CN103642344B - A kind of texture multicolor finish and preparation method thereof - Google Patents
A kind of texture multicolor finish and preparation method thereof Download PDFInfo
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- CN103642344B CN103642344B CN201310742215.6A CN201310742215A CN103642344B CN 103642344 B CN103642344 B CN 103642344B CN 201310742215 A CN201310742215 A CN 201310742215A CN 103642344 B CN103642344 B CN 103642344B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000006185 dispersion Substances 0.000 claims abstract description 54
- 239000002994 raw material Substances 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 20
- 239000004576 sand Substances 0.000 claims abstract description 20
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 19
- 239000000126 substance Substances 0.000 claims description 19
- -1 Polyoxyethylene octylphenol Polymers 0.000 claims description 18
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 18
- 239000002562 thickening agent Substances 0.000 claims description 13
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- IPGANOYOHAODGA-UHFFFAOYSA-N dilithium;dimagnesium;dioxido(oxo)silane Chemical compound [Li+].[Li+].[Mg+2].[Mg+2].[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O IPGANOYOHAODGA-UHFFFAOYSA-N 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 9
- 239000003513 alkali Substances 0.000 claims description 9
- 239000004816 latex Substances 0.000 claims description 9
- 229920000126 latex Polymers 0.000 claims description 9
- 230000008961 swelling Effects 0.000 claims description 9
- 239000004408 titanium dioxide Substances 0.000 claims description 9
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 8
- 239000005995 Aluminium silicate Substances 0.000 claims description 8
- PRPAGESBURMWTI-UHFFFAOYSA-N [C].[F] Chemical compound [C].[F] PRPAGESBURMWTI-UHFFFAOYSA-N 0.000 claims description 8
- 235000012211 aluminium silicate Nutrition 0.000 claims description 8
- 238000007599 discharging Methods 0.000 claims description 8
- 239000000839 emulsion Substances 0.000 claims description 8
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 8
- 239000004579 marble Substances 0.000 claims description 8
- WMGSQTMJHBYJMQ-UHFFFAOYSA-N aluminum;magnesium;silicate Chemical compound [Mg+2].[Al+3].[O-][Si]([O-])([O-])[O-] WMGSQTMJHBYJMQ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- QSSDFXGXUGCLSY-UHFFFAOYSA-N 3-[3-(3-butoxypropoxy)propoxy]propan-1-ol Chemical compound CCCCOCCCOCCCOCCCO QSSDFXGXUGCLSY-UHFFFAOYSA-N 0.000 claims description 6
- 239000002585 base Substances 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 claims description 6
- 238000005469 granulation Methods 0.000 claims description 4
- 230000003179 granulation Effects 0.000 claims description 4
- 239000000843 powder Substances 0.000 abstract description 15
- 229920000642 polymer Polymers 0.000 abstract description 12
- 239000011248 coating agent Substances 0.000 abstract description 9
- 238000000576 coating method Methods 0.000 abstract description 9
- 239000000463 material Substances 0.000 abstract description 8
- 239000011435 rock Substances 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 7
- 239000013543 active substance Substances 0.000 abstract description 6
- 239000001913 cellulose Substances 0.000 abstract description 6
- 229920002678 cellulose Polymers 0.000 abstract description 6
- 238000004581 coalescence Methods 0.000 abstract description 6
- 239000010438 granite Substances 0.000 abstract description 6
- 230000008719 thickening Effects 0.000 abstract description 6
- 230000014759 maintenance of location Effects 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000007921 spray Substances 0.000 abstract description 4
- MOVRNJGDXREIBM-UHFFFAOYSA-N aid-1 Chemical compound O=C1NC(=O)C(C)=CN1C1OC(COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C(NC(=O)C(C)=C2)=O)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C(NC(=O)C(C)=C2)=O)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C(NC(=O)C(C)=C2)=O)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)CO)C(O)C1 MOVRNJGDXREIBM-UHFFFAOYSA-N 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract description 3
- 239000003973 paint Substances 0.000 abstract description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 9
