CN106366814A - Sand-containing colorful environment-friendly coating and preparation method of same - Google Patents
Sand-containing colorful environment-friendly coating and preparation method of same Download PDFInfo
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- CN106366814A CN106366814A CN201610726195.7A CN201610726195A CN106366814A CN 106366814 A CN106366814 A CN 106366814A CN 201610726195 A CN201610726195 A CN 201610726195A CN 106366814 A CN106366814 A CN 106366814A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/29—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for multicolour effects
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention relates to a sand-containing colorful environment-friendly coating and a preparation method of the same. The coating is composed of a pigment component, a dispersion medium and varnish; the pigment component includes RO water, cellulose, a dispersant, pigments and fillers, a defoamer, a film forming additive, an emulsion, an anti-freeze agent, an inorganic protective glue solution, a pH regulator, a sterilizing agent, a first thickener, and natural colorful sands; the dispersion medium includes RO water, the film forming additive, a rheological agent, the emulsion, an organic protective glue solution, the defoamer and a coupling agent; and the varnish includes RO water, the emulsion, the pH regulator, the sterilizing agent, the defoamer, the film forming additive, the anti-freeze agent, and a second thickener. Compared with the prior art, the sand-containing colorful environment-friendly coating has good storage and construction stability, wherein a dried film of the coating is excellent in adhesion force and water resistant performance. The coating, when being used, has a good rough sense and has clear layer sense, thereby representing a texture effect of natural stone materials better.
Description
Technical field
The present invention relates to a kind of coating, especially relate to one kind containing colorful environmental protection coating material of sand mold and preparation method thereof.
Background technology
It is used natural granite to be just progressively eliminated as Discussion on architecture decoration for vertical face material, due to opening of lithotome
Adopt the peace that stone material hung by sleepiness, the destruction to natural environment for the exploitation and the pollution to environment, the natural aberration of stone material source ore deposit and steel
The factors such as full property difference, with paint pattern replace the pattern effect of natural granite by however raw.
Water-soluble colorful coating is the focus product applying to architecture inside and outside decoration paint field in recent years, and decorative effect is dashed forward
Go out, product passes through disposable spray finishing in emulsion paint or quartzy color sand paint surface, can assume multicolour decorative pattern after being dried simultaneously,
Vivid effect is true to nature, has similar to the exterior decorative effect as granite.Compare natural granite, there is very big price
Advantage, can save trimming cost, simultaneously the thin light weight of this dope layer, and construction technology is simple, safety and the feature of environmental protection and natural cladding
Stone material is compared and is all greatly improved, and is highly suitable to be applied for top-grade building thing such as office building, hotel, household, hospital and not
The decoration of alien invasion in villa etc., contributes to lifting building figure image and class.
In existing market, water-soluble colorful coating product is good lures uneven, and prior art material is no flexible, and product only plays
Decorate performance and ignore overall weather resistance, the rough sense of product is not enough, multicolor finish stereovision fuzzy is it is impossible to real embody
Stone texture effect, product stable storing degree is inadequate, easily because of gelatinizing after thickening between color point.
Content of the invention
The purpose of the present invention is exactly to overcome the defect of above-mentioned prior art presence to provide a kind of gradation sense to divide
Bright, adhesive force strong containing colorful environmental protection coating material of sand mold and preparation method thereof.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of colorful environmental protection coating material containing sand mold, is made up of pigment component, disperse medium and varnish, described pigment component bag
Include following component and weight portion content: ro water 23-40, cellulose 0.7-2.0, dispersant 0.1-0.3, color stuffing 5-15, froth breaking
Agent 0.05-0.3, coalescents 0.5-2, emulsion 15-30, antifreezing agent 0.5-1.5, inorganic protection sol solution 3-10, ph regulator
0.15-0.4, antibacterial 0.15-0.4, first thickening agent 1-5, natural colour sand 20-50；
Described disperse medium includes following component and weight portion content: ro water 20-85, coalescents 0.3-0.8, rheology
Agent 0.2-0.5, emulsion 5-10, organic protection sol solution 10-30, defoamer 0.1-0.3, inorganic protection sol solution 5-50, it is coupled
Agent 0.5-1.0；
Described varnish includes following component and weight portion content: ro water 13-40, emulsion 60-80, ph regulator 0.1-
0.3, antibacterial 0.1-0.3, defoamer 0.1-0.2, coalescents 0.6-3, antifreezing agent 0.8-1.5, second thickening agent 0.8-2.
