint is prepared from by the raw material of following mass percent:
Described protective colloid solution is prepared from by the raw material of following mass percent:
Water 85～94%;
Protective colloid 6～15%;
The B component of described protective colloid solution is prepared from by the raw material of following mass percent:
Water 85～94%;
Protective colloid 6～15%;
The described C component as varnish is prepared from by the raw material of following mass percent:
The ether of cellulose of described A component is methyl cellulose ether, cellulose ether, Walocel MT 20.000PV ether, hydroxyethyl ether cellulose, hydroxypropylcelluloether ether, TYLOSE 30000 or methylhydroxypropylcellulose ether.
The dispersion agent of described A component is polyacrylic acid dipersant.
The infrared reflecting paint of described A component is Hensel ALTIRIS advanced in years 550 or ALTIRIS 800, and they are the titanium whites with very high properties of infrared reflection, can need to recall shades of colour according to imitative stone effect, durable in use.
The thermal insulating filling of described A component is the hollow glass micro-ball of particle diameter 20-100 micron, due to its glass material, have good infrared barrier effect, glass also has stronger reflex action for sunlight, and its hollow structure is used in the effect that has good reduction thermal conductivity in coating in addition.
The film forming matter of described A component is the one in pure acrylic latex, Styrene And Chloroalkyl Acrylates copolymer emulsion and organosilicon crylic acid latex, has certain flexibility.
The negatively charged ion wetting agent of described A component is HG-6 or the Shanghai grid trade Co., Ltd 399 of Shanghai Hao Guan trading company.
The defoamer of described A component and C component is the composite of siloxane-based defoamer or siloxane-based defoamer.
The thickening material of described A component and C component is polyurethane-type thickening material or the swelling thickening material of alkali.
The pH adjusting agent of described A component is any one in 2-amino-2 methyl isophthalic acid propyl alcohol, aqueous sodium hydroxide solution, ammoniacal liquor.
The protective colloid of described A component and B component is zeopan.
The film coalescence aid of described C component is 2,2,4-trimethylammonium-1.3 pentanediol mono isobutyrate, dipropylene glycol methyl ether, dipropylene glycol butyl ether or propylene glycol.
The film forming matter of described C component is the one in pure acrylic latex, Styrene And Chloroalkyl Acrylates copolymer emulsion and organosilicon crylic acid latex, and water tolerance will be got well.
The sterilant of described C component is to be selected from isothiazoline alcohol/ketone mixtures or imdazole derivatives.
A preparation method for water-based reflective insulation stone-like coating, comprises the steps:
(1) prepare protective colloid solution in A component and the B component as protective colloid solution: protective colloid is added to the water in proportion, even with dispersion machine low rate mixing, stir 30min and become transparent colloidal liquid to make protective colloid solution in A component and the B component as protective colloid solution;
(2) prepare A component: ether of cellulose is added to the water in proportion, stir by dispersion machine middling speed until dissolve, then add dispersion agent, pH value conditioning agent, defoamer, stir until mix, according to this add infrared reflecting paint, thermal insulating filling high speed dispersion thereafter, until be uniformly dispersed, then add protective colloid solution, the thickening material in the A component of film forming matter, negatively charged ion wetting agent, step (1), and be uniformly mixed;
(3) prepare C component: by film forming matter, film coalescence aid, defoamer, thickening material, sterilant are added to the water successively in proportion, middling speed stirs, and mixes;
(4) granulation: A component use color paste toning prepared by step (2), according to the colored paint of imitative stone effect furnishing multiple color, the B component as protective colloid solution that adds step (1) to prepare described colored paint, forms AB mixture; And control look grain size by velocity of shear and time, and velocity of shear is at 100～1000r/min, and shear time is adjusted between 1～20min;
(5) prepare water-based reflective insulation stone-like coating: AB colour particles mixture prepared by step (4) adds in C component prepared by step (3), stir, both a kind of water-based reflective insulation stone-like coating.
The present invention compared with prior art tool has the following advantages:
The present invention's colorful dispersion used has decorative surface, improves the defect of conventional emulsion paint color dullness, forms marmorean decorative effect, has ornamental very by force.Colour particles of the present invention has reflective insulation function, and body of wall has been played to fine effect of heat insulation, belongs to green energy conservation product.The present invention has good environmental-protecting performance, good stability in storage and wall protection function, decoration functions, and construction is simple.
