CN107573791A - A kind of environment-friendly type inner wall face sealing wax - Google Patents
A kind of environment-friendly type inner wall face sealing wax Download PDFInfo
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- CN107573791A CN107573791A CN201710883123.8A CN201710883123A CN107573791A CN 107573791 A CN107573791 A CN 107573791A CN 201710883123 A CN201710883123 A CN 201710883123A CN 107573791 A CN107573791 A CN 107573791A
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Abstract
The present invention relates to sealing wax processing technique field, discloses a kind of environment-friendly type inner wall face sealing wax, contains following component according to mass percent meter：Silicone acrylic emulsion, which accounts for 25 27%, rutile titanium white powder and accounts for 20 22%, cellulose and account for 0.15 0.17%, dispersant and account for 0.8 0.9%, wetting agent and account for 0.12 0.14%, defoamer and account for 0.2 0.3%, anticorrosion and bactericidal agent and account for 0.2 0.3%, propane diols and account for 1.8 2.0%, coalescents and account for 1.6 1.8%, PH nertralizers and account for 0.15 0.20%, polyurethane levelling agent and account for 0.2 0.3%, thickener and account for 0.2 0.3%, mould inhibitor and account for 0.2 0.3%, filler, accounts for 20 25%, remaining as deionized water；Organosilicon acrylic resin is modified, the sealing wax environment protection health being prepared, there is the performances such as excellent weatherability, water resistance, alkali resistance, stain resistant and scrubbing resistance.
Description
Technical field
The invention belongs to sealing wax processing technique field, and in particular to a kind of environment-friendly type inner wall face sealing wax.
Background technology
With the continuous enhancing of mankind's environmental consciousness, various countries put into effect organic volatile among relevant law limitation coating successively
The use of property solvent.Also many related laws and regulations have been put into effect to encourage the research and development of environmental protection coating material and production in China.World's model
Coating expert in enclosing develops various environmental protection coating materials successively by constantly making great efforts and innovating.Mainly include:Powdery paints, water
Property coating, high solid coating etc..Wherein water paint is using water as solvent, and it avoids a large amount of uses of organic solvent, no
But pollute and avoid due to the wasting of resources caused by a large amount of uses of organic solvent caused by reducing solvent volatilization, therefore,
It occupies very important status in environmental protection coating material field.
Environmental protection coating material refers in the links such as raw material selection, product manufacturing, construction nonhazardous, pollution-free, is advantageous to human body
Health and the construction material of environmental protection.Indoors decorate in, interior wall coating turn into can not or few product, it is a variety of environment friendly coated
Material is all applied to interior decoration, but independently select from consumer and use from the point of view of, mainly still concentrate on water paint
Aspect.With the improvement of living standards, people it is also proposed higher requirement to interior wall coating and woodwork coating, i.e. interior wall applies
Material not only wants high-performance, high function, and more should be greenization, to health non-hazardous.Therefore, healthy functions type ring is protected
The research and development of inner wall surface sealing wax are extremely urgent.
The content of the invention
The purpose of the present invention is to be directed to the problem of existing, there is provided a kind of environment-friendly type inner wall face sealing wax, organosilicon acrylic resin is entered
Row is modified, the sealing wax environment protection health being prepared, and has excellent weatherability, water resistance, alkali resistance, stain resistant and scrubbing resistance etc.
Performance, also with antibacterial, deodorization etc. to human body beneficial effect.
