CN104845477A - Luminous basic paint and preparing method thereof - Google Patents
Luminous basic paint and preparing method thereof Download PDFInfo
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- CN104845477A CN104845477A CN201510275717.1A CN201510275717A CN104845477A CN 104845477 A CN104845477 A CN 104845477A CN 201510275717 A CN201510275717 A CN 201510275717A CN 104845477 A CN104845477 A CN 104845477A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/08—Homopolymers or copolymers of acrylic acid esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/22—Luminous paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/29—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for multicolour effects
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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Abstract
The invention relates to a functional building paint technology, and aims at providing luminous basic paint and a preparing method of the luminous basic paint. The luminous basic paint is formed by mixing the following ingredients in parts by weight: 30 to 50 parts of synthetic resin emulsion, 15 to 30 parts of luminous powder, 15 to 30 parts of pigment fillers, 5 to 8 parts of auxiliaries and 20 to 40 parts of deionized water. The luminous powder is introduced, so that film forming matters of the luminous basic paint have the functions that the film forming matters are stable for a long time (more than six months) in water-based paint, and the luminous time is up to 12 hours. Meanwhile, the preparing method is simple and convenient, and the industrial production cost is favorably reduced. When the luminous basic paint provided by the invention is applied, water-based luminous multi-color paint with stable particle distribution can be obtained only through grinding, stirring and dispersing raw materials; the preparing process is simple, the implementation is easy, and the operation is simple and convenient; the industrial large-scale production is favorably realized; the industrial production cost is reduced; the luminous basic paint is particularly suitable for occasions such as residential buildings, commercial buildings and public buildings, and wide application prospects are realized.
Description
Technical field
The invention belongs to Functional Architectural Coatings in China technical field, particularly luminous base paint of one and preparation method thereof.
Background technology
Water-soluble colorful coating obtains significant progress in building decoration field, and ever-changing with its shape, imitative stone effect advantage true to nature, aqueous, environmental protective is very popular.And the water-soluble colorful coating of several functions also emerges gradually.Publication number is that the Chinese invention patent application of CN201410753296.4 discloses the clean taste multicolor finish of a kind of water-based, comprise the water of 10 ~ 15% weight parts, the AMP-95 of 0.1 ~ 0.2% weight part, the film coalescence aid of 1.0 ~ 1.5% weight parts, the soap-free polymerization elastic emulsion of 20 ~ 30% weight parts, the sanitas of 0.1 ~ 0.3% weight part, the color grain of 53 ~ 68% weight parts.Publication number is that the Chinese invention patent application of CN201410668695.0 discloses a kind of reflective insulation multicolor finish, carries out granulation, and add synthetic resin emulsion and obtain finished product by the base paint with reflective insulation function is placed in protecting glue.
But water-soluble colorful coating cannot embody ornamental at night, limit its application to a certain extent.Therefore, prepare a kind of luminous base paint being applied to multicolor finish and seem particularly necessary.
Summary of the invention
The technical problem to be solved in the present invention is, overcomes deficiency of the prior art, provides a kind of luminous base paint and preparation method thereof.
For technical solution problem, solution of the present invention is:
Thering is provided a kind of luminous base paint, is mixed by the raw material of following weight part:
Described synthetic resin emulsion is the one in pure-acrylic emulsion, benzene emulsion, vinyl acetate emulsion, organosilicon crylic acid latex, polyaminoester emulsion, epoxy resin latex;
Described luminescent powder is commercially available long afterglow luminescent powder;
Described color stuffing is one or more in titanium dioxide, zinc sulfide white, kaolin, diatomite, calcium carbonate, pure aluminium silicate, mica, talcum powder;
Described auxiliary agent is one or more in film coalescence aid, dispersion agent, wetting agent, defoamer, thickening material, antiseptic-germicide, frostproofer, pH adjusting agent.
