CN104212288A - Water-based colourful building coating and preparation method thereof - Google Patents
Water-based colourful building coating and preparation method thereof Download PDFInfo
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Abstract
The invention discloses water-based colourful building coating. The water-based colourful building coating is formed by mixing the following components in percentage by mass: 5-20% of water-based colour paste, 60-70% of colour chip system and 30-40% of emulsion binder. A preparation method of the water-based colourful building coating comprises the following steps: preparing basic paint, matching colour, preparing a protection glue system, preparing a colour chip system, preparing an emulsion binder, and adding the colour chip system into the prepared emulsion binder, thus the stable water-based colourful building coating is formed. The water-based colourful building coating has the advantages that the protection glue system and cellulose in the basic paint interact with each other, so that produced gel is firmly wrapped on the surface of the basic paint of each colour, and surface activity of negative ions provides negative charges to form stable colour chips in various colours; the water-based colourful building coating can improve colour chip stability and storage stability, can prevent precipitation, colour bleeding and muddy water of the water-based colourful particles, is moulded by spraying in one step, good in recoatability, realistic in natural marble imitating effect and simple to maintain, has certain elasticity and can be used for making up micro cracks of a wall body.
Description
Technical field
The present invention relates to a kind of building coating, be specifically related to a kind of aqueous colorful building coating and preparation method thereof.
Background technology
At present, grouan, marble are with its serious texture, and durable quality, deeply by the favor of architect and user, is also one of important symbol of the external image of buildings.But along with China is to the implementation of the protection of natural resources and national building energy conservation, have impact on the widespread use of lithotome in building decoration field to a certain extent.Grouan is constructed comparatively complicated in use as building and ornament materials, not only increase unit body of wall load-bearing, but also exists as the many unsafe factors such as danger that come off; Some marble can discharge trace-level activity element, works the mischief to HUMAN HEALTH.In addition, country improves constantly the requirement of building energy conservation, and also make the application of External Walls Heating Insulation on external wall obtain penetration and promotion, heat insulation base layer carries out stone decoration again, and its construction process is more complicated.In order to pursue grouan appearance effect, people start the stone material exploring a kind of artificial granite of synthetic, and in this context, the colorful building coating of water-water arises at the historic moment.The mid-90 in 20th century, the colorful building coating of China's water bag (calling aqueous colorful building coating in the following text) just becomes the product can applied on buildings, aqueous colorful building coating is the quantum jump in artificial granite paint history, it effectively overcomes the shortcoming that O/W oil-in-water-type artificial granite paint contains the poisonous and harmful substances such as volatile organic compounds, environmental protection more, energy-conservation, be environment-friendly novel material of construction of new generation, there are boundless market outlook.But now, most of aqueous colorful building coating quality is very different on the market, and some stability in storagies are bad, and some colour particles easily condense, easily broken; Some look grain obscure boundaries are clear, and the bleeding of some look grains is serious, drastically influence popularization and the use of aqueous colorful building coating.
Summary of the invention
Object of the present invention is exactly the defect existed for prior art, there is provided one can improve look grain stability, package stability, prevent aqueous colorful particle precipitation, bleeding and muddy water, disposable spray finishing is shaping, recoatability is good, safeguard simple, there is certain elasticity, the aqueous colorful building coating of body of wall fine crack can be made up.
Another technical problem to be solved by this invention is to provide a kind of method preparing above-mentioned aqueous colorful building coating.