Described organic protection sol solution is organic cellulose ether compound, fine selected from hydroxyethyl cellulose, carboxymethyl
Dimension element or one or more mixture of polyanion cellulose, described inorganic protection sol solution is lithium magnesium silicate aqueous solution.
Described cellulose is cellulose ether, and described dispersant is hydrophobic copolymer sodium salt dispersant.
Described color stuffing be selected from calcined kaolin, triple superphosphate, one kind of mica powder, Pulvis Talci or Rutile type titanium dioxide or
Multiple mixture.
Described defoamer is one or two mixture of modified polyorganosiloxane or organic-silicon-modified mineral oil, described
Coalescents are Lauryl Alcohol ester, and described antibacterial is the nitrogen thia cyclics without organic volatile.
Described emulsion is waterborne acrylic, organosilicon waterborne acrylic or waterborne polyurethane resin
One or more mixture, described coupling agent is titanate coupling agent.
Described antifreezing agent is propylene glycol, and described ph regulator is 2-amino-2-methyl-1-propanol, described rheology
Agent is silicon dioxide.
The first described thickening agent is hydroxypropyl-trimethyl ammonium chloride, and the second described thickening agent is hydrophobically modified alkali solubility
Emulsion-type thickening agent or one or more mixture of association type polyurethane thickener.
The described preparation method containing the colorful environmental protection coating material of sand mold, specifically includes following steps:
(1) prepare pigment component
Get the raw materials ready by formula, in ro water, add cellulose, stir 10-20min, control stir speed (S.S.) is 1000-
1200rpm, sequentially adds dispersant, color stuffing, after defoamer, stirs 25-35min；Sequentially add coalescents, antifreeze
Agent, emulsion, inorganic protection sol solution, ph regulator, antibacterial, natural colour sand and the first thickening agent, control stir speed (S.S.) be
800-1000rpm, stirs 5-15min, obtains final product pigment component；
(2) prepare disperse medium
Get the raw materials ready by formula, ro water sequentially adds rheological agent and coalescents, control stir speed (S.S.) is 1000-
1200rpm, stirs 5-15min；Sequentially add emulsion, organic protection sol solution, defoamer, inorganic protection sol solution and coupling
Agent, control stir speed (S.S.) is 800-1000rpm, stirs 5-15min, obtains final product disperse medium；
(3) prepare varnish
Get the raw materials ready by formula, ro water adds emulsion, control mixing speed is 500-800rpm, stirs 5-15min；Again according to
Secondary addition ph regulator, antibacterial, defoamer, antifreezing agent and coalescents, are eventually adding the second thickening agent, and mixing speed controls
For 900-1200rpm, stir 5-15min, obtain final product varnish；
(4) contain the preparation of the colorful environmental protection coating material of sand mold
The multiple different pigment component that step (1) is obtained is added separately in the disperse medium that step (2) is obtained, point
Dispersion media coats to pigment component, then pelletize, standing, finally adds the varnish that step (3) is obtained, stirs and obtain final product
Containing the colorful environmental protection coating material of sand mold, using screen cloth pelletize, time of repose is 4-8h.
Compared with prior art, the present invention preparation containing the colorful environmental protection coating material of sand mold, using disperse medium to pigment component
Coated, except adding lithium magnesium silicate class inorganic protection sol solution, the sterically hindered effect having using it in disperse medium
Should come to protect the base paint mix particles of different color together can storage-stable, be unlikely to colour mixture or even different color particle melt
It is combined into outside single color material, is also added with organic Protection glue and carrys out coordinated, organic Protection glue auxiliary increases mineral-type protection
The space steric effect of glue, provides certain lubricant effect simultaneously, provides more preferable space steric effect for pigment component, makes many
The pigment component planting color, during production and storage, will not produce showing of colour contamination between color point and color point because contacting
As, so guarantee storage stability containing the colorful environmental protection coating material of sand mold and construction stability more preferably, and the adhesive force of dry film with
The performances such as resistance to water are more excellent, and product uses process, and well, multicolor finish is well arranged for rough sense, shows natural stone well
The grain effect of material.