Present invention also offers the method preparing aforementioned luminous base paint, comprise the following steps:
(1) stirring at low speed:
Deionized water, part of auxiliary are added in high speed dispersor, under the speed of 200 ~ 1000r/min, stir 5 ~ 10min;
This part of auxiliary refer in film coalescence aid, dispersion agent, wetting agent, defoamer, thickening material, antiseptic-germicide, frostproofer, pH adjusting agent one or more;
(2) high speed dispersion:
Luminescent powder, color stuffing are continued to be added in aforementioned high speed dispersor, under the speed of 1000 ~ 3000r/min, stirs 10 ~ 30min, obtain slurry;
(3) stirring at low speed dispersion:
Synthetic resin emulsion and remaining auxiliary agent are added in afore-mentioned slurry, dispersed with stirring 5 ~ 15min under the speed of 500 ~ 2000r/min, through 80 ~ 100 object screen filtrations, obtain luminous base paint.
Invention further provides preferred luminous base paint, is mixed by the raw material of following weight part:
In the present invention, the method preparing aforementioned preferred luminous base paint comprises the following steps:
(1) stirring at low speed:
By deionized water, propylene glycol, 2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrate, isothiazolones, polycarboxylate sodium's type dispersion agent, Natvosol type thickening material and 2-amino-2-methyl-1-propanol are added in high speed dispersor, under the speed of 200 ~ 1000r/min, stir 5 ~ 10min.
(2) high speed dispersion:
Titanium dioxide, kaolin, calcium carbonate, luminescent powder are added in high speed dispersor, under the speed of 1000 ~ 3000r/min, grinds 10 ~ 30min, obtain slurry.
(3) paint:
Synthetic resin emulsion and mineral oil antifoam agent are added in this slurry, dispersed with stirring 5 ~ 15min under the speed of 500 ~ 2000r/min, through 80 ~ 100 object screen filtrations, obtain luminous base paint.
In the present invention:
Described lithium magnesium silicate, its function forms physical gel by charge effect around luminous base paint, stops the infiltration of base paint, avoids producing grow diming phenomenon.
Described synthetic resin emulsion emulsion, it is mainly as the base material of coating, has vital role to the weathering resistance, mechanical property etc. of coating.As preferably, described filming emulsion is the one in pure-acrylic emulsion, benzene emulsion, vinyl acetate emulsion, organosilicon crylic acid latex, polyaminoester emulsion, epoxy resin latex, and affiliated emulsion all can adopt commercially available prod.
Described luminescent powder to have in water-borne coatings stable (more than 6 months) for a long time, fluorescent lifetime reaches the function of 12 hours.Luminescent powder of the present invention is commercially available long afterglow luminescent powder.
In described auxiliary agent, film coalescence aid specifically can select 2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrate, dispersion agent specifically can select polycarboxylate sodium's type dispersion agent, wetting agent can specifically select propylene glycol or glycerine, defoamer specifically can select methyl-silicone oil, thickening material specifically can select Natvosol type thickening material, antiseptic-germicide specifically can select isothiazolones (as BIT), and frostproofer specifically can select propylene glycol, and pH adjusting agent specifically can select 2-amino-2-methyl-1-propanol.
Compared with prior art, tool of the present invention has the following advantages:
The present invention, by introducing luminescent powder, such that the film forming matter of luminous base paint to have in water-borne coatings stable (more than 6 months) for a long time, fluorescent lifetime reaches the function of 12 hours.Meanwhile, preparation method of the present invention is simple, convenient, is conducive to reducing industrial production cost.
When applying product of the present invention, the water-based luminous multi-color paint of particle stabilized distribution only need be ground and can obtain after dispersed with stirring to raw material, its preparation technology is simple, easy to implement, easy and simple to handle, be conducive to industrialization scale operation, reduce industrial production cost, be specially adapted to the occasions such as civil construction, commercial building, public building, have broad application prospects.
Embodiment
Below in conjunction with case study on implementation, the present invention is further described." part " in the following example all refers to weight part.