The present invention is achieved by the following technical solutions：
A kind of environment-friendly type inner wall face sealing wax, contain following component according to mass percent meter：Silicone acrylic emulsion accounts for 25-27%, rutile
Titanium dioxide accounts for 20-22%, cellulose accounts for 0.15-0.17%, dispersant accounts for 0.8-0.9%, wetting agent accounts for 0.12-0.14%, defoamer
Account for 0.2-0.3%, anticorrosion and bactericidal agent accounts for 0.2-0.3%, propane diols accounts for 1.8-2.0%, coalescents account for 1.6-1.8%, PH nertralizer
Account for 0.15-0.20%, polyurethane levelling agent accounts for 0.2-0.3%, thickener accounts for 0.2-0.3%, mould inhibitor accounts for 0.2-0.3%, filler accounts for
20-25%, remaining as deionized water；
Its preparation for processing comprises the following steps：（1）Cellulose is added in deionized water and disperseed, dispersing speed control
In 1000-1200 revs/min of scope, disperse 10-15 minutes, rotating speed is adjusted to 400-500 revs/min by cellulose after melting；
（2）The PH nertralizers of dispersant → wetting agent → anticorrosion and bactericidal agent → propane diols → 1/2 are sequentially added into above-mentioned system
→ 1/2 defoamer, by dispersing speed control in 600-800 revs/min of scope, uniform stirring 15-20 minutes, reduction stirring
Speed stirs to 400-500 revs/min；
（3）Dispersing speed is brought up to 1200-1300 revs/min, filler is added, is sequentially rutile titanium white powder → kaolin
→ dicalcium powder → talcum powder, is dispersed with stirring 25-30 minutes；
（4）After scattered, by rotating speed control in 400-500 revs/min of scope, add successively silicone acrylic emulsion → coalescents →
Defoamer → thickener → polyurethane levelling agent of 1/ 2PH nertralizer → 1/2, be dispersed with stirring uniformly, obtain finished product according to want
Addition aqueous color paste is asked to be mixed colours.
Further described as to such scheme, the silicone acrylic emulsion is modified in preparation：Propylene will be mixed
Acid esters and AAEM mixing, mixed proportion 30-35:1, add the hydroxyl that volume fraction is 10-15%
Base silicone oil, is uniformly dispersed with dispersion machine, is then added in the aqueous solution containing emulsifying agent, with 2O-30 points of high speed dispersor stirring
Clock, then by mixed liquor ultrasound 10-15 minutes, put into and be equipped with four mouthfuls of agitator, condenser pipe, dropping funel and thermometer
In flask, the 35-40% of flask volume is accounted for, adds-methacryloxypropyl trimethoxy silane, accounts for flask volume
10-15%, be warming up to 70-80 DEG C, react 3-4 hours, add the silicon dioxide gel that mass fraction is 0.5-1.0%, stirring
After uniformly, 25-30 DEG C is cooled to, adjustment system pH value is that 7.2-7.3 can discharge.
Further described as to such scheme, the filler consists of the following composition in parts by weight：Kaolin
6-8 parts, dicalcium powder 12-14 parts, talcum powder 8-10 parts.
Further described as to such scheme, the mixing acrylate contains according to mass percent meter：Methyl
Methyl acrylate accounts for 30-40%, butyl acrylate accounts for 20-30%, remaining as Isooctyl acrylate monomer.
Further described as to such scheme, emulsifier content is 1.0- in the aqueous solution containing emulsifying agent
1.5%, volume is 1.5-2.0 times of scattered mixed ester.
The present invention has advantages below compared with prior art：In order to solve existing interior wall sealing wax health environment-friendly deficiency
Problem, the invention provides a kind of environment-friendly type inner wall face sealing wax, organosilicon acrylic resin is modified, has investigated auxiliary agent species and dosage
Influence to coating, solve that cohesive force of the Ludox during dehydrating polycondensation is excessive, and the cracking for easily causing film is asked
Topic, the sealing wax environment protection health being prepared, the coating VOC content it is low and can preferable formaldehyde adsorption the features such as, be a kind of new
The feature of environmental protection interior wall coating of type, there is the performances such as excellent weatherability, water resistance, alkali resistance, stain resistant and scrubbing resistance, also have
Antibacterial, deodorization etc. are to human body beneficial effect.
Embodiment
With reference to specific embodiment, the invention will be further described.
