CN101343436A - Novel water-covering water gorgeous paint and preparation thereof - Google Patents
Novel water-covering water gorgeous paint and preparation thereof Download PDFInfo
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- CN101343436A CN101343436A CNA2008101389399A CN200810138939A CN101343436A CN 101343436 A CN101343436 A CN 101343436A CN A2008101389399 A CNA2008101389399 A CN A2008101389399A CN 200810138939 A CN200810138939 A CN 200810138939A CN 101343436 A CN101343436 A CN 101343436A
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Abstract
The invention provides novel water in water multicolor paint and the preparation method, which belongs to the technical field of paint preparation. Dispersant, pigment, calcium carbonate, film forming additive, antifoaming agent, thickening agent, ammonia water and anti-corrosion agent are added into the dispersing pot, after being uniformly mixed and grinded, synthetic resin emulsion and antifoaming agent are added and mixed, then thickening agent is added, thus water dispersing phase is manufactured; water, dispersant, antifoaming agent, cellulose and anti-corrosion agent are added in a container, after being mixed uniformly, water soluble resin is added and mixed, thus protective glue is manufactured; organobentonite is added in warm water and mixed to colloid, aluminum sulfate and magnesium chloride is added and mixed, thus water dispersing medium is manufactured; the water dispersing medium is added into a blender, and the water dispersing phase and the protective glue are being added while being mixed, after being cut and stirred by a screen, the water in water multicolor paint with various colors mixed and surface of dispersed particle colloidized is obtained, the paint dispersing medium and the dispersing medium is apparently separated, the gloss is high, and the decorative effect and the stability are good.
Description
Technical field
The present invention relates to the preparing technical field of coating, specifically a kind of novel water-covering water gorgeous paint and preparation method thereof.
Background technology
Along with growth in the living standard, people not only have been confined to the scope of solving the basic living problems to the pursuit of life, but risen to pursuit to spirit and goods and materials aspect, simultaneously, aspect the household or the finishing of office office building, people begin to embody style simple, individual character gradually on the finishing of interior exterior wall, and the construction of gorgeous color coating material is fairly simple, in the personalization of product and variation, can satisfy the demands of consumers, therefore also attract people's attention gradually.In the prior art, gorgeous color coating material has begun the exploitation manufacturing and has used, but contain organic solvents such as toluene, dimethylbenzene because of it, in production, construction process, all can discharge a large amount of poisonous organic solvents, environment and HUMAN HEALTH have all been constituted great threat.
Along with people improve the cognition degree of environmental protection, the use of solvent in coating reduced day by day, development is the developing direction of low pollutionizations of coating with water as the water-borne coatings of medium replace organic solvent, the raising of the application percentage that gorgeous color coating material of while is fitted up in interior exterior wall.Shortcomings such as it is bad that but the gorgeous color coating material of the water-in-water type of Xiao Shouing ubiquity stability in the market, and two-phase is miscible easily.
Summary of the invention
Technical assignment of the present invention is to solve the deficiencies in the prior art, provides to have significantly between a kind of disperse phase and the dispersion medium to separate gloss height, good decorating effect, novel water-covering water gorgeous paint of good stability and preparation method thereof.
Technical scheme of the present invention realizes in the following manner, a kind of novel water-covering water gorgeous paint, and the component of this water-covering water gorgeous paint comprises water-dispersion phase, protection glue, water dispersion medium, its each component prescription and weight proportion are:
(1) water-dispersion phase
Synthetic resin emulsion: 20-60 part defoamer: 0-1 part
Film coalescence aid: 0.1-4 part thickening material: 0-1 part
Pigment: 1-15 part ammoniacal liquor: 0-50 part
Lime carbonate: 1-15 part sanitas: 0-0.5 part
Dispersion agent: 0.1-2 part water: 20-60 part;
(2) protection glue
Water soluble resin: 40-100 part Mierocrystalline cellulose: 0.1-2 part
Dispersion agent: 0.2-3 part sanitas: 0-0.5 part
Defoamer: 0-2 part water: 10-50 part;
(3) water dispersion medium
Water: 60-120 part Tai-Ace S 150: 1-15 part
Organobentonite: 0.1-10 part magnesium chloride: 0.1-10 part;
(4) the gorgeous color coating material of water-in-water type
Water-dispersion phase: 10-50 part protection glue: 10-50 part
Water dispersion medium: 20-100 part.