Embodiment:
Embodiment 1:
A kind of water-based reflective insulation stone-like coating, the component that contains following weight percent: as the A component 32% of base paint, as the B component 16% of protective colloid solution, as the C component 52% of varnish.
A component as base paint is prepared from by the raw material of following mass percent:
Protective colloid solution is prepared from by the raw material of following mass percent:
Water 93%;
Zeopan 7%.
B component as protective colloid solution is prepared from by the raw material of following mass percent:
Water 93%;
Zeopan 7%.
C component varnish comprises, by mass percentage:
The preparation method of embodiment 1, comprises the steps:
(1) prepare protective colloid solution in A component and the B component as protective colloid solution: protective colloid is added to the water in proportion, even with dispersion machine low rate mixing, stir 30min and become transparent colloidal liquid to make protective colloid solution in A component and the B component as protective colloid solution;
(2) prepare A component: ether of cellulose is added to the water, stir by dispersion machine middling speed until dissolve, then add dispersion agent, pH value conditioning agent, defoamer, stir until mix, thereafter add according to this infrared reflecting paint ALTIRIS 550, hollow glass micro-ball, high speed dispersion, until be uniformly dispersed, add again benzene emulsion, negatively charged ion wetting agent HG-6, protective colloid solution, thickening material, and be uniformly mixed;
(3) prepare C component: by organosilicon crylic acid latex, film coalescence aid, defoamer, thickening material, sterilant are added to the water successively, middling speed stirs, and mixes;
(4) granulation: A component use color paste toning prepared by step (2), according to the colored paint of imitative stone effect furnishing multiple color, the B component that adds step (1) to prepare colored paint, forms AB mixture according to component ratio; And control look grain size by velocity of shear and time, and velocity of shear is 200r/min, shear time is 3min.
(5) prepare water-based reflective insulation stone-like coating: AB colour particles mixture prepared by step (4) adds in C component prepared by step (3) according to ratio, stir, both a kind of water-based reflective insulation stone-like coating.
Embodiment 2:
A kind of water-based reflective insulation stone-like coating, the component that contains following weight percent: as the A component 38% of base paint, as the B component 20% of protective colloid solution, as the C component 42% of varnish.
A component as base paint is prepared from by the raw material of following mass percent:
Protective colloid solution is prepared from by the raw material of following mass percent:
Water 92%;
Zeopan 8%.
B component as protective colloid solution is prepared from by the raw material of following mass percent:
Water 92%;
Zeopan 8%.
C component as varnish is prepared from by the raw material of following mass percent:
The preparation method of embodiment 2, comprises the steps:
(1) prepare protective colloid solution in A component and the B component as protective colloid solution: protective colloid is added to the water in proportion, even with dispersion machine low rate mixing, stir 30min and become transparent colloidal liquid to make protective colloid solution in A component and the B component as protective colloid solution;
(2) prepare A component: ether of cellulose is added to the water, stir by dispersion machine middling speed until dissolve, then add dispersion agent, pH value conditioning agent, defoamer, stir until mix, thereafter add according to this infrared reflecting paint ALTIRIS 550, hollow glass micro-ball, high speed dispersion, until be uniformly dispersed, add again benzene emulsion, negatively charged ion wetting agent HG-6, protective colloid solution, thickening material, and be uniformly mixed;
(3) prepare C component: by organosilicon crylic acid latex, film coalescence aid, defoamer, thickening material, sterilant are added to the water successively, middling speed stirs, and mixes;
(4) granulation: A component use color paste toning prepared by step (2), according to the colored paint of imitative stone effect furnishing multiple color, the B component that adds step (1) to prepare colored paint, forms AB mixture according to component ratio; And control look grain size by velocity of shear and time, and velocity of shear is 200r/min, shear time is 3min.
(5) prepare water-based reflective insulation stone-like coating: AB colour particles mixture prepared by step (4) adds in C component prepared by step (3) according to ratio, stir, both a kind of water-based reflective insulation stone-like coating.
