CN103282310B - 制备过渡金属氢氧化物的方法 - Google Patents

制备过渡金属氢氧化物的方法 Download PDF

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CN103282310B
CN103282310B CN201280004527.0A CN201280004527A CN103282310B CN 103282310 B CN103282310 B CN 103282310B CN 201280004527 A CN201280004527 A CN 201280004527A CN 103282310 B CN103282310 B CN 103282310B
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transition metal
suspension
metal hydroxide
metal hydroxides
solution
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CN103282310A (zh
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U·克里佩尔斯
S·施勒德勒
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/36—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/80—Compounds containing cobalt, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G51/82—Compounds containing cobalt, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
CN201280004527.0A 2011-01-10 2012-01-09 制备过渡金属氢氧化物的方法 Active CN103282310B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11150470.0 2011-01-10
EP11150470 2011-01-10
PCT/EP2012/050219 WO2012095381A2 (de) 2011-01-10 2012-01-09 Verfahren zur herstellung von übergangsmetallhydroxiden

Publications (2)

Publication Number Publication Date
CN103282310A CN103282310A (zh) 2013-09-04
CN103282310B true CN103282310B (zh) 2015-04-29

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Country Status (6)

Country Link
EP (1) EP2663527B1 (OSRAM)
JP (1) JP5872587B2 (OSRAM)
KR (1) KR101903362B1 (OSRAM)
CN (1) CN103282310B (OSRAM)
TW (1) TW201236978A (OSRAM)
WO (1) WO2012095381A2 (OSRAM)

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CN101998932B (zh) * 2008-04-03 2013-05-01 株式会社Lg化学 用于制备锂复合过渡金属氧化物的新前体
KR101575024B1 (ko) * 2013-02-13 2015-12-07 주식회사 엘지화학 낮은 탭 밀도를 갖는 전이금속 전구체 및 높은 입자 강도를 가진 리튬 전이금속 산화물
WO2017119451A1 (ja) 2016-01-06 2017-07-13 住友金属鉱山株式会社 非水系電解質二次電池用正極活物質前駆体、非水系電解質二次電池用正極活物質、非水系電解質二次電池用正極活物質前駆体の製造方法、非水系電解質二次電池用正極活物質の製造方法
CN108432003B (zh) 2016-01-06 2021-08-24 住友金属矿山株式会社 用于非水性电解质二次电池的正极活性物质及其前体、以及它们的制造方法
EP3281915B1 (en) 2016-08-10 2019-02-20 Umicore Precursors for lithium transition metal oxide cathode materials for rechargeable batteries
PL3642160T3 (pl) 2017-06-23 2021-06-14 Umicore Wodorotlenek niklu beta domieszkowany glinem
CN108511671B (zh) * 2018-03-12 2021-04-06 中国科学院长春应用化学研究所 一种柔性电极及其制备方法、巨能柔性即用即制储电器件
WO2019185433A1 (en) 2018-03-27 2019-10-03 Basf Se Process for precipitating a carbonate or (oxy)hydroxide
CN109354077B (zh) * 2018-10-16 2021-05-07 中伟新材料股份有限公司 一种多结晶形态的三元前驱体及其制备方法
EP3659974A1 (en) * 2018-11-27 2020-06-03 Basf Se Process for making a nickel composite hydroxide
EP3659975A1 (en) * 2018-11-28 2020-06-03 Basf Se Process for the manufacture of a nickel composite hydroxide
EP3953305A1 (en) 2019-04-10 2022-02-16 Basf Se Process for precipitating a mixed hydroxide, and cathode active materials made from such hydroxide
CN114007986A (zh) 2019-10-01 2022-02-01 巴斯夫欧洲公司 用于沉淀混合碳酸盐或混合(氧)氢氧化物的方法
KR20230051180A (ko) 2020-08-13 2023-04-17 바스프 에스이 혼합 수산화물을 침전시키기 위한 방법
ES2988547T3 (es) * 2020-10-13 2024-11-21 Basf Se Procedimiento de fabricación de (oxi)hidróxido particulado, y (oxi)hidróxido particulado y su utilización
EP4281415B1 (en) * 2021-01-20 2024-12-11 Basf Se Process for making a particulate (oxy)hydroxide

Citations (3)

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CN1798699A (zh) * 2003-05-30 2006-07-05 杰富意矿物股份有限公司 金属复合氧化物的制造方法
DE102006015538A1 (de) * 2006-03-31 2007-10-11 H. C. Starck Gmbh & Co. Kg Vorrichtung und Verfahren zur Herstellung von Verbindungen durch Fällung
DE102007039471A1 (de) * 2007-08-21 2009-02-26 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Lithium-Sekundärbatterien

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JP3092222B2 (ja) * 1991-07-08 2000-09-25 松下電器産業株式会社 水酸化ニッケル活物質およびニッケル正極とこれを用いたアルカリ蓄電池
JP3136668B2 (ja) * 1991-07-08 2001-02-19 松下電器産業株式会社 水酸化ニッケル活物質粉末およびニッケル正極とこれを用いたアルカリ蓄電池
US5700596A (en) * 1991-07-08 1997-12-23 Matsushita Electric Industrial Co., Ltd. Nickel hydroxide active material powder and nickel positive electrode and alkali storage battery using them
JP3644186B2 (ja) * 1997-03-24 2005-04-27 松下電器産業株式会社 電池構成用金属水酸化物製造装置
US6660432B2 (en) 2000-09-14 2003-12-09 Ilion Technology Corporation Lithiated oxide materials and methods of manufacture
JP4929674B2 (ja) * 2004-10-27 2012-05-09 住友化学株式会社 球状ニッケル酸リチウム粒子の製造方法および球状の複合酸化物粒子の製造方法
DE102006049107A1 (de) * 2006-10-13 2008-04-17 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in elektrochemischen Anwendungen
JP5251332B2 (ja) * 2007-07-30 2013-07-31 住友金属鉱山株式会社 非水系電解質二次電池用正極活物質およびその製造方法、並びにこれを用いた非水系電解質二次電池
JP4877660B2 (ja) * 2008-09-30 2012-02-15 株式会社Ｇｓユアサ リチウム二次電池用活物質、その製造方法及びリチウム二次電池
WO2009063838A1 (ja) * 2007-11-12 2009-05-22 Gs Yuasa Corporation リチウム二次電池用活物質、リチウム二次電池及びその製造方法
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CN1798699A (zh) * 2003-05-30 2006-07-05 杰富意矿物股份有限公司 金属复合氧化物的制造方法
DE102006015538A1 (de) * 2006-03-31 2007-10-11 H. C. Starck Gmbh & Co. Kg Vorrichtung und Verfahren zur Herstellung von Verbindungen durch Fällung
CN101415474A (zh) * 2006-03-31 2009-04-22 H.C.施塔克有限公司 通过沉淀制备化合物的设备和方法
DE102007039471A1 (de) * 2007-08-21 2009-02-26 H.C. Starck Gmbh Pulverförmige Verbindungen, Verfahren zu deren Herstellung sowie deren Verwendung in Lithium-Sekundärbatterien
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Also Published As

Publication number Publication date
TW201236978A (en) 2012-09-16
WO2012095381A3 (de) 2012-11-15
JP2014510004A (ja) 2014-04-24
EP2663527A2 (de) 2013-11-20
KR20140047577A (ko) 2014-04-22
JP5872587B2 (ja) 2016-03-01
CN103282310A (zh) 2013-09-04
WO2012095381A2 (de) 2012-07-19
EP2663527B1 (de) 2014-11-19
KR101903362B1 (ko) 2018-10-02

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