The component of described a kind of novel water-covering water gorgeous paint comprises water-dispersion phase, protection glue, water dispersion medium, and its each component prescription and preferred weight proportioning are:
(1) water-dispersion phase
Synthetic resin emulsion: 40-45 part defoamer: 0.1-0.5 part
Film coalescence aid: 0.5-3 part thickening material: 0.1-0.5 part
Pigment: 2-10 part ammoniacal liquor: 0-50 part
Lime carbonate: 2-10 part sanitas: 0.2-0.5 part
Dispersion agent: 0.2-1 part water: 30-50 part;
(2) protection glue
Water soluble resin: 50-90 part Mierocrystalline cellulose: 0.2-1.5 part
Dispersion agent: 0.5-2.5 part sanitas: 0.05-0.4 part
Defoamer: 0.2-1.5 part water: 15-45 part
(3) water dispersion medium
Water: 80-100 part Tai-Ace S 150: 2-10 part
Organobentonite: 0.2-5 part magnesium chloride: 0.2-5 part
(4) the gorgeous color coating material of water-in-water type
Water-dispersion phase: 15-45 part protection glue: 10-40 part
Water dispersion medium: 20-80 part.
The component of described a kind of novel water-covering water gorgeous paint comprises water-dispersion phase, protection glue, water dispersion medium, and its each component prescription and optimum weight proportioning are:
(1) water-dispersion phase
Synthetic resin emulsion: 40-45 part defoamer: 0.25-0.35 part
Film coalescence aid: 1-2 part thickening material: 0.1-0.2 part
Pigment: 4-6 part ammoniacal liquor: 0-50 part
Lime carbonate: 4-6 part sanitas: 0.2-0.3 part
Dispersion agent: 0.4-0.6 part water: 35-45 part;
(2) protection glue
Water soluble resin: 65-75 part Mierocrystalline cellulose: 0.5-1 part
Dispersion agent: 1-1.5 part sanitas: 0.1-0.2 part
Defoamer: 0.5-1 part water: 25-35 part;
(3) water dispersion medium
Water: 90-95 part Tai-Ace S 150: 3-6 part
Organobentonite: 0.5-2 part magnesium chloride: 0.5-2 part;
(4) the gorgeous color coating material of water-in-water type
Water-dispersion phase: 25-35 part protection glue: 20-25 part
Water dispersion medium: 40-60 part.
Described synthetic resin emulsion comprises one or more mixtures in pure-acrylic emulsion, acrylate and vinyl acetate emulsion, the benzene emulsion, the GK-503 that also can adopt Qingzhou shellfish specialization worker company limited to produce;
Described film coalescence aid comprises one or more mixtures in alcohol ester 12, dibutyl phthalate, dioctyl phthalate (DOP), the butyl glycol ether;
Described dispersion agent is polyacrylic acid sodium salt or ammonium salt comprise shellfish specialization worker company limited WP-19, the WP-5040 that produces, one or more mixtures among the WP-5060;
Described thickening material is an alkali swelling type thickening material, comprises ATW-01, the ATW-06 of shellfish specialization worker company limited production, one or more mixtures among ATW-60, the ATW-2000;
Described water soluble resin comprises one or more mixtures in polyacrylic resin, the urethane resin; Also can adopt GK-504, GK-507 that Bei Te company produces, among the GK-102 one or both;
Described defoamer comprises W-090, the W-092 that the modest company of moral produces, one or more mixtures among the H-436 of Haichuan Company, the Defoamer 121;
Described pigment is one or more mixtures in the pigment of white, red, green, black, yellow five kinds of colors.What wherein white pigment adopted is titanium dioxide.