Above-described embodiment 1 and embodiment 2 carry out the detection of various indexs by " HGT 4343-2012 aqueous colorful building coating " and the standard of " JG/T235-2008 architectural reflective heat-insulation paint ", and partial results is as shown in the table:
More than show and described ultimate principle of the present invention, principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and specification sheets, describes just illustrates principle of the present invention; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (13)
1. a water-based reflective insulation stone-like coating, is prepared from by the component of following weight percent:
A component as base paint: 30%～50%;
B component as protective colloid solution: 12%～25%;
C component as varnish: 30%～60%;
The wherein said A component as base paint is prepared from by the raw material of following mass percent:
Described protective colloid solution is prepared from by the raw material of following mass percent:
Water 85～94%;
Protective colloid 6～15%;
The B component of described protective colloid solution is prepared from by the raw material of following mass percent:
Water 85～94%;
Protective colloid 6～15%;
The described C component as varnish is prepared from by the raw material of following mass percent:
2. water-based reflective insulation stone-like coating according to claim 1, it is characterized in that, the ether of cellulose of described A component is methyl cellulose ether, cellulose ether, Walocel MT 20.000PV ether, hydroxyethyl ether cellulose, hydroxypropylcelluloether ether, TYLOSE 30000 or methylhydroxypropylcellulose ether.
3. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the dispersion agent of described A component is polyacrylic acid dipersant.
4. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the infrared reflecting paint of described A component is Hensel ALTIRIS advanced in years 550 or ALTIRIS 800.
5. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the thermal insulating filling of described A component is the hollow glass micro-ball of particle diameter 20-100 micron.
6. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the film forming matter of described A component and C component is the one in pure acrylic latex, Styrene And Chloroalkyl Acrylates copolymer emulsion and organosilicon crylic acid latex.
7. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the defoamer of described A component and C component is the composite of siloxane-based defoamer or siloxane-based defoamer.
8. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the thickening material of described A component and C component is polyurethane-type thickening material or the swelling thickening material of alkali.
9. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the pH adjusting agent of described A component is any one in 2-amino-2 methyl isophthalic acid propyl alcohol, aqueous sodium hydroxide solution, ammoniacal liquor.
10. water-based reflective insulation stone-like coating according to claim 1, is characterized in that, the protective colloid of described A component and B component is zeopan.
11. water-based reflective insulation stone-like coatings according to claim 1, is characterized in that, the film coalescence aid of described C component is 2,2,4-trimethylammonium-1.3 pentanediol mono isobutyrate, dipropylene glycol methyl ether, dipropylene glycol butyl ether or propylene glycol.
12. water-based reflective insulation stone-like coatings according to claim 1, is characterized in that, the sterilant of described C component is to be selected from isothiazoline alcohol/ketone mixtures or imdazole derivatives.
13. 1 kinds according to the preparation method of the water-based reflective insulation stone-like coating described in claim 1 to 12 any one claim, it is characterized in that, comprises the steps:
(1) prepare protective colloid solution in A component and the B component as protective colloid solution: protective colloid is added to the water in proportion, even with dispersion machine low rate mixing, stir 30min and become transparent colloidal liquid to make protective colloid solution in A component and the B component as protective colloid solution;
(2) prepare A component: ether of cellulose is added to the water in proportion, stir by dispersion machine middling speed until dissolve, then add dispersion agent, pH value conditioning agent, defoamer, stir until mix, according to this add infrared reflecting paint, thermal insulating filling high speed dispersion thereafter, until be uniformly dispersed, then add protective colloid solution, the thickening material in the A component of film forming matter, negatively charged ion wetting agent, step (1), and be uniformly mixed;
(3) prepare C component: by film forming matter, film coalescence aid, defoamer, thickening material, sterilant are added to the water successively in proportion, middling speed stirs, and mixes;
(4) granulation: A component use color paste toning prepared by step (2), according to the colored paint of imitative stone effect furnishing multiple color, the B component as protective colloid solution that adds step (1) to prepare described colored paint, forms AB mixture; And control look grain size by velocity of shear and time, and velocity of shear is at 100～1000r/min, and shear time is adjusted between 1～20min;
(5) prepare water-based reflective insulation stone-like coating: AB colour particles mixture prepared by step (4) adds in C component prepared by step (3), stir, both a kind of water-based reflective insulation stone-like coating.