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 8
- 239000011734 sodium Substances 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 229910000019 calcium carbonate Inorganic materials 0.000 description 4
- 229920005646 polycarboxylate Polymers 0.000 description 4
- 229920002635 polyurethane Polymers 0.000 description 4
- 239000004814 polyurethane Substances 0.000 description 4
- 229920001817 Agar Polymers 0.000 description 3
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 description 3
- 239000008272 agar Substances 0.000 description 3
- 229940077388 benzenesulfonate Drugs 0.000 description 3
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 3
- 239000001863 hydroxypropyl cellulose Substances 0.000 description 3
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 description 3
- 239000010977 jade Substances 0.000 description 3
- WMOVHXAZOJBABW-UHFFFAOYSA-N tert-butyl acetate Chemical compound CC(=O)OC(C)(C)C WMOVHXAZOJBABW-UHFFFAOYSA-N 0.000 description 3
- 238000010276 construction Methods 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000004500 asepsis Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
The invention discloses a kind of texture multicolor finish, this coating is by A, B two component be added with appropriate mill base hybrid modulation and form, and the mass ratio of component A and B component is 1: 3 to 3: 1; Each raw material in component A by percentage to the quality, includes high molecular polymer 10% ~ 60%, powder 5% ~ 50%, Mierocrystalline cellulose 0.3% ~ 8%, sand powder 5% ~ 50%, gelifying agent 0.1% ~ 30%, tensio-active agent 0.1% ~ 10%, water 10% ~ 60%; Each raw material in B component by percentage to the quality, includes high molecular polymer 10% ~ 80%, dispersion agent 0.1% ~ 5%, thickening material 0.1% ~ 5%, film coalescence aid 1% ~ 15%, water 5% ~ 70%.Its preparation method comprises component A preparation, B component preparation and finished product preparation.Manufacturing process of the present invention is simple, with low cost, also can have the coarse texture of rock itself, have the high simulated effect of natural granite after spray mo(u)lding drying while presenting rock decorative pattern, and tint retention is good, not fugitive color, is the decorative paint of building trade.
Description
Technical field
The present invention relates to a kind of aqueous architectural coating, specifically a kind of texture multicolor finish and preparation method thereof.
Background technology
Water-soluble colorful coating is a kind of novel environment protecting building paint, can obtain multiple color mix particles in the exterior decorative effect of one by disposable spray finishing construction.This coating is by two immiscible phase composites, and wherein one is disperse phase mutually, and another is external phase (dispersion medium) mutually.Disperse phase contains multiple different colours and difform color grain; these color grains are immiscible; stably suspended dispersed is in external phase, shows rich and varied and multi-level decorative effect, can replace the true stone external wall decorative material such as grouan, marble after construction.Water-soluble colorful coating compares these true stone finishing material, there is lightweight, the feature such as strong adhesion, snappiness are good, water-fast, stain resistant, ageing-resistant and environment-protecting asepsis, be applied in external decoration of high-rise building, solving the potential safety hazards such as brought falling from high altitude long neglected and in disrepair.Water-soluble colorful coating can imitate the decorative pattern of natural granite or marble, acquisition safety and environmental protection, attractive appearance, excellent property, the novel decorative coating that cost is low.But at present the color dot of multicolor finish is all flat, does not have the texture that rock itself is coarse, color is easily with exposing to the sun and rain and fade all the year round.
Summary of the invention
Technical problem to be solved by this invention is for above-mentioned prior art present situation, and provides that tint retention is good, not fugitive color have a kind of texture multicolor finish of the coarse texture of rock itself and natural granite height simulated effect.