Embodiment 1-1
In high speed dispersor, add deionized water 95 parts, under the speed of 2000r/min, add lithium magnesium silicate 5 parts, continue dispersion 45min, obtain protecting glue solution.
Embodiment 1-2
In high speed dispersor, add deionized water 90 parts, under the speed of 2000r/min, add lithium magnesium silicate 10 parts, continue dispersion 45min, obtain protecting glue solution.
Embodiment 1-3
In high speed dispersor, add deionized water 93 parts, under the speed of 2000r/min, add lithium magnesium silicate 7 parts, continue dispersion 45min, obtain protecting glue solution.
Embodiment 2
Synthetic resin emulsion 95.5 parts (the rich 998A of Ahmedabad) is added in high speed dispersor, 2 are added under the speed of 300r/min, 2,4-trimethylammonium-1,3-pentanediol mono isobutyrate 4 parts, the swelling acrylic thickener of alkali 0.5 part (Tao Shi TT-935), continues dispersion 30min, obtains physically modified synthetic resin emulsion.
Embodiment 3
Deionized water 20 parts, propylene glycol 2.5 parts, 2 is added in high speed dispersor, 2,4-trimethylammonium-1,3-pentanediol mono isobutyrate 0.8 part, BIT 0.5 part, polycarboxylate sodium's type dispersion agent 0.1 part (Nuo Pu section SN-5040), Natvosol type thickening material 2 parts (Tao Shi Cellusize ER-30M) and 2-amino-2-methyl-1-propanol 1 part, disperse 10min under the speed of 200r/min; Add Rutile type Titanium Dioxide 15 parts, kaolin 5 parts, 5 parts, calcium carbonate, luminescent powder 15 parts (the bright PLO-8C in road) again, under the speed of 2000r/min, disperse 20min to obtain slurry; Under the speed of 600r/min, by pure-acrylic emulsion 30 parts, (ROHM AND HAAS is easily tough to be reached
tM2468) and mineral oil antifoam agent 0.1 part add in this slurry, dispersed with stirring 10min, through 80 object screen filtrations, obtains luminous base paint.
To sum up, the luminous base paint product of the present embodiment is prepared by the raw material of following weight part:
Embodiment 4
Deionized water 30 parts, propylene glycol 0.5 part, 2 is added in high speed dispersor machine, 2,4-trimethylammonium-1,3-pentanediol mono isobutyrate 5 parts, BIT 0.1 part, polycarboxylate sodium's type dispersion agent 0.5 part (Nuo Pu section SN-5040), Natvosol type thickening material 1.3 parts (Tao Shi Cellusize ER-30M) and 2-amino-2-methyl-1-propanol 0.1 part, disperse 7min under the speed of 600r/min; Add Rutile type Titanium Dioxide 10 parts, kaolin 10 parts, 10 parts, calcium carbonate, luminescent powder 30 parts (the bright PLO-8C in road) again, under the speed of 3000r/min, disperse 10min to obtain slurry; Under the speed of 2000r/min, benzene emulsion 50 parts and mineral oil antifoam agent 0.5 part are added in this slurry, dispersed with stirring 5min, through 90 object screen filtrations, obtain luminous base paint.
Embodiment 5
Deionized water 40 parts, propylene glycol 0.7 part, 2 is added in high speed dispersor machine, 2,4-trimethylammonium-1,3-pentanediol mono isobutyrate 0.5 part, BIT 0.2 part, polycarboxylate sodium's type dispersion agent 1 part (Nuo Pu section SN-5040), Natvosol type thickening material 1 part (Tao Shi Cellusize ER-30M) and 2-amino-2-methyl-1-propanol 0.6 part, disperse 5min under the speed of 1000r/min; Add Rutile type Titanium Dioxide 5 parts, 10 parts, calcium carbonate, luminescent powder 20 parts (the bright PLO-8C in road) again, under the speed of 1000r/min, disperse 30min to obtain slurry; Under the speed of 500r/min, vinyl acetate emulsion 40 parts and mineral oil antifoam agent 1 part are added in this slurry, dispersed with stirring 15min, through 100 object screen filtrations, obtain luminous base paint.
