CN105670429A - Water-based matte clear top-coat for furniture - Google Patents
Water-based matte clear top-coat for furniture Download PDFInfo
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- CN105670429A CN105670429A CN201610076697.XA CN201610076697A CN105670429A CN 105670429 A CN105670429 A CN 105670429A CN 201610076697 A CN201610076697 A CN 201610076697A CN 105670429 A CN105670429 A CN 105670429A
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- water
- dumb light
- furniture
- clear finish
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses water-based matte clear top-coat for furniture. The water-based matte clear top-coat is composed of, by weight, 100-120 parts of modified acrylic emulsion, 1-1.4 parts of an antifoaming agent, 16-20 parts of matte slurry, 4-6 parts of a coalescing agent, 2-3 parts of poly butyl acrylate, 2-4 parts of thickener, 0.8-1 part of polyethyleneimine and 1-3 parts of polybenzimidazole. According to the water-based matte clear top-coat, sodium polyacrylate is adopted as dispersant, the surface of matting powder can be well moistened, micro bubbles on the surface of the matting powder are eliminated, the matting powder can be better wrapped in emulsion particles, a coating which is relatively more uniform is achieved, scattering of light cannot occur easily inside the coating, thereby better transparency is achieved, all raw materials are reasonable in complex formulation, and the top-coat has the excellent decoration performance and protection effect for furniture woodenware, is easy to construct and applicable to multiple types of construction modes such as spraying, electrostatic spraying and brush coating and contains no chemical substance harmful to the human body.
Description
Technical field
The present invention relates to a kind of furniture clear finish, relate in particular to a kind of water-based dumb light furniture clear finish.
Background technology
Water-borne wood coating divides by its gloss, can be divided into dumb light, half matte and glossy, is coated with at present at furnitureThe application of material market is matte varnish very widely, enjoys consumers in general's because its gloss is soft, feel is fine and smoothFavor. But in actual formula Design, there are a lot of problems in water-based matte varnish, such as flatting silica notThe bin stability of easy dispersion, coating, the transparency of final film etc., particularly Black walnut, black palm fibreWood etc. are particularly evident on dark ground, and it often, with mist shadow, blue light, the disadvantage such as turn white, has restricted aqueous wooden wareThe market development confidence of coating. At present, the transparence evaluating of woodwork coating is relied on to coating working to a great extentPerson's experience accumulation, lacks corresponding examination criteria, and this has also increased subjectivity on evaluation means, makes formulaFurther optimization acceptor to see influence degree larger;
Wood furniture alcohol acid and polyurethane white finish paint on market, though there is good decorative effect, contains benzene class etc.The material of harmful health, and solvent and a small amount of free TDI residence time long, not volatile, smellBe difficult to eliminate. So exploitation is without benzene, clean taste, low-free TDI, the furniture lacquer new product that is harmful to human healthParticularly necessary.
Summary of the invention
The present invention has overcome the shortcomings such as the not environmental protection existing in prior art, provides a kind of water-based dumb light furniture clearFinish paint.
The present invention is achieved by the following technical solutions:
A kind of water-based dumb light furniture clear finish, it is made up of the raw material of following weight parts:
Modified acrylic acid emulsion 100-120, defoamer 1-1.4, mute slurry 16-20, coalescents 4-6, polypropyleneAcid butyl ester 2-3, thickener 2-4, polymine 0.8-1, polybenzimidazoles 1-3.
A kind of water-based dumb light furniture clear finish, described defoamer is dimethicone.
A kind of water-based dumb light furniture clear finish, described mute slurry is made up of the raw material of following weight parts:
Polyurethanes 0.4-1, ethoxylated alkyl ammonium sulfate 2-3, propane diols 1-2, nanometer titanium dioxideSilicon 10-17, Sodium Polyacrylate 2-3, HMPA 0.1-0.2, deionized water 70-80, tetrahydrochysene chaffAlcohol 0.7-1, linolenic acid 1-2.
A kind of water-based dumb light furniture clear finish, described coalescents is made up of the raw material of following weight parts:
Propane diols phenylate 20-30, oleic acid diethyl amide 0.8-1, acetylated lanolin 3-4, methyl mercaptanTin 0.01-0.02, γ-methacryloxypropyl trimethoxy silane 0.5-1, polyglycereol castor-oil plant alcohol ester1-2。
A kind of water-based dumb light furniture clear finish, described thickener is made up of the raw material of following weight parts:
Polyvinyl alcohol 10-16, rosin 3-5, phosphite ester 1-2, sodium lauroyl sarcosine 0.7-1, diphenylSilicon diol 3-4, maleic anhydride 1-2.