The present invention solves the problems of the technologies described above adopted technical scheme: a kind of texture multicolor finish, and this coating is by A, B two component be added with appropriate mill base hybrid modulation and form, and the mass ratio of component A and B component is 1: 3 to 3: 1; Each raw material in component A by percentage to the quality, includes high molecular polymer 10% ~ 60%, powder 5% ~ 50%, Mierocrystalline cellulose 0.3% ~ 8%, sand powder 5% ~ 50%, gelifying agent 0.1% ~ 30%, tensio-active agent 0.1% ~ 10%, water 10% ~ 60%; Each raw material in B component by percentage to the quality, includes high molecular polymer 10% ~ 80%, dispersion agent 0.1% ~ 5%, thickening material 0.1% ~ 5%, film coalescence aid 1% ~ 15%, water 5% ~ 70%.
High molecular polymer in above-mentioned component A is one or more in pure acrylic acid polymkeric substance, organosilicon-modified acrylic polymkeric substance and styrenated acrylic's polymkeric substance; High molecular polymer in above-mentioned B component is one or more in organosilicon crylic acid latex and fluorine carbon emulsion.
Powder in above-mentioned component A is one or more in titanium dioxide, talcum powder, calcium carbonate, barium sulfate and kaolin.
Mierocrystalline cellulose in above-mentioned component A is one or more in Walocel MT 20.000PV, Natvosol and hydroxypropylcellulose.
Sand powder in above-mentioned component A is one or more in the color sand of 120 order to 180 object white marbles, the color sand of Snow Flower White and the color sand of careless white jade.
Gelifying agent in above-mentioned component A is one or more in neusilin, lithium magnesium silicate, organobentonite and agar powder.
Tensio-active agent in above-mentioned component A is one or more in polycarboxylate sodium, polyoxyethylene octylphenol ether, sodium alkyl benzene sulfonate and alkyl phenol ethoxylates.
Dispersion agent in above-mentioned B component is aqueous high molecular hyper-dispersant; Thickening material in above-mentioned B component is one or more in the swelling associative thickener of hydrophobically-modified alkali and aqueous polyurethane associative thickener.
Film coalescence aid in above-mentioned B component is one or more in alcohol ester 12, Tri(propylene glycol)butyl ether,mixture of isomers, tert.-butyl acetate and ethylene glycol.
The preparation method of a kind of texture multicolor finish of the present invention, the method comprises component A preparation, B component preparation and finished product preparation successively;
One, component A preparation comprise the following steps: following raw material by mass percentage:
A), the water of 10% ~ 60% is poured into the Scattered Kettle of dispersion machine, in dispersing speed be add under the condition of 300r/min ~ 800r/min 0.3% ~ 8% Mierocrystalline cellulose, dispersion 10min ~ 30min;
B), add in Scattered Kettle described in step a 0.1% ~ 10% tensio-active agent, dispersion 10min ~ 30min;
C), add in Scattered Kettle described in step b 5% ~ 50% powder, adjustment dispersing speed is 800r/min ~ 1500r/min, dispersion 10min ~ 30min;
D), add in Scattered Kettle described in step c 5% ~ 50% sand powder, dispersion 10min ~ 30min;
E), add in Scattered Kettle described in steps d 10% ~ 60% high molecular polymer, dispersion 20min ~ 50min;
F), add in Scattered Kettle described in step e 0.1% ~ 30% gelifying agent, adjustment dispersing speed is 1600r/min ~ 3200r/min, dispersion 10min ~ 20min, discharging obtains component A;
Described B component preparation comprises the following steps: following raw material by mass percentage:
G), pouring in the Scattered Kettle of dispersion machine by the high molecular polymer of 10% ~ 80% and the water of 5% ~ 70%, is disperse 10min ~ 30min under the condition of 300r/min ~ 1000r/min in dispersing speed;
H), add in Scattered Kettle described in step g the dispersion agent of 0.1% ~ 5%, the film coalescence aid of 1% ~ 15% and 0.1% ~ 5% thickening material, dispersion 10min ~ 30min, discharging obtains B component;
Described finished product preparation comprises the following steps:
I), be in mass ratio 1: 3 to 3: 1 ratio extract component A and B component;
J), by the B component of said extracted put into Scattered Kettle, the rotating speed of adjustment dispersion machine is 200r/min ~ 600r/min;
K), by mill base by component A furnishing shades of colour, then the component A of furnishing shades of colour is joined in the Scattered Kettle described in step I and disperse granulation, can this product be obtained.