Existing coating, due to realizing stability requirement, with the addition of too many inorganic gel class material, often in formula
The shortcomings of lead to higher, the anti-accumulation of salt in the surface soil ability of water penetration and paint film partially crisp, simultaneously colorful color point is smaller, fidelity and moulding from
It is greatly lowered by degree, the colorful environmental protection coating material individual packages of present invention preparation, use in concrete spraying front, then and emulsion components
It is mixed into a set of finished product, sprays after mixing, this mode enhances storage stability, reaches the excellent property of paint film after construction simultaneously
Can, it is to avoid the problems referred to above；The present invention adds thickening agent hydroxypropyl-trimethyl ammonium chloride also by pigment component, using crosslinking
Reaction principle, makes the surface of pigment component form network structure, enhance stability containing the colorful environmental protection coating material of sand mold, outward appearance and
Dry film performance, makes formula containing the colorful environmental protection coating material of sand mold and technique more accurate, rigorous, reliable.
Specific embodiment
With reference to specific embodiment, the present invention is described in detail.
Embodiment 1-3 and comparative example 1
As shown in table 1, table 2, wherein, cellulose adopts cellulose ether to the dispensing of embodiment 1-3 and comparative example 1；
Dispersant is hydrophobic copolymer sodium salt dispersant；Color stuffing is calcined kaolin, triple superphosphate, mica powder, Pulvis Talci or rutile-type
Titanium dioxide；Defoamer is modified polyorganosiloxane；Coalescents are Lauryl Alcohol ester；Emulsion is waterborne acrylic；Antifreeze
Agent is propylene glycol；Ph regulator is 2-amino-2-methyl-1-propanol；Antibacterial is the nitrogen sulfur heterocyclic without organic volatile
Compound；Rheological agent is silicon dioxide；Coupling agent is titanate coupling agent；Inorganic protection sol solution is lithium magnesium silicate aqueous solution；
First thickening agent is hydroxypropyl-trimethyl ammonium chloride；Second thickening agent is hydrophobically modified alkali-soluble emulsion type thickening agent；Organic guarantor
Shield sol solution is hydroxyethyl cellulose.
Table 1 embodiment 1-3, comparative example 1 pigment component and varnish dispensing
Table 2 disperse medium dispensing
| Component | Comparative example 1 | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Ro water | 85 | 75 | 65 | 20 |
| Coalescents | 0.5 | 0.5 | 0.5 | 0.5 |
| Rheological agent | 0.5 | 0.5 | 0.5 | 0.5 |
| Emulsion | 10 | 10 | 10 | 10 |
| Organic protection sol solution | 0 | 10 | 20 | 30 |
| Defoamer | 0.2 | 0.2 | 0.2 | 0.2 |
| Inorganic protection sol solution | 5 | 5 | 5 | 40 |
| Coupling agent | 1 | 1 | 1 | 1 |
Following steps are specifically adopted to prepare:
(1) prepare pigment component
Add cellulose in ro water, stir 10-20min, controls stir speed (S.S.) is 1000-1200rpm, sequentially adds point
After powder, color stuffing, defoamer, stir 25-35min；Sequentially add coalescents, antifreezing agent, emulsion, inorganic protection peptization
Liquid, ph regulator, antibacterial, natural colour sand and the first thickening agent, control stir speed (S.S.) is 800-1000rpm, stirs 5-
15min, obtains final product pigment component；
(2) prepare disperse medium
Sequentially add rheological agent and coalescents in ro water, control stir speed (S.S.) is 1000-1200rpm, stirs 5-
15min；Sequentially add emulsion, organic protection sol solution, defoamer, inorganic protection sol solution and coupling agent, control stirring speed
Rate is 800-1000rpm, stirs 5-15min, obtains final product disperse medium；
(3) prepare varnish
Add emulsion in ro water, control mixing speed is 500-800rpm, stirs 5-15min；Sequentially add ph to adjust
Section agent, antibacterial, defoamer, antifreezing agent and coalescents, are eventually adding the second thickening agent, mixing speed is controlled to 900-
1200rpm, stirs 5-15min, obtains final product varnish；
(4) contain the preparation of the colorful environmental protection coating material of sand mold
The multiple different pigment component that step (1) is obtained is added separately in the disperse medium that step (2) is obtained, point
Dispersion media coats to pigment component, using screen cloth pelletize, standing 4-8h, finally adds the varnish that step (3) is obtained, stirring
Uniformly obtain final product environmental protection coating material colorful containing sand mold.