Embodiment 1
A kind of environment-friendly type inner wall face sealing wax, contain following component according to mass percent meter：Silicone acrylic emulsion accounts for 25%, rutile titanium
White powder, which accounts for 20%, cellulose and accounts for 0.15%, dispersant and account for 0.8%, wetting agent and account for 0.12%, defoamer and account for 0.2%, anticorrosion and bactericidal agent, to be accounted for
0.2%th, propane diols, which accounts for 1.8%, coalescents and accounts for 1.6%, PH nertralizers and account for 0.15%, polyurethane levelling agent, accounts for 0.2%, thickener and accounts for
0.2%th, mould inhibitor accounts for 0.2%, filler and accounts for 20%, remaining as deionized water；
Its preparation for processing comprises the following steps：（1）Cellulose is added in deionized water and disperseed, dispersing speed control
In 1000-1200 revs/min of scope, disperse 10 minutes, rotating speed is adjusted to 400 revs/min by cellulose after melting；
（2）The PH nertralizers of dispersant → wetting agent → anticorrosion and bactericidal agent → propane diols → 1/2 are sequentially added into above-mentioned system
→ 1/2 defoamer, by dispersing speed control in 600-800 revs/min of scope, uniform stirring 15 minutes, reduction stirring speed
Degree stirs to 400 revs/min；
（3）Dispersing speed is brought up to 1200-1300 revs/min, filler is added, is sequentially rutile titanium white powder → kaolin
→ dicalcium powder → talcum powder, it is dispersed with stirring 25 minutes；
（4）After scattered, by rotating speed control in 400-500 revs/min of scope, add successively silicone acrylic emulsion → coalescents →
Defoamer → thickener → polyurethane levelling agent of 1/ 2PH nertralizer → 1/2, be dispersed with stirring uniformly, obtain finished product according to want
Addition aqueous color paste is asked to be mixed colours.
Further described as to such scheme, the silicone acrylic emulsion is modified in preparation：Propylene will be mixed
Acid esters and AAEM mixing, mixed proportion 30:1, add the hydroxyl silicon that volume fraction is 10%
Oil, it is uniformly dispersed, is then added in the aqueous solution containing emulsifying agent with dispersion machine, is stirred 2O minutes with high speed dispersor, then will
Mixed liquor ultrasound 10 minutes, puts into the four-hole boiling flask for being equipped with agitator, condenser pipe, dropping funel and thermometer, accounts for
The 35% of flask volume ,-methacryloxypropyl trimethoxy silane is added, account for the 10% of flask volume, be warming up to
70 DEG C, react 3 hours, add the silicon dioxide gel that mass fraction is 0.5%, after stirring, be cooled to 25 DEG C, adjusting body
It is that pH value can discharge for 7.2.
Further described as to such scheme, the filler consists of the following composition in parts by weight：Kaolin 6
Part, 12 parts of dicalcium powder, 8 parts of talcum powder.
Further described as to such scheme, the mixing acrylate contains according to mass percent meter：Methyl
Methyl acrylate accounts for 30%, butyl acrylate and accounts for 20%, remaining as Isooctyl acrylate monomer.
Being further described as to such scheme, emulsifier content is 1.0% in the aqueous solution containing emulsifying agent,
Volume is 1.5 times of scattered mixed ester.
Embodiment 2
A kind of environment-friendly type inner wall face sealing wax, contain following component according to mass percent meter：Silicone acrylic emulsion accounts for 26%, rutile titanium
White powder, which accounts for 21%, cellulose and accounts for 0.16%, dispersant and account for 0.85%, wetting agent and account for 0.13%, defoamer, accounts for 0.25%, anticorrosion and bactericidal agent
Account for 0.25%, propane diols account for 1.9%, coalescents account for 1.7%, PH nertralizers account for 0.18%, polyurethane levelling agent account for 0.25%, thickening
Agent, which accounts for 0.25%, mould inhibitor and accounts for 0.25%, filler, accounts for 23%, remaining as deionized water；
Its preparation for processing comprises the following steps：（1）Cellulose is added in deionized water and disperseed, dispersing speed control
In 1000-1200 revs/min of scope, disperse 12 minutes, rotating speed is adjusted to 450 revs/min by cellulose after melting；
（2）The PH nertralizers of dispersant → wetting agent → anticorrosion and bactericidal agent → propane diols → 1/2 are sequentially added into above-mentioned system
→ 1/2 defoamer, by dispersing speed control in 600-800 revs/min of scope, uniform stirring 18 minutes, reduction stirring speed
Degree stirs to 450 revs/min；
（3）Dispersing speed is brought up to 1250 revs/min, filler is added, is sequentially rutile titanium white powder → kaolin → weight
Calcium powder → talcum powder, it is dispersed with stirring 28 minutes；
（4）After scattered, by rotating speed control in 400-500 revs/min of scope, add successively silicone acrylic emulsion → coalescents →
Defoamer → thickener → polyurethane levelling agent of 1/ 2PH nertralizer → 1/2, be dispersed with stirring uniformly, obtain finished product according to want
Addition aqueous color paste is asked to be mixed colours.