A kind of water-based dumb light furniture clear finish, described modified acrylic acid emulsion is the raw material group by following weight partsBecome:
Phytic acid 3-4, alum 4.3-5, cellulose propionate 0.7-1, sweet mellow wine 2-3, acrylic acidEmulsion 100-110, glycerin polyoxyethylene ether cocounut oil acid esters 1-2, Span-800.4-1, ammonium fluoroborate 1-2.
A kind of water-based dumb light furniture clear finish, the preparation method of described mute slurry comprises the following steps:
(1) get the 40-50% of above-mentioned deionized water weight, add ethoxylated alkyl ammonium sulfate, stirring conditionUnder add tetrahydrofurfuryl alcohol, be heated to 70-80 DEG C, add Sodium Polyacrylate, be stirred to normal temperature, obtain dispersion liquid;
(2) nano silicon is joined in remaining deionized water, ultrasonic 1-2 minute, adds flaxOleic acid, stirs, and mixes with above-mentioned dispersion liquid, adds polyurethanes, HMPA, risesHigh-temperature is 70-80 DEG C, the sulfuric acid that dropping concentration is 96-98%, and adjusting PH is 2-3, insulation reaction 40-50Minute, cooling, add the each raw material of residue, stir, to obtain final product.
A kind of water-based dumb light furniture clear finish, the preparation method of described coalescents comprises the following steps:
(1) acetylated lanolin, polyglycereol castor-oil plant alcohol ester are mixed, be heated to 50-60 DEG C, add methylTin mercaptides, is stirred to normal temperature;
(2) above-mentioned oleic acid diethyl amide is joined in propane diols phenylate, stir, add above-mentioned stepSuddenly the compound of (1), adds γ-methacryloxypropyl trimethoxy silane under stirring condition, stirsEvenly, to obtain final product.
A kind of water-based dumb light furniture clear finish, described thickener is that above-mentioned each raw material is mixed, at 70-75 DEG CLower insulated and stirred 20-30 minute, cooling, to obtain final product.
A kind of water-based dumb light furniture clear finish, the preparation method of described modified acrylic acid emulsion comprises following stepRapid:
(1) alum is joined in 4-6 times of deionized water, stirs, add cellulose propionate,Send in the water-bath of 80-90 DEG C, insulated and stirred 10-14 minute, adds the 10-16% of acrylic emulsion weight,Continue insulated and stirred 3-5 minute, discharging is cooling;
(2) above-mentioned phytic acid is joined in remaining acrylic emulsion, under stirring condition, add glycerineAPEO cocounut oil acid esters, insulated and stirred 10-13 minute at 60-70 DEG C, obtains with above-mentioned steps (1)The compound arriving mixes, and adds the each raw material of residue under stirring condition, and 600-1000 rev/min is stirred 20-30 minute,Obtain.
Compared with prior art, advantage of the present invention is:
The present invention adopts Sodium Polyacrylate as dispersant, can well soak the surface of flatting silica, and elimination disappearsThe microvesicle on light powder surface, is wrapped in emulsion particle flatting silica better, realizes film relatively more even,Be not easy to occur scattering of light in film inside, thereby realize good transparency, each raw material is composite rationally, thisThe finish paint of invention has good ornamental and protection effect to furniture woodenware, and is easy to construction, applicable spraying,The multiple form of construction work such as electrostatic spraying, brushing, does not contain the chemical substance of harmful health.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail:
Embodiment 1:
A kind of water-based dumb light furniture clear finish, it is made up of the raw material of following weight parts:
Modified acrylic acid emulsion 120, defoamer 1.4, mute slurry 20, coalescents 6, butyl polyacrylate 2,Thickener 2, polymine 0.8, polybenzimidazoles 3.
A kind of water-based dumb light furniture clear finish, described defoamer is dimethicone.
A kind of water-based dumb light furniture clear finish, described mute slurry is made up of the raw material of following weight parts:
Polyurethanes 0.4, ethoxylated alkyl ammonium sulfate 3, propane diols 2, nano silicon 17,Sodium Polyacrylate 2, HMPA 0.1, deionized water 80, tetrahydrofurfuryl alcohol 0.7, linolenic acid 2.
A kind of water-based dumb light furniture clear finish, described coalescents is the raw material composition of field following weight parts:
Propane diols phenylate 30, oleic acid diethyl amide 0.8, acetylated lanolin 3, Methyl stannum mercaptide 0.02,γ-methacryloxypropyl trimethoxy silane 0.5, polyglycereol castor-oil plant alcohol ester 1.