The preparation method of described a kind of novel water-covering water gorgeous paint comprises the preparation of water-dispersion phase, preparation, the preparation of water dispersion medium and the preparation of the gorgeous color coating material of water-in-water type of protection glue, the method for each component preparation specifically:
The preparation of (1) water-dispersion phase
In dispersion tank, add dispersion agent, pigment, lime carbonate, film coalescence aid, defoamer, thickening material, ammoniacal liquor, sanitas, mix, grind the back and add synthetic resin emulsion, defoamer, stir, add an amount of thickening material, promptly make the water-dispersion phase;
(2) preparation of protection glue
In container, add entry, dispersion agent, defoamer, Mierocrystalline cellulose, sanitas, after stirring, add water soluble resin, stir, promptly make the protection sol solution;
(3) preparation of water dispersion medium
In warm water, add organobentonite and be stirred to glue, add Tai-Ace S 150, magnesium chloride then, stir, promptly make water dispersion medium;
(4) preparation of the gorgeous color coating material of water-in-water type
Described water dispersion medium is added in the mixing tank, add water-dispersion phase and protection glue while stirring,, slowly stir, obtain the gorgeous color coating material of water-in-water type of the surperficial gel of shades of colour blended dispersed particle with the screen cloth cutting.
The beneficial effect that a kind of novel water-covering water gorgeous paint of the present invention and preparation method thereof is compared with prior art produced is:
This a kind of novel water-covering water gorgeous paint and preparation method thereof, wherein in the process of preparation disperse phase, adding the surface-treated lime carbonate of a kind of process, is surface treated lime carbonate with this lime carbonate, and the dispersion of preparation is on good terms to have significantly with water and is separated; By adding protection glue component, protection glue is wrapped up disperse phase, make the gorgeous color coating material good stability of making, have significantly between disperse phase and the dispersion medium and separate, make the gorgeous color coating material two-phase good separating effect, gloss height, the good decorating effect that make.
This novel water-covering water gorgeous paint is with the water-borne coatings of water as the medium replace organic solvent, water Bao Shui is to be disperse phase with various emulsion paints, with water is external phase, so it is nontoxic, tasteless, pollution-free, and have performances such as good water tolerance, abrasion resistance and fire prevention, be current ideal finishing material therefore.
This novel water-covering water gorgeous paint is by two not miscible phase composites, and wherein one is external phase (dispersion medium) mutually, and another is disperse phase mutually.By once spraying, just can obtain luxurious, colorful pattern.Characteristics such as it is convenient that therefore gorgeous color coating material has application, and bright in luster, graceful, good decorating effect have stronger stereoscopic sensation, and touch-up paint is easy.
The present invention adopts special source materials; and by adding gorgeous color coating material two-phase good separating effect, gloss height, the good gorgeous color coating material of decorative effect that protection glue component makes; overcome sell on the market the gorgeous color coating material of water-in-water type ubiquity shortcomings such as stability bad, and two-phase is easily miscible.
Embodiment
Below described embodiment explain below coming a kind of novel water-covering water gorgeous paint of the present invention and preparation method thereof done.
A kind of novel water-covering water gorgeous paint of the present invention and preparation method thereof comprises the preparation of water-dispersion phase, preparation, the preparation of water dispersion medium and the preparation of the gorgeous color coating material of water-in-water type of protection glue, and the prescription of its each component and the preparation method of each component are:
1. the preparation of water-dispersion phase
Method: add dispersion agent, titanium dioxide or other coloured pigment, lime carbonate, film coalescence aid, defoamer, thickening material, ammoniacal liquor, sanitas successively by last table formula ratio, in dispersion tank, mix, and be ground to suitable fineness by sand mill, at room temperature add synthetic resin emulsion, defoamer, stir 40-60min, and be adjusted to suitable viscosity with thickening material, promptly make the water-dispersion phase.
2. the preparation of protection glue
Method: join by last table and high-volume to add entry, dispersion agent, defoamer, Mierocrystalline cellulose, sanitas successively, treat that Mierocrystalline cellulose dissolves fully, after stirring, add water soluble resin, stir, promptly make the protection sol solution.