Further described as to such scheme, the silicone acrylic emulsion is modified in preparation：Propylene will be mixed
Acid esters and AAEM mixing, mixed proportion 33:1, add the hydroxyl silicon that volume fraction is 13%
Oil, it is uniformly dispersed, is then added in the aqueous solution containing emulsifying agent with dispersion machine, is stirred 25 minutes with high speed dispersor, then will
Mixed liquor ultrasound 13 minutes, puts into the four-hole boiling flask for being equipped with agitator, condenser pipe, dropping funel and thermometer, accounts for
The 38% of flask volume ,-methacryloxypropyl trimethoxy silane is added, account for the 12% of flask volume, be warming up to
75 DEG C, react 3.5 hours, add the silicon dioxide gel that mass fraction is 0.8%, after stirring, be cooled to 28 DEG C, adjustment
System pH value can discharge for 7.2.
Further described as to such scheme, the filler consists of the following composition in parts by weight：Kaolin 7
Part, 13 parts of dicalcium powder, 9 parts of talcum powder.
Further described as to such scheme, the mixing acrylate contains according to mass percent meter：Methyl
Methyl acrylate accounts for 35%, butyl acrylate and accounts for 25%, remaining as Isooctyl acrylate monomer.
Being further described as to such scheme, emulsifier content is 1.2% in the aqueous solution containing emulsifying agent,
Volume is 1.7 times of scattered mixed ester.
Embodiment 3
A kind of environment-friendly type inner wall face sealing wax, contain following component according to mass percent meter：Silicone acrylic emulsion accounts for 27%, rutile titanium
White powder, which accounts for 22%, cellulose and accounts for 0.17%, dispersant and account for 0.9%, wetting agent and account for 0.14%, defoamer and account for 0.3%, anticorrosion and bactericidal agent, to be accounted for
0.3%th, propane diols, which accounts for 2.0%, coalescents and accounts for 1.8%, PH nertralizers and account for 0.20%, polyurethane levelling agent, accounts for 0.3%, thickener and accounts for
0.3%th, mould inhibitor accounts for 0.3%, filler and accounts for 25%, remaining as deionized water；
Its preparation for processing comprises the following steps：（1）Cellulose is added in deionized water and disperseed, dispersing speed control
In 1000-1200 revs/min of scope, disperse 15 minutes, rotating speed is adjusted to 500 revs/min by cellulose after melting；
（2）The PH nertralizers of dispersant → wetting agent → anticorrosion and bactericidal agent → propane diols → 1/2 are sequentially added into above-mentioned system
→ 1/2 defoamer, by dispersing speed control in 600-800 revs/min of scope, uniform stirring 20 minutes, reduction stirring speed
Degree stirs to 500 revs/min；
（3）Dispersing speed is brought up to 1300 revs/min, filler is added, is sequentially rutile titanium white powder → kaolin → weight
Calcium powder → talcum powder, it is dispersed with stirring 30 minutes；
（4）After scattered, by rotating speed control in 400-500 revs/min of scope, add successively silicone acrylic emulsion → coalescents →
Defoamer → thickener → polyurethane levelling agent of 1/ 2PH nertralizer → 1/2, be dispersed with stirring uniformly, obtain finished product according to want
Addition aqueous color paste is asked to be mixed colours.