Its technical scheme is: aqueous colorful building coating; the aqueous color paste, the mass percent that are 5 ~ 20% by mass percent are that the look plastochondria system of 60 ~ 70% and the emulsion binder of 30 ~ 40% mix, and described look plastochondria system is made up of the base paint of following mass percent and protecting glue system:
Consisting of of described base paint:
Mierocrystalline cellulose 0.7 ~ 1.1% multifunctional assistant 0.1 ~ 0.2%
Dispersion agent 0.1 ~ 0.2% sterilant 0.1 ~ 0.4%
Defoamer 0.2 ~ 0.4% 3.0 ~ 5.0% protecting glue 10 ~ 15%
Film coalescence aid 0.5 ~ 1.0% 20% modified alta-muds 10 ~ 15%
Elastic emulsion 20 ~ 30% color stuffing 4.0 ~ 8.0%
Excess water;
Consisting of of described protecting glue system:
5% ~ 8% protecting glue 60 ~ 65% wetting agent 1.0 ~ 2.0%
4%T-935 protecting glue 35 ~ 40%;
Described look plastochondria system consists of:
Assorted base paint 45 ~ 50% protecting glue system 50 ~ 55%;
Consisting of of described emulsion binder:
Organosilicon crylic acid latex 60 ~ 75% film coalescence aid 4.2 ~ 5.3%
Propylene glycol 1.0 ~ 2.0% defoamer 1.0 ~ 2.0%
Sterilant 0.1 ~ 0.2% thickening material 0.3 ~ 1.0%
Excess water.
Described Mierocrystalline cellulose is nonionic cellulose; Described wetting agent adopts anion surfactant; The described silicate compound of protection rubber powder behaviour wage reform or the wilkinite of modification.
Described film coalescence aid is alkoxide, and described sterilant is anticorrosion and bactericidal agent AQ, and described thickening material is hydrophobically-modified alkali swelling type thickening material.
Described elastic emulsion is synthetic resin emulsion; Described defoamer adopts mineral oil defoaming agent.
Described color stuffing is the arbitrary proportion mixture of one or more in titanium dioxide, kaolin, coarse whiting, wollastonite.
The Chinese of the sheet through modification that described protection rubber powder adopts takes off soil structure-Na magnesium lithium silicates.
The preparation method of aqueous colorful building coating, comprises the following steps:
1) preparation of base paint
Described water, Mierocrystalline cellulose, multifunctional assistant, dispersion agent, defoamer and color stuffing are added in Scattered Kettle successively according to proportioning, high speed dispersion is to fineness less than 50 μm, add under the stirring of middling speed again 3.0 ~ 5.0% protecting glue, film coalescence aid, elastic emulsion, sterilant and 20% modified alta-mud, adjustment viscosity reaches 120-130k μ, can obtain base paint;
2) toning of base paint
The base paint of above-mentioned preparation is put into stirrer stirring at low speed, according to the chromatic pattern feature of the granite building material that will copy, modulates assorted base paint with the aqueous color paste of above-mentioned base paint and coupling;
3) preparation of protecting glue system
Be added to the water by 5% ~ 8% protecting glue of described mass percent, high speed dispersion is dissolved completely to protecting glue, becomes complete transparent liquid, then middling speed stirring under add wetting agent and 4%T-935 protecting glue, mix completely, be protecting glue system;
4) preparation of look plastochondria system
Assorted base paint is added in protecting glue system by above-mentioned mass percent, according to the color grain size of design, selects the square hole sieve of different order number sizes, filter and can obtain required look plastochondria system;
5) preparation of emulsion binder
Described water, film coalescence aid, defoamer, propylene glycol, sterilant and organosilicon crylic acid latex are joined Scattered Kettle successively by proportioning, then adds the viscosity of thickening material adjustment emulsion binder as required, namely obtain emulsion binder;
6) preparation of aqueous colorful building coating
In obtained emulsion binder, add the look plastochondria system of above-mentioned mass percent, namely form stable aqueous colorful building coating.
The present invention compared with prior art, have the following advantages: when assorted base paint is added into after in protecting glue system, Mierocrystalline cellulose in protecting glue system and base paint interacts, the gel produced is made to be wrapped in assorted base paint surface securely, anion surface activity provides negative charge to form stable assorted look grain, the present invention can improve look grain stability, package stability, aqueous colorful particle precipitation can be prevented, bleeding and muddy water, disposable spray finishing is shaping, recoatability is good, imitating natural marble material effect is true to nature, safeguard simple, there is certain elasticity, body of wall fine crack can be made up.