To above-mentioned finished product, through spraying equipment spraying, observe affecting and carrying out grading evaluation to material, Storage period is half
Year, storage stability rating result is as shown in table 3,
Table 3 stability rating result
| Embodiment title | Spraying effect is commented | Storage stability |
| Comparative example 1 | Difference | Difference |
| Embodiment 1 | Excellent | Excellent |
| Embodiment 2 | Excellent | Excellent |
| Embodiment 3 | In | In |
The product that embodiment 1 is obtained send the detection of national testing agency, and performance report is as shown in table 4.
Table 4 survey report
Pass through in disperse medium to add organic protection sol solution of different proportion, to the color molding effect put and stable storing
Property have significant impact, during without organic Protection glue, material cannot molding, color point pasty state, organic Protection glue amount is in 10-20 weight
During amount part, preferably, when reaching 30 weight portion, color point is partially hard, and whole structure starts to be deteriorated for effect；For storage stability, have
Machine Protection glue without when, material cannot molding, color point assumes pasty state；With the raising of organic Protection glue amount, to the storage of color point
There is notable help, after storing 6 months, take out material to even application, the clear simultaneously ungelatinized of color point；But adding with addition
When greatly, more than 30 weight portion, color point is complete but slightly less than normal, and partially firmly, whole structure is not good.
Embodiment 4-6
Embodiment 4-6 is identical with embodiment 1 preparation method, Ju Ti Pei Fang as illustrated in tables 5-7:
Table 5 embodiment 4-6 pigment component formula
Table 6 embodiment 4-6 disperse medium formula
Table 7 embodiment 4-6 lacquer formulation
Above-mentioned, cellulose is cellulose ether；Dispersant is hydrophobic copolymer sodium salt dispersant；Color stuffing is calcination
Kaolin, triple superphosphate, mica powder, Pulvis Talci or Rutile type titanium dioxide；Defoamer is organic-silicon-modified mineral oil；Coalescents are
Lauryl Alcohol ester；Emulsion is organosilicon waterborne acrylic；Antifreezing agent is propylene glycol；Ph regulator is 2- amino -2- first
Base -1- propanol；Antibacterial is the nitrogen thia cyclics without organic volatile；Rheological agent is silicon dioxide；Coupling agent is
Titanate coupling agent；First thickening agent is hydroxypropyl-trimethyl ammonium chloride；Second thickening agent is association type polyurethane thickener；No
Machine protection sol solution is lithium magnesium silicate aqueous solution, and organic polymer protection sol solution is carboxymethyl cellulose.
Claims (10)
1. one kind contains the colorful environmental protection coating material of sand mold it is characterised in that being made up of pigment component, disperse medium and varnish,
Described pigment component includes following component and weight portion content: ro water 23-40, cellulose 0.7-2.0, dispersant 0.1-
0.3, color stuffing 5-15, defoamer 0.05-0.3, coalescents 0.5-2, emulsion 15-30, antifreezing agent 0.5-1.5, inorganic protection
Sol solution 3-10, ph regulator 0.15-0.4, antibacterial 0.15-0.4, first thickening agent 1-5, natural colour sand 20-50；
Described disperse medium includes following component and weight portion content: ro water 20-85, coalescents 0.3-0.8, rheological agent
0.2-0.5, emulsion 5-10, organic protection sol solution 10-30, defoamer 0.1-0.3, inorganic protection sol solution 5-50, coupling agent
0.5-1.0；
Described varnish includes following component and weight portion content: ro water 13-40, emulsion 60-80, ph regulator 0.1-0.3, kills
Microbial inoculum 0.1-0.3, defoamer 0.1-0.2, coalescents 0.6-3, antifreezing agent 0.8-1.5, second thickening agent 0.8-2.
2. according to claim 1 a kind of containing the colorful environmental protection coating material of sand mold it is characterised in that described organic protection peptization
Liquid is organic cellulose ether compound, selected from one kind of hydroxyethyl cellulose, carboxymethyl cellulose or polyanion cellulose
Or multiple mixture, described inorganic protection sol solution is lithium magnesium silicate aqueous solution.
3. according to claim 1 a kind of containing the colorful environmental protection coating material of sand mold it is characterised in that described cellulose be second
Base cellulose ether, described dispersant is hydrophobic copolymer sodium salt dispersant.
