CN102666514B - 用于环氧化启动的方法 - Google Patents

用于环氧化启动的方法 Download PDF

Info

Publication number
CN102666514B
CN102666514B CN201080057763.XA CN201080057763A CN102666514B CN 102666514 B CN102666514 B CN 102666514B CN 201080057763 A CN201080057763 A CN 201080057763A CN 102666514 B CN102666514 B CN 102666514B
Authority
CN
China
Prior art keywords
temperature
moderator
catalyst
epoxidation
ethylene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201080057763.XA
Other languages
English (en)
Chinese (zh)
Other versions
CN102666514A (zh
Inventor
霍华德·萨克斯
安杰伊·罗基茨基
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Scientific Design Co Inc
Original Assignee
Scientific Design Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=44152004&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN102666514(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Scientific Design Co Inc filed Critical Scientific Design Co Inc
Publication of CN102666514A publication Critical patent/CN102666514A/zh
Application granted granted Critical
Publication of CN102666514B publication Critical patent/CN102666514B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/04—Ethylene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201080057763.XA 2009-12-17 2010-12-16 用于环氧化启动的方法 Expired - Fee Related CN102666514B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US28739309P 2009-12-17 2009-12-17
US61/287,393 2009-12-17
PCT/US2010/060769 WO2011084600A2 (en) 2009-12-17 2010-12-16 Process for epoxidation start-up

Publications (2)

Publication Number Publication Date
CN102666514A CN102666514A (zh) 2012-09-12
CN102666514B true CN102666514B (zh) 2015-11-25

Family

ID=44152004

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080057763.XA Expired - Fee Related CN102666514B (zh) 2009-12-17 2010-12-16 用于环氧化启动的方法

Country Status (13)

Country Link
US (1) US8530682B2 (enExample)
EP (2) EP2513077B1 (enExample)
JP (1) JP5946772B2 (enExample)
KR (1) KR101790254B1 (enExample)
CN (1) CN102666514B (enExample)
BR (1) BR112012014695A2 (enExample)
CA (1) CA2783604C (enExample)
IN (1) IN2012DN05178A (enExample)
MX (1) MX2012007043A (enExample)
MY (1) MY157612A (enExample)
RU (1) RU2542978C2 (enExample)
TW (1) TWI485141B (enExample)
WO (1) WO2011084600A2 (enExample)

Families Citing this family (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008141027A2 (en) 2007-05-09 2008-11-20 Shell Oil Company An epoxidation catalyst, a process for preparing the catalyst, and a process for the production of an olefin oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine
EP2513077B1 (en) * 2009-12-17 2014-06-11 Scientific Design Company Inc. Process for epoxidation start-up
US20110152073A1 (en) 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure
CA2832552C (en) 2011-04-11 2020-09-01 Dow Technology Investments Llc Process for conditioning a high efficiency ethylene oxide catalyst
KR20140106713A (ko) 2011-12-30 2014-09-03 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 형상화 연마입자 및 이의 형성방법
KR101667943B1 (ko) 2012-01-10 2016-10-20 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 복잡한 형상들을 가지는 연마 입자들 및 이의 성형 방법들
PL2852473T3 (pl) 2012-05-23 2021-06-28 Saint-Gobain Ceramics & Plastics Inc. Ukształtowane cząstki ścierne i sposoby ich formowania
KR101736085B1 (ko) 2012-10-15 2017-05-16 생-고뱅 어브레이시브즈, 인코포레이티드 특정한 형태들을 가진 연마 입자들 및 이러한 입자들을 형성하는 방법들
WO2014105770A1 (en) * 2012-12-31 2014-07-03 Scientific Design Company, Inc. Start-up process for high selectivity ethylene oxide catalysts
EP2943477B1 (en) * 2013-01-11 2018-03-07 Scientific Design Company Inc. Epoxidation process with post-conditioning step
BR112015024901B1 (pt) 2013-03-29 2022-01-18 Saint-Gobain Abrasifs Partículas abrasivas tendo formas particulares e métodos para formar essas partículas
MX2016004000A (es) 2013-09-30 2016-06-02 Saint Gobain Ceramics Particulas abrasivas moldeadas y metodos para formación de ellas.
US9221776B2 (en) 2013-12-23 2015-12-29 Scientific Design Company, Inc. Epoxidation process
JP6290428B2 (ja) 2013-12-31 2018-03-07 サンーゴバン アブレイシブズ，インコーポレイティド 成形研磨粒子を含む研磨物品
US9771507B2 (en) 2014-01-31 2017-09-26 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particle including dopant material and method of forming same
MX394114B (es) 2014-04-14 2025-03-24 Saint Gobain Ceramics Articulo abrasivo que incluye particulas abrasivas conformadas.
US9914864B2 (en) 2014-12-23 2018-03-13 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particles and method of forming same
CN107636109A (zh) 2015-03-31 2018-01-26 圣戈班磨料磨具有限公司 固定磨料制品和其形成方法
TWI634200B (zh) 2015-03-31 2018-09-01 聖高拜磨料有限公司 固定磨料物品及其形成方法
WO2016196767A1 (en) * 2015-06-02 2016-12-08 Scientific Design Company, Inc. Epoxidation process
WO2016201104A1 (en) 2015-06-11 2016-12-15 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
WO2017197006A1 (en) 2016-05-10 2017-11-16 Saint-Gobain Ceramics & Plastics, Inc. Abrasive particles and methods of forming same
US20170335155A1 (en) 2016-05-10 2017-11-23 Saint-Gobain Ceramics & Plastics, Inc. Abrasive particles and methods of forming same
US11230653B2 (en) 2016-09-29 2022-01-25 Saint-Gobain Abrasives, Inc. Fixed abrasive articles and methods of forming same
CN110035998B (zh) 2016-12-02 2024-02-20 国际壳牌研究有限公司 调节乙烯环氧化催化剂的方法和生产环氧乙烷的相关方法
US10563105B2 (en) 2017-01-31 2020-02-18 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
EP3642293A4 (en) 2017-06-21 2021-03-17 Saint-Gobain Ceramics&Plastics, Inc. PARTICULATE MATERIALS AND METHOD FOR MANUFACTURING THEREOF
US11059017B2 (en) 2017-09-15 2021-07-13 MultiPhase Solutions, Inc. Halogen selective detection gas chromatography for the on-line analysis and control of selective oxidation chemical production processes
US20210039074A1 (en) * 2018-02-07 2021-02-11 Basf Se Method for preparing a silver impregnation solution
US12129422B2 (en) 2019-12-27 2024-10-29 Saint-Gobain Ceramics & Plastics, Inc. Abrasive articles and methods of forming same
EP4081369A4 (en) 2019-12-27 2024-04-10 Saint-Gobain Ceramics & Plastics Inc. Abrasive articles and methods of forming same
EP4081370A4 (en) 2019-12-27 2024-04-24 Saint-Gobain Ceramics & Plastics Inc. ABRASIVE ARTICLES AND THEIR FORMATION PROCESSES
CN113121474A (zh) * 2019-12-30 2021-07-16 中国石油化工股份有限公司 乙烯环氧化银催化剂的开车方法
CN114057669B (zh) * 2020-07-29 2023-12-08 中国石油化工股份有限公司 一种乙烯环氧化恒温开车方法
CN114436998A (zh) * 2020-11-05 2022-05-06 中国石油化工股份有限公司 一种乙烯环氧化开车方法
CN118541241A (zh) 2021-12-30 2024-08-23 圣戈班磨料磨具有限公司 磨料制品及其形成方法
MX2024007593A (es) 2021-12-30 2024-08-20 Saint Gobain Abrasives Inc Artículos abrasivos y métodos de formación de los mismos.