Embodiment
Embodiment one:
Consisting of of described base paint:
Mierocrystalline cellulose 0.8% multifunctional assistant 0.1%
Dispersion agent 0.1% sterilant 0.1%
Titanium dioxide 2.0% kaolin 2.0%
Defoamer 0.4% 3.0 ~ 5.0% protecting glue 10%
Film coalescence aid 0.5% 20% modified alta-mud 10%
Elastic emulsion 25% water 49%;
Base paint is mixing the assorted base paint being deployed into different colours of aqueous color paste of different colours as requested, and assorted base paint is dispersed in protecting glue system in strict accordance with proportioning and makes different look plastochondria systems.
Consisting of of described protecting glue system:
5% ~ 8% protecting glue 60% wetting agent 1.0%
4%T-935 protecting glue 39%;
Described look plastochondria system consists of:
Assorted base paint 50% protecting glue system 50%;
Consisting of of described emulsion binder:
Organosilicon crylic acid latex 66% film coalescence aid 4.2%
Propylene glycol 1.0% defoamer 1.0%
Sterilant 0.1% thickening material 0.7%
Water 27%;
The finished product of aqueous colorful building coating consists of:
Emulsion binder 35% look plastochondria system 65%;
Above per-cent is mass percent.
Wherein, Mierocrystalline cellulose can adopt nonionic cellulose; PH conditioning agent can adopt multifunctional assistant; Dispersion agent in base paint can adopt polycarboxylate sodium's dispersion agent; The protecting glue of 3.0 ~ 5.0%, it is helpful to the granulating of multi-color lacquer.Film coalescence aid can adopt alkoxide material, its chemical name: 2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrate, has splendid film forming efficiency, can be lowered into film temperature, improves the snappiness of color particle.
Elastic emulsion is synthetic resin emulsion, is formed by nucleocapsid process polymerisation, has self-crosslinking performance, and its solids content is 46.0 ~ 50.0%, and viscosity is 500 ~ 1500mPas/25 DEG C; Described defoamer adopts the mineral oil defoaming agent of waterborne general, especially plays superior froth breaking and broken bubble effect to polyacrylic ester system emulsion.
Protection rubber powder is that the synthesizing flaky silicate through modification adopted takes off soil structure-Na magnesium lithium silicates as the Chinese.Outward appearance is white powder, and specific surface area is 350 ~ 400 ㎡/g.Protecting glue is a kind of elastomerics, and particle soft or hard is adjustable, is applicable to all decorative patterns; Nontoxic, tasteless, nonirritant; Water insoluble, oil and ethanol.Soak swelling, compared with the nanogel that can form high-clarity, high viscosity, high thixotropic under low-solid content.
Organosilicon crylic acid latex can adopt commercial synthetic resin emulsion, and it is formed by methacrylate-based monomer or acrylic ester monomer and the copolymerization of the functional monomer such as vinylformic acid, organosilicon, and its solids content is 42-46.0%, and viscosity is 100-500mpa.s/25 DEG C.
Thickening material can adopt the swelling associative thickener of hydrophobically-modified alkali; Titanium dioxide adopts surface-treated modified titanium; Kaolin is calcined kaolin; Sanitas can adopt Novel industrial environment friendly corrosion protection sterilant, and as sterilant AQ, main component is BIT, and chemical name is BIT, has spectrum and the pH value scope of application widely.
The preparation method of aqueous colorful building coating:
The preparation process of base paint:
Water, Mierocrystalline cellulose, multifunctional assistant, dispersion agent, defoamer and color stuffing are added in Scattered Kettle successively according to proportioning; high speed dispersion is to fineness less than 50 μm; add under the stirring of middling speed again 3.0 ~ 5.0% protecting glue of above-mentioned mass percent, film coalescence aid, elastic emulsion, sterilant and 20% modified alta-mud; adjustment viscosity reaches 120-130k μ; can base paint be obtained, for subsequent use.