3. the preparation of water dispersion medium
Method: in 20-50 ℃ water, add organobentonite and be stirred to glue (dispersed with stirring 15min at least), add Tai-Ace S 150, magnesium chloride after dissolving then, stir, promptly make water dispersion medium.
4. the preparation of the gorgeous color coating material of water-in-water type
Method: above-mentioned water dispersion medium is added in the mixing tank; add water-dispersion phase and protection glue while stirring, the screen cloth cutting with not of uniform size cuts into required shape, size; slowly stir then, obtain the gorgeous color coating material of water-in-water type of shades of colour blended dispersed particle surface gel.
The gorgeous color coating material that adopts above-mentioned examples preparation to come out meets GB/T 9755-2001, the standard of exterior wall coating material of synthetic resin emulsion.
Claims (6)
1, a kind of novel water-covering water gorgeous paint is characterized in that the component of this water-covering water gorgeous paint comprises water-dispersion phase, protection glue, water dispersion medium, and its each component prescription and weight proportion are:
(1) water-dispersion phase
Synthetic resin emulsion: 20-60 part defoamer: 0-1 part
Film coalescence aid: 0.1-4 part thickening material: 0-1 part
Pigment: 1-15 part ammoniacal liquor: 0-50 part
Lime carbonate: 1-15 part sanitas: 0-0.5 part
Dispersion agent: 0.1-2 part water: 20-60 part;
(2) protection glue
Water soluble resin: 40-100 part Mierocrystalline cellulose: 0.1-2 part
Dispersion agent: 0.2-3 part sanitas: 0-0.5 part
Defoamer: 0-2 part water: 10-50 part;
(3) water dispersion medium
Water: 60-120 part Tai-Ace S 150: 1-15 part
Organobentonite: 0.1-10 part magnesium chloride: 0.1-10 part;
(4) the gorgeous color coating material of water-in-water type
Water-dispersion phase: 10-50 part protection glue: 10-50 part
Water dispersion medium: 20-100 part.
2, a kind of novel water-covering water gorgeous paint according to claim 1 is characterized in that the component of this water-covering water gorgeous paint comprises water-dispersion phase, protection glue, water dispersion medium, and its each component prescription and weight proportion are:
(1) water-dispersion phase
Synthetic resin emulsion: 40-45 part defoamer: 0.1-0.5 part
Film coalescence aid: 0.5-3 part thickening material: 0.1-0.5 part
Pigment: 2-10 part ammoniacal liquor: 0-50 part
Lime carbonate: 2-10 part sanitas: 0.2-0.5 part
Dispersion agent: 0.2-1 part water: 30-50 part;
(2) protection glue
Water soluble resin: 50-90 part Mierocrystalline cellulose: 0.2-1.5 part
Dispersion agent: 0.5-2.5 part sanitas: 0.05-0.4 part
Defoamer: 0.2-1.5 part water: 15-45 part
(3) water dispersion medium
Water: 80-100 part Tai-Ace S 150: 2-10 part
Organobentonite: 0.2-5 part magnesium chloride: 0.2-5 part
(4) the gorgeous color coating material of water-in-water type
Water-dispersion phase: 15-45 part protection glue: 10-40 part
Water dispersion medium: 20-80 part.
3, a kind of novel water-covering water gorgeous paint according to claim 1 is characterized in that the component of this water-covering water gorgeous paint comprises water-dispersion phase, protection glue, water dispersion medium, and its each component prescription and weight proportion are:
(1) water-dispersion phase
Synthetic resin emulsion: 40-45 part defoamer: 0.25-0.35 part
Film coalescence aid: 1-2 part thickening material: 0.1-0.2 part
Pigment: 4-6 part ammoniacal liquor: 0-50 part
Lime carbonate: 4-6 part sanitas: 0.2-0.3 part
Dispersion agent: 0.4-0.6 part water: 35-45 part;
(2) protection glue
Water soluble resin: 65-75 part Mierocrystalline cellulose: 0.5-1 part
Dispersion agent: 1-1.5 part sanitas: 0.1-0.2 part
Defoamer: 0.5-1 part water: 25-35 part;
(3) water dispersion medium
Water: 90-95 part Tai-Ace S 150: 3-6 part
Organobentonite: 0.5-2 part magnesium chloride: 0.5-2 part;
(4) the gorgeous color coating material of water-in-water type
Water-dispersion phase: 25-35 part protection glue: 20-25 part
Water dispersion medium: 40-60 part.