Compared with prior art, a kind of texture multicolor finish of the present invention, not only possesses the advantage that traditional multicolor finish can imitate natural granite or marble decorative pattern, and coating of the present invention is through a spray mo(u)lding, also there is after drying the coarse texture of rock itself while presenting rock decorative pattern, have the high simulated effect of natural granite, and tint retention is good, not fugitive color, can show rich and varied and multi-level decorative effect.Manufacture craft of the present invention is simple, production is easy and safety non-toxic, has lightweight, that strong adhesion, snappiness are good feature.
Accompanying drawing explanation
Fig. 1 is the process flow sheet of texture multicolor finish of the present invention.
Embodiment
Below in conjunction with accompanying drawing embodiment, the present invention is described in further detail.
A kind of texture multicolor finish of the present invention by A, B two component be added with appropriate mill base hybrid modulation and form, wherein: the mass ratio of component A and B component is 1: 3 to 3: 1; Each raw material in component A by percentage to the quality, includes high molecular polymer 10% ~ 60%, powder 5% ~ 50%, Mierocrystalline cellulose 0.3% ~ 8%, sand powder 5% ~ 50%, gelifying agent 0.1% ~ 30%, tensio-active agent 0.1% ~ 10%, water 10% ~ 60%; Each raw material in B component by percentage to the quality, includes high molecular polymer 10% ~ 80%, dispersion agent 0.1% ~ 5%, thickening material 0.1% ~ 5%, film coalescence aid 1% ~ 15%, water 5% ~ 70%.
High molecular polymer in component A is one or more in pure acrylic acid polymkeric substance, organosilicon-modified acrylic polymkeric substance and styrenated acrylic's polymkeric substance; High molecular polymer in B component is one or more in organosilicon crylic acid latex and fluorine carbon emulsion.
Powder in component A is one or more in titanium dioxide, talcum powder, calcium carbonate, barium sulfate and kaolin.
Mierocrystalline cellulose in component A is one or more in Walocel MT 20.000PV, Natvosol and hydroxypropylcellulose.
Sand powder in component A is one or more in the color sand of 120 order to 180 object white marbles, the color sand of Snow Flower White and the color sand of careless white jade.
Gelifying agent in component A is one or more in neusilin, lithium magnesium silicate, organobentonite and agar powder.
Tensio-active agent in component A is one or more in polycarboxylate sodium, polyoxyethylene octylphenol ether, sodium alkyl benzene sulfonate and alkyl phenol ethoxylates.
Dispersion agent in B component is aqueous high molecular hyper-dispersant; Thickening material in described B component is one or more in the swelling associative thickener of hydrophobically-modified alkali and aqueous polyurethane associative thickener.
Film coalescence aid in B component is one or more in alcohol ester 12, Tri(propylene glycol)butyl ether,mixture of isomers, tert.-butyl acetate and ethylene glycol.
The preparation method of a kind of texture multicolor finish of the present invention, the method comprises component A preparation, B component preparation and finished product preparation successively.