The tinting step of base paint:
The base paint of above-mentioned preparation is put into stirrer stirring at low speed, according to the chromatic pattern feature of the granite building material that will copy, modulates assorted base paint with the aqueous color paste of above-mentioned base paint and coupling.
The preparation process of protecting glue system:
Be added to the water by 5% ~ 8% protecting glue of described mass percent, high speed dispersion is dissolved completely to protecting glue, becomes complete transparent liquid, then middling speed stirring under add wetting agent and 4%T-935 protecting glue, mix completely, be protecting glue system.
The preparation process of look plastochondria system:
Assorted base paint is added in proportion in protecting glue system, according to the color grain size of design, select the square hole sieve of different order number sizes, filter and can obtain required look plastochondria system; When assorted base paint is added into after in protecting glue system, the Mierocrystalline cellulose in protecting glue system and base paint interacts, and make the gel produced be wrapped in assorted base paint surface securely, anion surface activity provides negative charge to form stable assorted look grain.
The preparation process of emulsion binder:
Water, film coalescence aid, defoamer, propylene glycol, sterilant and organosilicon crylic acid latex are joined Scattered Kettle successively by proportioning, then adds the viscosity of thickening material adjustment emulsion binder, namely obtain emulsion binder.
The preparation process of aqueous colorful building coating:
In obtained emulsion binder, add the look plastochondria system of above-mentioned mass percent, namely form stable aqueous colorful building coating.
When protecting glue mixes with water, particle undergoes rapid expansion is until slice separates.Because laminated layer wears negative charge, end face is positively charged, and the thin slice end face after separation attracted to the aspect of another thin slice, thus forms rapidly three-dimensional glue for structure, and system viscosity is increased.Its stable viscosity, nonbleeding, granulation easily, are convenient to extensive construction application thus.
Embodiment two:
Consisting of of described base paint:
Mierocrystalline cellulose 1.1% multifunctional assistant 0.2%
Dispersion agent 0.2% sterilant 0.4%
Titanium dioxide 4.0% kaolin 4.0%
Defoamer 0.4% 3.0 ~ 5.0% protecting glue 15%
Film coalescence aid 0.7% 20% modified alta-mud 15%
Elastic emulsion 30% water 29%;
Base paint is mixing the assorted base paint being deployed into different colours of aqueous color paste of different colours as requested, and assorted base paint is dispersed in protecting glue system in strict accordance with proportioning and makes different look plastochondria systems.
Consisting of of described protecting glue system:
5% ~ 8% protecting glue 62% wetting agent 1.0%
4%T-935 protecting glue 37%;
Described look plastochondria system consists of:
Assorted base paint 50% protecting glue system 50%;
Consisting of of described emulsion binder:
Organosilicon crylic acid latex 66% film coalescence aid 4.2%
Propylene glycol 1.0% defoamer 1.0%
Sterilant 0.1% thickening material 0.7%
Water 27%;
The finished product of aqueous colorful building coating consists of:
Emulsion binder 35% look plastochondria system 65%;
Above per-cent is mass percent.
Preparation method is identical with embodiment one, does not repeat them here.
Embodiment three:
Consisting of of described base paint:
Mierocrystalline cellulose 0.8% multifunctional assistant 0.1%
Dispersion agent 0.2% sterilant 0.2%
Titanium dioxide 3.0% kaolin 3.0%
Defoamer 0.2% 3.0 ~ 5.0% protecting glue 13%
Film coalescence aid 0.5% 20% modified alta-mud 13%
Elastic emulsion 25% water 41%;
Base paint is mixing the assorted base paint being deployed into different colours of aqueous color paste of different colours as requested, and assorted base paint is dispersed in protecting glue system in strict accordance with proportioning and makes different look plastochondria systems.
Consisting of of described protecting glue system:
5% ~ 8% protecting glue 64% wetting agent 1.0%
4%T-935 protecting glue 35%;
Described look plastochondria system consists of:
Assorted base paint 50% protecting glue system 50%;
Consisting of of described emulsion binder:
Organosilicon crylic acid latex 66% film coalescence aid 4.2%
Propylene glycol 1.0% defoamer 1.0%
Sterilant 0.1% thickening material 0.7%
Water 27%;
The finished product of aqueous colorful building coating consists of:
Emulsion binder 35% look plastochondria system 65%;
Above per-cent is mass percent.