4, according to claim 1,2,3 described a kind of novel water-covering water gorgeous paints, it is characterized in that:
Described synthetic resin emulsion comprises one or more mixtures in pure-acrylic emulsion, acrylate and vinyl acetate emulsion, the benzene emulsion;
Described film coalescence aid comprises one or more mixtures in alcohol ester 12, dibutyl phthalate, dioctyl phthalate (DOP), the butyl glycol ether;
Described dispersion agent is polyacrylic acid sodium salt or ammonium polyacrylate salt;
Described water soluble resin comprises one or more mixtures in polyacrylic resin, the urethane resin;
Described pigment is one or more mixtures in the pigment of white, red, green, black, yellow five kinds of colors.
5, a kind of method for preparing the described novel water-covering water gorgeous paint of claim 1; it is characterized in that comprising the preparation of water-dispersion phase, preparation, the preparation of water dispersion medium and the preparation of the gorgeous color coating material of water-in-water type of protection glue, the method for each component preparation specifically:
The preparation of (1) water-dispersion phase
In dispersion tank, add dispersion agent, pigment, lime carbonate, film coalescence aid, defoamer, thickening material, ammoniacal liquor, sanitas, mix, grind the back and add synthetic resin emulsion, defoamer, stir, add an amount of thickening material, promptly make the water-dispersion phase;
(2) preparation of protection glue
In container, add entry, dispersion agent, defoamer, Mierocrystalline cellulose, sanitas, after stirring, add water soluble resin, stir, promptly make the protection sol solution;
(3) preparation of water dispersion medium
In warm water, add organobentonite and be stirred to glue, add Tai-Ace S 150, magnesium chloride then, stir, promptly make water dispersion medium;
(4) preparation of the gorgeous color coating material of water-in-water type
Above-mentioned water dispersion medium is added in the mixing tank, add water-dispersion phase and protection glue while stirring,, slowly stir, obtain the gorgeous color coating material of water-in-water type of the surperficial gel of shades of colour blended dispersed particle with the screen cloth cutting.
6, the preparation method of a kind of novel water-covering water gorgeous paint according to claim 5 is characterized in that:
The preparation of (1) water-dispersion phase
In dispersion tank, add dispersion agent, pigment, lime carbonate, film coalescence aid, defoamer, thickening material, ammoniacal liquor, sanitas successively, mix, and be ground to suitable fineness by sand mill, at room temperature add synthetic resin emulsion, defoamer, stir 40-60min, and be adjusted to suitable viscosity with thickening material, promptly make the water-dispersion phase;
(2) preparation of protection glue
In container, add entry, dispersion agent, defoamer, Mierocrystalline cellulose, sanitas successively, treat that Mierocrystalline cellulose dissolves fully, after stirring, add water soluble resin, stir, promptly make the protection sol solution;
(3) preparation of water dispersion medium
In 20-50 ℃ water, add the organobentonite dispersed with stirring and be no less than 15min, add Tai-Ace S 150, magnesium chloride after dissolving then, stir, promptly make water dispersion medium to gluey;
(4) preparation of the gorgeous color coating material of water-in-water type
Described water dispersion medium is added in the mixing tank, add water-dispersion phase and protection glue while stirring,, slowly stir then, obtain the gorgeous color coating material of water-in-water type of the surperficial gel of shades of colour blended dispersed particle with the screen cloth cutting of sieve aperture not of uniform size.