Embodiment one,
1: prepare the raw material in component A and the raw material in B component by following formula; Wherein:
Component A formula (each raw material in formula by mass percentage)
Pure acrylic acid polymkeric substance 30%
Natvosol 0.5%
Titanium dioxide 5%
Calcium carbonate 10%
The color sand 20% of Snow Flower White
Organobentonite 5%
Lithium magnesium silicate 3%
Polycarboxylate sodium 0.3%
Water 26.2%
B component formula (each raw material in formula by mass percentage)
Organosilicon crylic acid latex 60%
Dispersion agent 0.5%
The swelling associative thickener 0.2% of alkali
Alcohol ester ten two 12%
Water 27.3%
2:A component prepare: the Scattered Kettle water of 26.2% first being poured into dispersion machine, in dispersing speed be add under the condition of 300r/min ~ 800r/min 0.5% Natvosol, dispersion 10min ~ 30min; Then in above-mentioned Scattered Kettle, the polycarboxylate sodium of 0.3% is added, dispersion 10min ~ 30min; In Scattered Kettle, add the titanium dioxide of 5% and the calcium carbonate of 10% again, adjustment dispersing speed is 800r/min ~ 1500r/min, dispersion 10min ~ 30min; The color sand of Snow Flower White of 20% is added again, dispersion 10min ~ 30min in Scattered Kettle; The pure acrylic acid polymkeric substance of 30% is added again in Scattered Kettle, dispersion 20min ~ 50min, in Scattered Kettle, finally add the lithium magnesium silicate of 3% and the organobentonite of 5%, adjustment dispersing speed is 1600r/min ~ 3200r/min, dispersion 10min ~ 20min, discharging obtains component A;
3, B component preparation: pouring in the Scattered Kettle of dispersion machine by the organosilicon crylic acid latex of 60% and the water of 27.3%, is disperse 10min ~ 30min under the condition of 300r/min ~ 1000r/min in dispersing speed; After add in Scattered Kettle the dispersion agent of 0.5%, the alcohol ester 12 of 12% and 0.2% the swelling associative thickener of alkali, dispersion 10min ~ 30min, discharging obtains B component;
4, finished product preparation: be ratio extraction component A and the B component of 1: 1 in mass ratio, the B component of extraction is put into Scattered Kettle, and the rotating speed of adjustment dispersion machine is 200r/min ~ 600r/min; By mill base by component A furnishing shades of colour, then the component A of furnishing shades of colour is joined in Scattered Kettle disperse granulation, can this product be obtained.
Embodiment two,
1: prepare the raw material in component A and the raw material in B component by following formula; Wherein:
Component A formula (each raw material in formula by mass percentage)
Pure acrylic acid polymkeric substance 15%
Organosilicon-modified acrylic polymkeric substance 15%
Natvosol 0.5%
Titanium dioxide 5%
Kaolin 10%
The color sand 20% of white marble
Neusilin 5%
Lithium magnesium silicate 3%
Polyoxyethylene octylphenol ether 0.3%
Water 26.2%
B component formula (each raw material in formula by mass percentage)
Organosilicon crylic acid latex 30%
Fluorine carbon emulsion 30%
Dispersion agent 0.5%
The swelling associative thickener 0.2% of alkali
Tri(propylene glycol)butyl ether,mixture of isomers 15%
Water 24.3%
2:A component prepare: the Scattered Kettle water of 26.2% first being poured into dispersion machine, in dispersing speed be add under the condition of 300r/min ~ 800r/min 0.5% Natvosol, dispersion 10min ~ 30min; Then in above-mentioned Scattered Kettle, the polyoxyethylene octylphenol ether of 0.3% is added, dispersion 10min ~ 30min; In Scattered Kettle, add the titanium dioxide of 5% and the kaolin of 10% again, adjustment dispersing speed is 800r/min ~ 1500r/min, dispersion 10min ~ 30min; The color sand of white marble of 20% is added again, dispersion 10min ~ 30min in Scattered Kettle; The pure acrylic acid polymkeric substance of 15% and the organosilicon-modified acrylic polymkeric substance of 15% is added again in Scattered Kettle, dispersion 20min ~ 50min, finally in Scattered Kettle, add the lithium magnesium silicate of 3% and the neusilin of 5%, adjustment dispersing speed is 1600r/min ~ 3200r/min, dispersion 10min ~ 20min, discharging obtains component A.