Further described as to such scheme, the silicone acrylic emulsion is modified in preparation：Propylene will be mixed
Acid esters and AAEM mixing, mixed proportion 35:1, add the hydroxyl silicon that volume fraction is 15%
Oil, it is uniformly dispersed, is then added in the aqueous solution containing emulsifying agent with dispersion machine, is stirred 30 minutes with high speed dispersor, then will
Mixed liquor ultrasound 15 minutes, puts into the four-hole boiling flask for being equipped with agitator, condenser pipe, dropping funel and thermometer, accounts for
The 40% of flask volume ,-methacryloxypropyl trimethoxy silane is added, account for the 15% of flask volume, be warming up to
80 DEG C, react -4 hours, add the silicon dioxide gel that mass fraction is 1.0%, after stirring, be cooled to 30 DEG C, adjusting body
It is that pH value can discharge for 7.3.
Further described as to such scheme, the filler consists of the following composition in parts by weight：Kaolin 8
Part, 14 parts of dicalcium powder, 10 parts of talcum powder.
Further described as to such scheme, the mixing acrylate contains according to mass percent meter：Methyl
Methyl acrylate accounts for 40%, butyl acrylate and accounts for 30%, remaining as Isooctyl acrylate monomer.
Being further described as to such scheme, emulsifier content is 1.5% in the aqueous solution containing emulsifying agent,
Volume is 2.0 times of scattered mixed ester.
Comparative example 1
With differing only in for embodiment 1, the non-modified processing of organosilicon acrylic resin, remaining is consistent.
Comparative example 2
With differing only in for embodiment 2, in preparation method, cellulose is added and mixed jointly with silicone acrylic emulsion, remaining holding
Unanimously.
Comparative example 3
With differing only in for embodiment 3, in preparation method, defoamer and film forming agent disposably add, and remaining is consistent.
Contrast experiment
Embodiment 1-3 and comparative example 1-3 method processing and fabricating water-based inner wall finish paint is used respectively, while with existing environment-friendly type
For water-based interior paint as control, coating prepared by each group carries out performance comparision, as a result as shown in the table：
As can be seen here：The present invention is modified to organosilicon acrylic resin, the sealing wax environment protection health being prepared, and is had excellent weather-proof
The performance such as property, water resistance, alkali resistance, stain resistant and scrubbing resistance.
Claims (5)
1. a kind of environment-friendly type inner wall face sealing wax, it is characterised in that contain following component according to mass percent meter：Silicone acrylic emulsion accounts for
25-27%, rutile titanium white powder account for 20-22%, cellulose accounts for 0.15-0.17%, dispersant accounts for 0.8-0.9%, wetting agent accounts for 0.12-
0.14%th, defoamer accounts for 0.2-0.3%, anticorrosion and bactericidal agent accounts for 0.2-0.3%, propane diols accounts for 1.8-2.0%, coalescents account for 1.6-
1.8%th, PH nertralizers account for 0.15-0.20%, polyurethane levelling agent accounts for 0.2-0.3%, thickener accounts for 0.2-0.3%, mould inhibitor accounts for
0.2-0.3%, filler account for 20-25%, remaining as deionized water；
Its preparation for processing comprises the following steps：（1）Cellulose is added in deionized water and disperseed, dispersing speed control
In 1000-1200 revs/min of scope, disperse 10-15 minutes, rotating speed is adjusted to 400-500 revs/min by cellulose after melting；
（2）The PH nertralizers of dispersant → wetting agent → anticorrosion and bactericidal agent → propane diols → 1/2 are sequentially added into above-mentioned system
→ 1/2 defoamer, by dispersing speed control in 600-800 revs/min of scope, uniform stirring 15-20 minutes, reduction stirring
Speed stirs to 400-500 revs/min；
（3）Dispersing speed is brought up to 1200-1300 revs/min, filler is added, is sequentially rutile titanium white powder → kaolin
→ dicalcium powder → talcum powder, is dispersed with stirring 25-30 minutes；
（4）After scattered, by rotating speed control in 400-500 revs/min of scope, add successively silicone acrylic emulsion → coalescents →
Defoamer → thickener → polyurethane levelling agent of 1/ 2PH nertralizer → 1/2, be dispersed with stirring uniformly, obtain finished product according to want
Addition aqueous color paste is asked to be mixed colours.