Preparation method is identical with embodiment one, does not repeat them here.
Performance and the general aqueous colorful building coating of the super self-cleaning grouan building coating of the various embodiments described above uvioresistant contrast as follows, perform in strict accordance with new standard HG/T4343-2012 " aqueous colorful building coating ":
| Sequence number | Project | Embodiment one | Embodiment two | Embodiment three | General colorful building coating |
| 1 | Appearance of film | Normally | Normally | Normally | Normally |
| 2 | Water tolerance (96h) | Without exception | Without exception | Without exception | Slight whiting |
| 3 | Alkali resistance (48h) | Without exception | Without exception | Without exception | Without exception |
| 4 | Abrasion resistance/time | ﹥ 5000 | ﹥ 5000 | 4500 | 2000 |
| 5 | Package stability | Pass through | Pass through | Pass through | Viscosity becomes large, and look grain condenses |
| 6 | Cover crack ability (standard state)/mm | ＞1 | ＞1 | 0.8 | 0.6 |
| 7 | Resistance to artificial weathering | 1900h is non-foaming, does not come off, efflorescence 0, variable color 0 grade | 2500h does not steep, and does not come off, efflorescence 0 grade, variable color 0 grade | 3200h is non-foaming, does not come off, efflorescence 0 grade, variable color 0 grade | 800h is non-foaming, does not come off, efflorescence 1 grade, variable color 2 grades |
Aqueous colorful building coating provided by the present invention and prepare, is combined into granule medium and is improved look grain effect, the package stability of aqueous colorful building coating by protection rubber powder (particularly adopting the synthesizing flaky silicate containing properties-correcting agent)/Mierocrystalline cellulose protective colloid and improve the defect of aqueous colorful particle to the bleeding in external phase, muddy water.The present invention has the following advantages:
(1) good stability of look grain, resistance to bleed(ing) is strong, not muddy water;
(2) good stability of finished product paint, the not sedimentation of look grain, does not condense;
(3) energy-conserving and environment-protective take water as solvent;
(4) true to nature, the cost of imitating natural marble material effect just;
(5) disposable spray finishing is shaping, and easy construction, recoatability are good, safeguards simple.
The fundamental property index of aqueous colorful building coating of the present invention is all better than generally spending hilllock coating index, meets the standard-required of HG/T4343-2012 " aqueous colorful building coating " completely, and has certain elasticity, can make up the fine crack of body of wall.
Claims (7)
1. aqueous colorful building coating; it is characterized in that: the aqueous color paste, the mass percent that are 5 ~ 20% by mass percent are that the look plastochondria system of 60 ~ 70% and the emulsion binder of 30 ~ 40% mix, described look plastochondria system is made up of the base paint of following mass percent and protecting glue system:
Consisting of of described base paint:
Mierocrystalline cellulose 0.7 ~ 1.1% multifunctional assistant 0.1 ~ 0.2%
Dispersion agent 0.1 ~ 0.2% sterilant 0.1 ~ 0.4%
Defoamer 0.2 ~ 0.4% 3.0 ~ 5.0% protecting glue 10 ~ 15%
Film coalescence aid 0.5 ~ 1.0% 20% modified alta-muds 10 ~ 15%
Elastic emulsion 20 ~ 30% color stuffing 4.0 ~ 8.0%
Excess water;
Consisting of of described protecting glue system:
5% ~ 8% protecting glue 60 ~ 65% wetting agent 1.0 ~ 2.0%
4%T-935 protecting glue 35 ~ 40%;
Described look plastochondria system consists of:
Assorted base paint 45 ~ 50% protecting glue system 50 ~ 55%;
Consisting of of described emulsion binder:
Organosilicon crylic acid latex 60 ~ 75% film coalescence aid 4.2 ~ 5.3%
Propylene glycol 1.0 ~ 2.0% defoamer 1.0 ~ 2.0%
Sterilant 0.1 ~ 0.2% thickening material 0.3 ~ 1.0%
Excess water.