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| CN104530874A (en) * | 2015-01-22 | 2015-04-22 | 北京莱恩斯涂料有限公司 | High-washing-resistance colorful coating and preparation method thereof |
| CN104804601A (en) * | 2015-04-23 | 2015-07-29 | 东莞市金基环保科技有限公司 | High-performance heat-insulation heat-preservation multicolor paint |
| CN104845478A (en) * | 2015-05-27 | 2015-08-19 | 浙江大学自贡创新中心 | Water-based light-emitting multicolor paint and preparation method thereof |
| CN105017906A (en) * | 2015-08-14 | 2015-11-04 | 刘善江 | Water-in-water multi-color water paint and preparation method thereof |
| CN105419543A (en) * | 2015-12-30 | 2016-03-23 | 江苏日出化工有限公司 | Colorful reflection heat insulation coating layer manufacturing method |
| CN105601177A (en) * | 2015-12-18 | 2016-05-25 | 三棵树涂料股份有限公司 | Thermal insulation reflective stone-like coating and preparation method thereof |
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| CN109554046A (en) * | 2018-11-30 | 2019-04-02 | 沈阳理工大学 | A kind of environment-friendly type aqueous heat reflection multicolor finish and preparation method thereof |
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| CN104804601A (en) * | 2015-04-23 | 2015-07-29 | 东莞市金基环保科技有限公司 | High-performance heat-insulation heat-preservation multicolor paint |
| CN106280817A (en) * | 2015-05-12 | 2017-01-04 | 上海三银涂料科技股份有限公司 | Aqueous colorful luminous paint and preparation method thereof |
| CN104845478A (en) * | 2015-05-27 | 2015-08-19 | 浙江大学自贡创新中心 | Water-based light-emitting multicolor paint and preparation method thereof |
| CN105017906A (en) * | 2015-08-14 | 2015-11-04 | 刘善江 | Water-in-water multi-color water paint and preparation method thereof |
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| CN105419543A (en) * | 2015-12-30 | 2016-03-23 | 江苏日出化工有限公司 | Colorful reflection heat insulation coating layer manufacturing method |
| CN105419543B (en) * | 2015-12-30 | 2017-09-29 | 江苏日出化工有限公司 | Colorful reflective insulation coating preparation method |
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| CN106381042A (en) * | 2016-09-07 | 2017-02-08 | 广西大学 | Water-in-water antimicrobial multicolor paint and preparation method thereof |
| CN106752595A (en) * | 2017-03-05 | 2017-05-31 | 江苏华盛节能科技有限公司 | A kind of stone imitation material |
| CN107129735A (en) * | 2017-06-08 | 2017-09-05 | 广东东艺宝建材有限公司 | A kind of artificial granite speckle multicolor finish of waterproof and heat-insulating and preparation method thereof |
| CN107118645A (en) * | 2017-06-08 | 2017-09-01 | 广东东艺宝建材有限公司 | A kind of waterproof artificial granite speckle multicolor finish and preparation method thereof |
| CN109233413A (en) * | 2018-09-18 | 2019-01-18 | 广东福莱特建筑材料有限公司 | A kind of inorganic coating and preparation method thereof with reflective insulation performance |
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| CN109554046A (en) * | 2018-11-30 | 2019-04-02 | 沈阳理工大学 | A kind of environment-friendly type aqueous heat reflection multicolor finish and preparation method thereof |
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| CN114702867A (en) * | 2022-04-06 | 2022-07-05 | 湖南大途新材料有限公司 | Aerogel thermal insulation decorative water-based paint, and preparation method and application thereof |
| CN116144234A (en) * | 2022-09-08 | 2023-05-23 | 广东立时涂料科技有限公司 | Composite sand-in-water constant-temperature ecological stone coating |
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Effective date of registration: 20220107 Address after: 201799 6th floor, building 1, 1318 Xiangda East Road, Qingpu District, Shanghai Patentee after: Crocodile Nica (Shanghai) new materials Co.,Ltd. Address before: Floor 17, No. 468, Changshou Road, Putuo District, Shanghai 200060 Patentee before: ALLIGATOR COATINGS (SHANGHAI) CO.,LTD. Patentee before: Shanghai Shen Zhen Enterprise Development Co., Ltd. |
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