3, B component preparation: by the organosilicon crylic acid latex of 30%, the fluorine carbon emulsion of 30% and 24.3% water pour in the Scattered Kettle of dispersion machine, be disperse 10min ~ 30min under the condition of 300r/min ~ 1000r/min in dispersing speed; After add in Scattered Kettle the dispersion agent of 0.5%, the Tri(propylene glycol)butyl ether,mixture of isomers of 15% and 0.2% the swelling associative thickener of alkali, dispersion 10min ~ 30min, discharging obtains B component;
4, finished product preparation: be ratio extraction component A and the B component of 2: 3 in mass ratio, the B component of extraction is put into Scattered Kettle, and the rotating speed of adjustment dispersion machine is 200r/min ~ 600r/min; By mill base by component A furnishing shades of colour, then the component A of furnishing shades of colour is joined in Scattered Kettle disperse granulation, can this product be obtained.
Embodiment three,
1: prepare the raw material in component A and the raw material in B component by following formula; Wherein:
Component A formula (each raw material in formula by mass percentage)
Styrenated acrylic's polymkeric substance 10%
Organosilicon-modified acrylic polymkeric substance 15%
Natvosol 0.5%
Walocel MT 20.000PV 0.3%
Barium sulfate 5%
Talcum powder 5%
Kaolin 5%
The color sand 30% of white marble
Neusilin 5%
Lithium magnesium silicate 3%
Alkyl phenol ethoxylates 0.3%
Water 20.9%
B component formula (each raw material in formula by mass percentage)
Organosilicon crylic acid latex 10%
Fluorine carbon emulsion 60%
Dispersion agent 0.8%
Polyurethane associative thickener 0.5%
Ethylene glycol 10%
Alcohol ester ten two 7%
Water 11.7%
Following making method and embodiment one are identical with implementing two, and just the mass ratio of component A and B component is 1: 2.
Embodiment four,
Component A formula (each raw material in formula by mass percentage)
Organosilicon-modified acrylic polymkeric substance 35%
Natvosol 1%
Hydroxypropylcellulose 0.2%
Titanium dioxide 5%
Kaolin 10%
The color sand 25% of grass white jade
Agar powder 5%
Lithium magnesium silicate 3%
Sodium alkyl benzene sulfonate 1%
Water 14.8%
B component formula (each raw material in formula by mass percentage)
Fluorine carbon emulsion 60%
Dispersion agent 0.8%
Polyurethane associative thickener 0.2%
The swelling associative thickener 0.3% of alkali
Tert.-butyl acetate 8%
Water 30.7%
Following making method and embodiment one are identical with implementing two, and just the mass ratio of component A and B component is 2: 1.
Manufacturing process of the present invention is simple, with low cost, also can have the coarse texture of rock itself, have the high simulated effect of natural granite after spray mo(u)lding drying while presenting rock decorative pattern, and tint retention is good, not fugitive color, is the decorative paint of building trade.