2. aqueous colorful building coating according to claim 1, is characterized in that: described Mierocrystalline cellulose is nonionic cellulose; Described wetting agent adopts anion surfactant; The described silicate compound of protection rubber powder behaviour wage reform or the wilkinite of modification.
3. aqueous colorful building coating according to claim 1, is characterized in that: described film coalescence aid is alkoxide, and described sterilant is anticorrosion and bactericidal agent AQ, and described thickening material is hydrophobically-modified alkali swelling type thickening material.
4. aqueous colorful building coating according to claim 1, is characterized in that: described elastic emulsion is synthetic resin emulsion; Described defoamer adopts mineral oil defoaming agent.
5. aqueous colorful building coating according to claim 1, is characterized in that: described color stuffing is the arbitrary proportion mixture of one or more in titanium dioxide, kaolin, coarse whiting, wollastonite.
6. aqueous colorful building coating according to claim 1, is characterized in that: the Chinese of the sheet through modification that described protection rubber powder adopts takes off soil structure-Na magnesium lithium silicates.
7. the preparation method of aqueous colorful building coating according to claim 1, is characterized in that: comprise the following steps:
1) preparation of base paint
Described water, Mierocrystalline cellulose, multifunctional assistant, dispersion agent, defoamer and color stuffing are added in Scattered Kettle successively according to proportioning, high speed dispersion is to fineness less than 50 μm, add under the stirring of middling speed again 3.0 ~ 5.0% protecting glue, film coalescence aid, elastic emulsion, sterilant and 20% modified alta-mud, adjustment viscosity reaches 120-130k μ, can obtain base paint;
2) toning of base paint
The base paint of above-mentioned preparation is put into stirrer stirring at low speed, according to the chromatic pattern feature of the granite building material that will copy, modulates assorted base paint with the aqueous color paste of above-mentioned base paint and coupling;
3) preparation of protecting glue system
Be added to the water by 5% ~ 8% protecting glue of described mass percent, high speed dispersion is dissolved completely to protecting glue, becomes complete transparent liquid, then middling speed stirring under add wetting agent and 4%T-935 protecting glue, mix completely, be protecting glue system;
4) preparation of look plastochondria system
Assorted base paint is added in protecting glue system by above-mentioned mass percent, according to the color grain size of design, selects the square hole sieve of different order number sizes, filter and can obtain required look plastochondria system;
5) preparation of emulsion binder
Described water, film coalescence aid, defoamer, propylene glycol, sterilant and organosilicon crylic acid latex are joined Scattered Kettle successively by proportioning, then adds the viscosity of thickening material adjustment emulsion binder as required, namely obtain emulsion binder;
6) preparation of aqueous colorful building coating
In obtained emulsion binder, add the look plastochondria system of above-mentioned mass percent, namely form stable aqueous colorful building coating.
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| CN104845478A (en) * | 2015-05-27 | 2015-08-19 | 浙江大学自贡创新中心 | Water-based light-emitting multicolor paint and preparation method thereof |
| CN105086713A (en) * | 2015-09-09 | 2015-11-25 | 山东秦恒科技有限公司 | Composite waterborne multi-color architectural coating and preparation method thereof |
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| CN106147467A (en) * | 2015-04-01 | 2016-11-23 | 山西亮龙涂料有限公司 | A kind of water-soluble colorful coating and preparation technology thereof |
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| CN104845478A (en) * | 2015-05-27 | 2015-08-19 | 浙江大学自贡创新中心 | Water-based light-emitting multicolor paint and preparation method thereof |
| CN105086713A (en) * | 2015-09-09 | 2015-11-25 | 山东秦恒科技有限公司 | Composite waterborne multi-color architectural coating and preparation method thereof |
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