4. according to claim 1 a kind of containing the colorful environmental protection coating material of sand mold it is characterised in that described color stuffing be selected from forging
Burn Kaolin, triple superphosphate, one or more mixture of mica powder, Pulvis Talci or Rutile type titanium dioxide.
5. according to claim 1 a kind of containing the colorful environmental protection coating material of sand mold it is characterised in that described defoamer be modification
One or two mixture of polysiloxanes or organic-silicon-modified mineral oil, described coalescents are Lauryl Alcohol ester, described
Antibacterial be nitrogen thia cyclics without organic volatile.
6. according to claim 1 a kind of containing the colorful environmental protection coating material of sand mold it is characterised in that described emulsion be aqueouss third
One or more mixture of olefin(e) acid system resin, organosilicon waterborne acrylic or waterborne polyurethane resin, described idol
Connection agent is titanate coupling agent.
7. according to claim 1 a kind of containing the colorful environmental protection coating material of sand mold it is characterised in that described antifreezing agent is the third two
Alcohol, described ph regulator is 2-amino-2-methyl-1-propanol, and described rheological agent is silicon dioxide.
8. according to claim 1 a kind of containing the colorful environmental protection coating material of sand mold it is characterised in that the first described thickening agent is
Hydroxypropyl-trimethyl ammonium chloride, the second described thickening agent is hydrophobically modified alkali-soluble emulsion type thickening agent or association type polyurethane
One or more mixture of thickening agent.
9. a kind of preparation method containing as claimed in claim 1 the colorful environmental protection coating material of sand mold it is characterised in that specifically include with
Lower step:
(1) prepare pigment component
Get the raw materials ready by formula, in ro water, add cellulose, stir 10-20min, control stir speed (S.S.) is 1000-1200rpm, according to
After secondary addition dispersant, color stuffing, defoamer, stir 25-35min；Sequentially add coalescents, antifreezing agent, emulsion, inorganic
Protection sol solution, ph regulator, antibacterial, natural colour sand and the first thickening agent, control stir speed (S.S.) is 800-1000rpm, stirs
Mix 5-15min, obtain final product pigment component；
(2) prepare disperse medium
Get the raw materials ready by formula, ro water sequentially adds rheological agent and coalescents, control stir speed (S.S.) is 1000-1200rpm, stirs
Mix 5-15min；Sequentially add emulsion, organic protection sol solution, defoamer, inorganic protection sol solution and coupling agent, control is stirred
Mixing speed is 800-1000rpm, stirs 5-15min, obtains final product disperse medium；
(3) prepare varnish
Get the raw materials ready by formula, ro water adds emulsion, control mixing speed is 500-800rpm, stirs 5-15min；Add successively again
Enter ph regulator, antibacterial, defoamer, antifreezing agent and coalescents, be eventually adding the second thickening agent, mixing speed is controlled to
900-1200rpm, stirs 5-15min, obtains final product varnish；
(4) contain the preparation of the colorful environmental protection coating material of sand mold
The multiple different pigment component that step (1) is obtained is added separately in the disperse medium that step (2) is obtained, and dispersion is situated between
Confrontation pigment component is coated, then pelletize, standing, finally adds the varnish that step (3) is obtained, stirs and obtain final product containing sand
The colorful environmental protection coating material of type.
10. the preparation method containing the colorful environmental protection coating material of sand mold according to claim 9 is it is characterised in that step (4) is described
Pelletize adopt screen cloth pelletize, time of described standing is 4-8h.
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| CN109735233A (en) * | 2019-01-25 | 2019-05-10 | 上海贝塔建筑科技有限公司 | A kind of coating and its preparation method and application |
| CN109796824A (en) * | 2018-12-17 | 2019-05-24 | 亚士漆(上海)有限公司 | A kind of emulation mineral varnish color grain, emulation mineral varnish and its preparation method and application |
| CN110015864A (en) * | 2018-01-09 | 2019-07-16 | 广州芬得利建筑材料有限公司 | A kind of water-base resin base gap filler |
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| CN113881302A (en) * | 2020-12-25 | 2022-01-04 | 上海磐彩环保科技股份有限公司 | Water-based 5G granite imitation coating and preparation method thereof |
| CN114015340A (en) * | 2021-12-01 | 2022-02-08 | 厦门富思特新材料科技有限公司 | Sand-in-water multicolor paint and preparation method and application thereof |
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