Claims (1)
1. a preparation method for texture multicolor finish, is characterized in that: prepare the raw material in component A and the raw material in B component by following formula; Wherein: each raw material in component A formula by mass percentage
Pure acrylic acid polymkeric substance 15%
Organosilicon-modified acrylic polymkeric substance 15%
Natvosol 0.5%
Titanium dioxide 5%
Kaolin 10%
The color sand 20% of white marble
Neusilin 5%
Lithium magnesium silicate 3%
Polyoxyethylene octylphenol ether 0.3%
Water 26.2%
Each raw material in B component formula by mass percentage
Organosilicon crylic acid latex 30%
Fluorine carbon emulsion 30%
Dispersion agent 0.5%
The swelling associative thickener 0.2% of alkali
Tri(propylene glycol)butyl ether,mixture of isomers 15%
Water 24.3%
Component A prepare: the Scattered Kettle water of 26.2% first being poured into dispersion machine, in dispersing speed be add under the condition of 300r/min ~ 800r/min 0.5% Natvosol, dispersion 10min ~ 30min; Then in above-mentioned Scattered Kettle, the polyoxyethylene octylphenol ether of 0.3% is added, dispersion 10min ~ 30min; In Scattered Kettle, add the titanium dioxide of 5% and the kaolin of 10% again, adjustment dispersing speed is 800r/min ~ 1500r/min, dispersion 10min ~ 30min; The color sand of white marble of 20% is added again, dispersion 10min ~ 30min in Scattered Kettle; The pure acrylic acid polymkeric substance of 15% and the organosilicon-modified acrylic polymkeric substance of 15% is added again in Scattered Kettle, dispersion 20min ~ 50min, finally in Scattered Kettle, add the lithium magnesium silicate of 3% and the neusilin of 5%, adjustment dispersing speed is 1600r/min ~ 3200r/min, dispersion 10min ~ 20min, discharging obtains component A;
B component prepare: by the organosilicon crylic acid latex of 30%, the fluorine carbon emulsion of 30% and 24.3% water pour in the Scattered Kettle of dispersion machine, be disperse 10min ~ 30min under the condition of 300r/min ~ 1000r/min in dispersing speed; After add in Scattered Kettle the dispersion agent of 0.5%, the Tri(propylene glycol)butyl ether,mixture of isomers of 15% and 0.2% the swelling associative thickener of alkali, dispersion 10min ~ 30min, discharging obtains B component;
Prepared by finished product: be ratio extraction component A and the B component of 2: 3 in mass ratio, the B component of extraction is put into Scattered Kettle, and the rotating speed of adjustment dispersion machine is 200r/min ~ 600r/min; By mill base by component A furnishing shades of colour, then the component A of furnishing shades of colour is joined in Scattered Kettle disperse granulation, texture multicolor finish can be obtained.
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| CN106566346A (en) * | 2016-10-31 | 2017-04-19 | 四川泓川美居新材料科技有限公司 | Aqueous multi-color granite coating material |
| CN108912865A (en) * | 2017-04-05 | 2018-11-30 | 杨更生 | A kind of natural bottom surface integrated color coating of exterior wall |
| CN107236459A (en) * | 2017-06-05 | 2017-10-10 | 山东华德隆建材科技有限公司 | Colorful former stone stone-like coating |
| CN107177261B (en) * | 2017-06-23 | 2019-07-26 | 河北晨阳工贸集团有限公司 | High-performance sand textured coating and preparation method thereof |
| CN109233524A (en) * | 2018-10-18 | 2019-01-18 | 扬州中涂科技集团有限公司 | A kind of aqueous liquid two-component granite and marble paint |
| CN111607294A (en) * | 2019-02-23 | 2020-09-01 | 湖南梨树园涂料有限公司 | Sand-in-water multi-color paint toning bag and preparation method thereof |
| CN110698930A (en) * | 2019-10-30 | 2020-01-17 | 石家庄市油漆厂 | Long-acting high-weather-resistance self-cleaning water-based multicolor paint and preparation method thereof |
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| CN101492577A (en) * | 2008-01-23 | 2009-07-29 | 吴钢 | Process for producing watersoluble stone design imitating color slice and use scheme |
| CN101525506B (en) * | 2009-04-03 | 2012-07-04 | 富思特制漆（北京）有限公司 | Liquid granite paint and preparing method thereof |
| CN102079946B (en) * | 2010-12-20 | 2012-06-20 | 贺佑康 | Low-carbon water granite paint |
| DE102011014250A1 (en) * | 2011-03-17 | 2012-09-20 | Clariant International Ltd. | Powder coating composition for structuring and texturing of painted surfaces |
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Denomination of invention: A textured and colorful coating and its preparation method Granted publication date: 20160217 Pledgee: Zhejiang Tailong Commercial Bank Co.,Ltd. Ningbo Beilun sub branch Pledgor: NINGBO XIN'AN PAINT CO.,LTD. Registration number: Y2024330000507 |