Embodiment 5-2 (comparative example)
Deionized water 40 parts, propylene glycol 0.7 part, 2 is added in high speed dispersor machine, 2,4-trimethylammonium-1,3-pentanediol mono isobutyrate 0.5 part, BIT 0.2 part, polycarboxylate sodium's type dispersion agent 1 part (Nuo Pu section SN-5040), Natvosol type thickening material 1 part (Tao Shi Cellusize ER-30M) and 2-amino-2-methyl-1-propanol 0.6 part, disperse 5min under the speed of 1000r/min; Add Rutile type Titanium Dioxide 5 parts, 8 parts, calcium carbonate, (the bright PLO-8C in road) again, under the speed of 1000r/min, disperse 30min to obtain slurry; Under the speed of 500r/min, vinyl acetate emulsion 40 parts and mineral oil antifoam agent 1 part are added in this slurry, dispersed with stirring 15min, through 100 object screen filtrations, obtain conventional foundation paint.
Embodiment 6
The luminous base paint 30 parts obtained in embodiment 3 is joined in the 50 parts of protecting glue solution obtained in embodiment 1-1; stir and obtain the suspension that particulate state distributes, particle diameter is different; add the 15 serving reason modified synthetic resin emulsions obtained in embodiment 2 again, obtain the water-based luminous multi-color paint of particle stabilized distribution.
Protecting glue solution 50 parts;
Luminous base paint 30 parts;
Physically modified synthetic resin emulsion 15 parts;
Embodiment 7
The luminous base paint 15 parts obtained in embodiment 4 is joined in the 30 parts of protecting glue solution obtained in embodiment 1-2; stir and obtain the suspension that particulate state distributes, particle diameter is different; add the 30 serving reason modified synthetic resin emulsions obtained in embodiment 2 again, obtain the water-based luminous multi-color paint of particle stabilized distribution.
Protecting glue solution 30 parts;
Luminous base paint 15 parts;
Physically modified synthetic resin emulsion 30 parts;
Embodiment 8-1
The luminous base paint 20 parts obtained in embodiment 5 is joined in the 40 parts of protecting glue solution obtained in embodiment 1-3; stir and obtain the suspension that particulate state distributes, particle diameter is different; add the 25 serving reason modified synthetic resin emulsions obtained in embodiment 2 again, obtain the water-based luminous multi-color paint of particle stabilized distribution.
Protecting glue solution 40 parts;
Luminous base paint 20 parts;
Physically modified synthetic resin emulsion 25 parts;
Embodiment 8-2 (comparative example)
20 parts, the conventional foundation paint obtained in embodiment 5-2 is joined in the 40 parts of protecting glue solution obtained in embodiment 1-3; stir and obtain the suspension that particulate state distributes, particle diameter is different; add the 25 serving reason modified synthetic resin emulsions obtained in embodiment 2 again, obtain the common water borne multicolor finish of particle stabilized distribution.
Protecting glue solution 40 parts;
20 parts, conventional foundation paint;
Physically modified synthetic resin emulsion 25 parts;
By embodiment 6,7, the coating that obtains of 8-2 carries out actual application, its luminous detection result is as shown in table 1.
The luminous characteristics of table 1 water-based luminous multi-color paint
| Embodiment 6 | Embodiment 7 | Embodiment 8-2 | |
| Luminous characteristics | 12 hours | 12 hours | Not luminous |
From table 1, the water-based luminous multi-color paint product improved by introducing luminescent powder in base paint has the feature of long-term luminous at night, is applicable to the occasions such as civil construction, commercial building, public building.