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| CNA2008101389399A CN101343436A (en) | 2008-08-06 | 2008-08-06 | Novel water-covering water gorgeous paint and preparation thereof |
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| CNA2008101389399A CN101343436A (en) | 2008-08-06 | 2008-08-06 | Novel water-covering water gorgeous paint and preparation thereof |
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| CN102167944A (en) * | 2011-05-31 | 2011-08-31 | 苏州市金近涂料有限公司 | Water-based dipping lacquer and preparation method thereof |
| CN102174285A (en) * | 2011-03-04 | 2011-09-07 | 苏州市金近涂料有限公司 | Aqueous anti-corrosion and anti-frost paint for steel structure and preparation method thereof |
| CN102181196A (en) * | 2011-01-24 | 2011-09-14 | 张兴艺 | Water-in-water colorful stone simulated paint |
| CN102391767A (en) * | 2011-07-07 | 2012-03-28 | 聂群锋 | High-solid-content interior and exterior crosslinked type water-in-water colorful granite paint and preparation method thereof |
| CN102660178A (en) * | 2012-05-08 | 2012-09-12 | 新疆红山涂料有限公司 | Production method of odor-free total effect emulsion paint |
| CN103183994A (en) * | 2011-12-31 | 2013-07-03 | 青岛乐化科技有限公司 | Camouflage cooling coating material |
| CN104725944A (en) * | 2013-12-18 | 2015-06-24 | 浙江曼得丽涂料有限公司 | Aqueous rock color paint and preparation method thereof |
| CN105440811A (en) * | 2014-09-02 | 2016-03-30 | 立邦涂料（中国）有限公司 | Aqueous liquid simulation wallpaper coating, coating layer and product |
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| CN102181196A (en) * | 2011-01-24 | 2011-09-14 | 张兴艺 | Water-in-water colorful stone simulated paint |
| CN102174285A (en) * | 2011-03-04 | 2011-09-07 | 苏州市金近涂料有限公司 | Aqueous anti-corrosion and anti-frost paint for steel structure and preparation method thereof |
| CN102174285B (en) * | 2011-03-04 | 2013-09-11 | 苏州市金近涂料有限公司 | Aqueous anti-corrosion and anti-frost paint for steel structure and preparation method thereof |
| CN102167944B (en) * | 2011-05-31 | 2013-02-13 | 苏州市金近涂料有限公司 | Water-based dipping lacquer and preparation method thereof |
| CN102167944A (en) * | 2011-05-31 | 2011-08-31 | 苏州市金近涂料有限公司 | Water-based dipping lacquer and preparation method thereof |
| CN102391767B (en) * | 2011-07-07 | 2013-07-24 | 嘉兴市威纳建材有限公司 | High-solid-content interior and exterior crosslinked type water-in-water colorful granite paint and preparation method thereof |
| CN102391767A (en) * | 2011-07-07 | 2012-03-28 | 聂群锋 | High-solid-content interior and exterior crosslinked type water-in-water colorful granite paint and preparation method thereof |
| CN103183994A (en) * | 2011-12-31 | 2013-07-03 | 青岛乐化科技有限公司 | Camouflage cooling coating material |
| CN103183994B (en) * | 2011-12-31 | 2016-08-17 | 青岛乐化科技有限公司 | Camouflage cool coat material |
| CN102660178A (en) * | 2012-05-08 | 2012-09-12 | 新疆红山涂料有限公司 | Production method of odor-free total effect emulsion paint |
| CN102660178B (en) * | 2012-05-08 | 2014-02-19 | 新疆红山涂料有限公司 | Production method of odor-free total effect emulsion paint |
| CN104725944A (en) * | 2013-12-18 | 2015-06-24 | 浙江曼得丽涂料有限公司 | Aqueous rock color paint and preparation method thereof |
| CN105440811A (en) * | 2014-09-02 | 2016-03-30 | 立邦涂料（中国）有限公司 | Aqueous liquid simulation wallpaper coating, coating layer and product |
| CN107189605A (en) * | 2017-05-09 | 2017-09-22 | 河北晨阳工贸集团有限公司 | Reflective insulation water-in-water multicolor coating and preparation method thereof |
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Open date: 20090114 |