A kind of water-based dumb light furniture clear finish, described thickener is made up of the raw material of following weight parts:
Polyvinyl alcohol 16, rosin 3, phosphite ester 2, sodium lauroyl sarcosine 0.7, diphenyl silanediol 4,Maleic anhydride 1.
A kind of water-based dumb light furniture clear finish, described modified acrylic acid emulsion is the raw material group by following weight partsBecome:
Phytic acid 4, alum 4.3, cellulose propionate 0.7, sweet mellow wine 3, acrylic emulsion 110,Glycerin polyoxyethylene ether cocounut oil acid esters 1, Span-800.4, ammonium fluoroborate 2.
A kind of water-based dumb light furniture clear finish, the preparation method of described mute slurry comprises the following steps:
(1) get 50% of above-mentioned deionized water weight, add ethoxylated alkyl ammonium sulfate, under stirring conditionAdd tetrahydrofurfuryl alcohol, be heated to 80 DEG C, add Sodium Polyacrylate, be stirred to normal temperature, obtain dispersion liquid;
(2) nano silicon is joined in remaining deionized water, ultrasonic 1 minute, add linseed oilAcid, stirs, and mixes with above-mentioned dispersion liquid, adds polyurethanes, HMPA, raisesTemperature is 80 DEG C, the sulfuric acid that dropping concentration is 96-98%, and regulating PH is 3, insulation reaction 50 minutes is coldBut, add the each raw material of residue, stir, to obtain final product.
A kind of water-based dumb light furniture clear finish, the preparation method of described coalescents comprises the following steps:
(1) acetylated lanolin, polyglycereol castor-oil plant alcohol ester are mixed, be heated to 60 DEG C, add methyl mercaptanTin, is stirred to normal temperature;
(2) above-mentioned oleic acid diethyl amide is joined in propane diols phenylate, stir, add above-mentioned stepSuddenly the compound of (1), adds γ-methacryloxypropyl trimethoxy silane under stirring condition, stirsEvenly, to obtain final product.
A kind of water-based dumb light furniture clear finish, described thickener is that above-mentioned each raw material is mixed, at 70-75 DEG CLower insulated and stirred 20 minutes, cooling, to obtain final product.
A kind of water-based dumb light furniture clear finish, the preparation method of described modified acrylic acid emulsion comprises following stepRapid:
(1) alum is joined in 6 times of deionized waters, stir, add cellulose propionate, sendEnter in the water-bath of 90 DEG C, insulated and stirred 14 minutes, adds 16% of acrylic emulsion weight, continues insulation and stirsMix 3 minutes, discharging is cooling;
(2) above-mentioned phytic acid is joined in remaining acrylic emulsion, under stirring condition, add glycerineAPEO cocounut oil acid esters, insulated and stirred 13 minutes at 70 DEG C, with mixing that above-mentioned steps (1) obtainsClose material and mix, add the each raw material of residue under stirring condition, 1000 revs/min are stirred 20 minutes, to obtain final product.
The combination property of finished product:
Bin stability (50 DEG C) is without abnormal;
Hardness B;
Adhesive force (2mm)/level 0;
Resistance to blocking (500g, 50 DEG C, 4h) MM:A-0; MB:A-0;
Resistance to water (24h) is without abnormal;
Boiling water resistance (15min) is without abnormal.
Claims (10)
1. a water-based dumb light furniture clear finish, is characterized in that, it is made up of the raw material of following weight parts:
Modified acrylic acid emulsion 100-120, defoamer 1-1.4, mute slurry 16-20, coalescents 4-6, polypropyleneAcid butyl ester 2-3, thickener 2-4, polymine 0.8-1, polybenzimidazoles 1-3.
2. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedDefoamer is dimethicone.
3. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedMute slurry is made up of the raw material of following weight parts:
Polyurethanes 0.4-1, ethoxylated alkyl ammonium sulfate 2-3, propane diols 1-2, nanometer titanium dioxideSilicon 10-17, Sodium Polyacrylate 2-3, HMPA 0.1-0.2, deionized water 70-80, tetrahydrochysene chaffAlcohol 0.7-1, linolenic acid 1-2.
4. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedCoalescents is made up of the raw material of following weight parts:
Propane diols phenylate 20-30, oleic acid diethyl amide 0.8-1, acetylated lanolin 3-4, methyl mercaptanTin 0.01-0.02, γ-methacryloxypropyl trimethoxy silane 0.5-1, polyglycereol castor-oil plant alcohol ester1-2。
5. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedThickener is made up of the raw material of following weight parts:
Polyvinyl alcohol 10-16, rosin 3-5, phosphite ester 1-2, sodium lauroyl sarcosine 0.7-1, diphenylSilicon diol 3-4, maleic anhydride 1-2.
6. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedModified acrylic acid emulsion is made up of the raw material of following weight parts:
Phytic acid 3-4, alum 4.3-5, cellulose propionate 0.7-1, sweet mellow wine 2-3, acrylic acidEmulsion 100-110, glycerin polyoxyethylene ether cocounut oil acid esters 1-2, Span-800.4-1, ammonium fluoroborate 1-2.
7. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedThe preparation method of mute slurry comprises the following steps:
(1) get the 40-50% of above-mentioned deionized water weight, add ethoxylated alkyl ammonium sulfate, stirring conditionUnder add tetrahydrofurfuryl alcohol, be heated to 70-80 DEG C, add Sodium Polyacrylate, be stirred to normal temperature, obtain dispersion liquid;
(2) nano silicon is joined in remaining deionized water, ultrasonic 1-2 minute, adds flaxOleic acid, stirs, and mixes with above-mentioned dispersion liquid, adds polyurethanes, HMPA, risesHigh-temperature is 70-80 DEG C, the sulfuric acid that dropping concentration is 96-98%, and adjusting PH is 2-3, insulation reaction 40-50Minute, cooling, add the each raw material of residue, stir, to obtain final product.
8. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedThe preparation method of coalescents comprises the following steps:
(1) acetylated lanolin, polyglycereol castor-oil plant alcohol ester are mixed, be heated to 50-60 DEG C, add methylTin mercaptides, is stirred to normal temperature;
(2) above-mentioned oleic acid diethyl amide is joined in propane diols phenylate, stir, add above-mentioned stepSuddenly the compound of (1), adds γ-methacryloxypropyl trimethoxy silane under stirring condition, stirsEvenly, to obtain final product.
9. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedThickener is that above-mentioned each raw material is mixed, and at 70-75 DEG C, insulated and stirred 20-30 minute, cooling, to obtain final product.
10. a kind of water-based dumb light furniture clear finish according to claim 1, is characterized in that, describedThe preparation method of modified acrylic acid emulsion comprises the following steps:
(1) alum is joined in 4-6 times of deionized water, stirs, add cellulose propionate,Send in the water-bath of 80-90 DEG C, insulated and stirred 10-14 minute, adds the 10-16% of acrylic emulsion weight,Continue insulated and stirred 3-5 minute, discharging is cooling;
(2) above-mentioned phytic acid is joined in remaining acrylic emulsion, under stirring condition, add glycerineAPEO cocounut oil acid esters, insulated and stirred 10-13 minute at 60-70 DEG C, obtains with above-mentioned steps (1)The compound arriving mixes, and adds the each raw material of residue under stirring condition, and 600-1000 rev/min is stirred 20-30 minute,Obtain.
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CN201610076697.XA CN105670429A (en) | 2016-02-02 | 2016-02-02 | Water-based matte clear top-coat for furniture |
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CN201610076697.XA CN105670429A (en) | 2016-02-02 | 2016-02-02 | Water-based matte clear top-coat for furniture |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106349853A (en) * | 2016-08-28 | 2017-01-25 | 桐乡市美意家具有限公司 | Fireproof coating for materials for wooden furniture |
CN108586670A (en) * | 2018-04-04 | 2018-09-28 | 广东衡光新材料科技有限公司 | A kind of hydroxyl acrylic aqueous dispersion and its synthetic method |
CN112466663A (en) * | 2020-11-09 | 2021-03-09 | 太仓优盛电子有限公司 | High-temperature dipping treatment process of transformer |
CN113150675A (en) * | 2021-03-24 | 2021-07-23 | 纳琳威纳米科技(上海)有限公司 | Matte self-repairing coating for automobile paint surface protective film and preparation method thereof |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106349853A (en) * | 2016-08-28 | 2017-01-25 | 桐乡市美意家具有限公司 | Fireproof coating for materials for wooden furniture |
CN108586670A (en) * | 2018-04-04 | 2018-09-28 | 广东衡光新材料科技有限公司 | A kind of hydroxyl acrylic aqueous dispersion and its synthetic method |
CN108586670B (en) * | 2018-04-04 | 2021-01-29 | 广东衡光新材料科技有限公司 | Hydroxyl acrylic acid dispersoid and synthetic method thereof |
CN112466663A (en) * | 2020-11-09 | 2021-03-09 | 太仓优盛电子有限公司 | High-temperature dipping treatment process of transformer |
CN113150675A (en) * | 2021-03-24 | 2021-07-23 | 纳琳威纳米科技(上海)有限公司 | Matte self-repairing coating for automobile paint surface protective film and preparation method thereof |
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Application publication date: 20160615 |