Claims (4)
1. a luminous base paint, is characterized in that, is to be mixed by the raw material of following weight part:
Described synthetic resin emulsion is the one in pure-acrylic emulsion, benzene emulsion, vinyl acetate emulsion, organosilicon crylic acid latex, polyaminoester emulsion, epoxy resin latex;
Described luminescent powder is commercially available long afterglow luminescent powder;
Described color stuffing is one or more in titanium dioxide, zinc sulfide white, kaolin, diatomite, calcium carbonate, pure aluminium silicate, mica, talcum powder;
Described auxiliary agent is one or more in film coalescence aid, dispersion agent, wetting agent, defoamer, thickening material, antiseptic-germicide, frostproofer, pH adjusting agent.
2. prepare a method for luminous base paint described in claim 1, it is characterized in that, comprise the following steps:
(1) stirring at low speed:
Deionized water, part of auxiliary are added in high speed dispersor, under the speed of 200 ~ 1000r/min, stir 5 ~ 10min;
This part of auxiliary refer in film coalescence aid, dispersion agent, wetting agent, defoamer, thickening material, antiseptic-germicide, frostproofer, pH adjusting agent one or more;
(2) high speed dispersion:
Luminescent powder, color stuffing are continued to be added in aforementioned high speed dispersor, under the speed of 1000 ~ 3000r/min, stirs 10 ~ 30min, obtain slurry;
(3) stirring at low speed dispersion:
Synthetic resin emulsion and remaining auxiliary agent are added in afore-mentioned slurry, dispersed with stirring 5 ~ 15min under the speed of 500 ~ 2000r/min, through 80 ~ 100 object screen filtrations, obtain luminous base paint.
3. a luminous base paint, is characterized in that, is to be mixed by the raw material of following weight part:
4. prepare a method for luminous base paint described in claim 3, it is characterized in that, comprise the following steps:
(1) stirring at low speed:
By deionized water, propylene glycol, 2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrate, isothiazolones, polycarboxylate sodium's type dispersion agent, Natvosol type thickening material and 2-amino-2-methyl-1-propanol are added in high speed dispersor, under the speed of 200 ~ 1000r/min, stir 5 ~ 10min;
(2) high speed dispersion:
Titanium dioxide, kaolin, calcium carbonate, luminescent powder are added in high speed dispersor, under the speed of 1000 ~ 3000r/min, grinds 10 ~ 30min, obtain slurry;
(3) paint:
Synthetic resin emulsion and mineral oil antifoam agent are added in this slurry, dispersed with stirring 5 ~ 15min under the speed of 500 ~ 2000r/min, through 80 ~ 100 object screen filtrations, obtain luminous base paint.
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| CN201510275717.1A CN104845477A (en) | 2015-05-27 | 2015-05-27 | Luminous basic paint and preparing method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105331171A (en) * | 2015-12-08 | 2016-02-17 | 安徽中益新材料科技有限公司 | Retro-reflection energy-storing luminous paint and preparing method thereof |
| CN106675318A (en) * | 2016-10-31 | 2017-05-17 | 蔡洪祥 | Luminescent paint and manufacturing method thereof |
| RU2662530C1 (en) * | 2017-07-03 | 2018-07-26 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Казанский государственный архитектурно-строительный университет" КГАСУ | Water-dispersed protective paint and varnish composition |
| CN108753148A (en) * | 2018-05-25 | 2018-11-06 | 安徽猛牛彩印包装有限公司 | A kind of preparation method of epoxy resin luminous paint |
| CN109836876A (en) * | 2019-03-06 | 2019-06-04 | 长安大学 | A kind of road aqueous double-deck modified luminous paint of silicon fiml grafting and its preparation method and application |
| CN111944401A (en) * | 2020-07-15 | 2020-11-17 | 杭州蓝田涂料有限公司 | Waterborne polyurethane noctilucent crack paint and preparation method thereof |
| CN116102935A (en) * | 2023-02-22 | 2023-05-12 | 贵州大学 | Preparation method of water-based luminescent coating with efficient mixed structure |
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