2. a kind of environment-friendly type inner wall face as claimed in claim 1 sealing wax, it is characterised in that the silicone acrylic emulsion is carried out in preparation
Modification：Mixing acrylate and AAEM are mixed, mixed proportion 30-35:1, add body
Fraction is 10-15% hydroxy silicon oil, is uniformly dispersed, is then added in the aqueous solution containing emulsifying agent with dispersion machine, with a high speed
Dispersion machine stirs 2O-30 minutes, then by mixed liquor ultrasound 10-15 minutes, puts into and be equipped with agitator, condenser pipe, dropping liquid leakage
In the four-hole boiling flask of bucket and thermometer, the 35-40% of flask volume is accounted for, adds-methacryloxypropyl trimethoxy
Base silane, the 10-15% of flask volume is accounted for, be warming up to 70-80 DEG C, react 3-4 hours, it is 0.5-1.0%'s to add mass fraction
Silicon dioxide gel, after stirring, 25-30 DEG C is cooled to, adjustment system pH value is that 7.2-7.3 can discharge.
A kind of 3. environment-friendly type inner wall face sealing wax as claimed in claim 1, it is characterised in that the filler in parts by weight by with
Lower composition composition：Kaolin 6-8 parts, dicalcium powder 12-14 parts, talcum powder 8-10 parts.
A kind of 4. environment-friendly type inner wall face sealing wax as claimed in claim 1 or 2, it is characterised in that the mixing acrylate according to
Mass percent meter contains：Methyl methacrylate accounts for 30-40%, butyl acrylate accounts for 20-30%, different pungent remaining as acrylic acid
Ester.
5. a kind of environment-friendly type inner wall face as claimed in claim 1 or 2 sealing wax, it is characterised in that described to contain the water-soluble of emulsifying agent
Emulsifier content is 1.0-1.5% in liquid, and volume is 1.5-2.0 times of scattered mixed ester.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710883123.8A CN107573791A (en) | 2017-09-26 | 2017-09-26 | A kind of environment-friendly type inner wall face sealing wax |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710883123.8A CN107573791A (en) | 2017-09-26 | 2017-09-26 | A kind of environment-friendly type inner wall face sealing wax |
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Family
ID=61038557
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| CN201710883123.8A Withdrawn CN107573791A (en) | 2017-09-26 | 2017-09-26 | A kind of environment-friendly type inner wall face sealing wax |
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| CN109135462A (en) * | 2018-07-08 | 2019-01-04 | 张文杰 | A kind of anti-pollution fungicidal paint and preparation method thereof |
| CN109321068A (en) * | 2018-10-19 | 2019-02-12 | 华夏创美(北京）科技有限公司 | A kind of preparation method for the preparation removing interior decoration peculiar smell |
| CN109504209A (en) * | 2018-10-19 | 2019-03-22 | 华夏创美(北京）科技有限公司 | A kind of preparation method for removing decomposing formaldehyde preparation |
| CN110128884A (en) * | 2019-06-18 | 2019-08-16 | 淮北庆丰涂料有限公司 | A kind of children special-purpose metope net taste paint and preparation method thereof |
| CN110385918A (en) * | 2018-04-23 | 2019-10-29 | 苏汉东 | A kind of multi-angle automatic tracing metope colored drawing machine |
| CN111704839A (en) * | 2020-07-16 | 2020-09-25 | 江门市锦富百年建材有限公司 | Multifunctional coating |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110385918A (en) * | 2018-04-23 | 2019-10-29 | 苏汉东 | A kind of multi-angle automatic tracing metope colored drawing machine |
| CN109135462A (en) * | 2018-07-08 | 2019-01-04 | 张文杰 | A kind of anti-pollution fungicidal paint and preparation method thereof |
| CN109321068A (en) * | 2018-10-19 | 2019-02-12 | 华夏创美(北京）科技有限公司 | A kind of preparation method for the preparation removing interior decoration peculiar smell |
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| CN110128884A (en) * | 2019-06-18 | 2019-08-16 | 淮北庆丰涂料有限公司 | A kind of children special-purpose metope net taste paint and preparation method thereof |
| CN111704839A (en) * | 2020-07-16 | 2020-09-25 | 江门市锦富百年建材有限公司 | Multifunctional coating |
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