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1040794A (zh) * 1988-07-25 1990-03-28 国际壳牌研究有限公司 环氧乙烷反应器的启动方法
CN1282327A (zh) * 1997-12-18 2001-01-31 阿科化学技术公司 采用以二氧化碳处理的载体上的银催化剂的环氧化方法
CN1665797A (zh) * 2002-06-28 2005-09-07 国际壳牌研究有限公司 环氧化方法的开车方法和烯烃环氧化方法
CN1860109A (zh) * 2003-09-29 2006-11-08 联合碳化化学及塑料技术公司 使用气相助催化剂系统制备烯化氧的方法
US20090082584A1 (en) * 2007-09-26 2009-03-26 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for initiating a highly selective ethylene oxide catalyst

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1170663A (en) 1967-03-22 1969-11-12 Shell Int Research Process for preparing Silver Catalysts
US3702259A (en) 1970-12-02 1972-11-07 Shell Oil Co Chemical production of metallic silver deposits
US4766105A (en) 1986-10-31 1988-08-23 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4761394A (en) 1986-10-31 1988-08-02 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4908343A (en) 1987-02-20 1990-03-13 Union Carbide Chemicals And Plastics Company Inc. Catalyst composition for oxidation of ethylene to ethylene oxide
US5057481A (en) 1987-02-20 1991-10-15 Union Carbide Chemicals And Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
EP0357292A1 (en) 1988-08-30 1990-03-07 Imperial Chemical Industries Plc Production of ethylene oxide and catalysts therefor
US5187140A (en) 1989-10-18 1993-02-16 Union Carbide Chemicals & Plastics Technology Corporation Alkylene oxide catalysts containing high silver content
US5102848A (en) 1990-09-28 1992-04-07 Union Carbide Chemicals & Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US5155242A (en) 1991-12-05 1992-10-13 Shell Oil Company Process for starting-up an ethylene oxide reactor
US5407888A (en) 1992-05-12 1995-04-18 Basf Aktiengesellschaft Silver catalyst
JP4042332B2 (ja) * 2001-02-27 2008-02-06 三菱化学株式会社 レニウム含有触媒を用いるオレフィンオキシドの製造方法
CA2491523C (en) 2002-06-28 2013-01-08 Shell Internationale Research Maatschappij B.V. A method for improving the selectivity of a catalyst and a process for the epoxidation of an olefin
KR101098051B1 (ko) * 2002-06-28 2011-12-26 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 에폭시화 방법의 개시방법, 올레핀 에폭시화 촉매 및 방법
US8791280B2 (en) 2005-08-10 2014-07-29 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for preparation of catalyst carrier and its use in catalyst preparation
JP2010527352A (ja) 2007-05-11 2010-08-12 ビリッグ，バリー，ジェイ． 酸化オレフィンプラントにおける高選択性触媒の開始
WO2009137427A2 (en) * 2008-05-07 2009-11-12 Shell Oil Company A process for the start-up of an epoxidation process, a process for the production of ethylene oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine
EP2513077B1 (en) * 2009-12-17 2014-06-11 Scientific Design Company Inc. Process for epoxidation start-up
US20110152073A1 (en) 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1040794A (zh) * 1988-07-25 1990-03-28 国际壳牌研究有限公司 环氧乙烷反应器的启动方法
CN1282327A (zh) * 1997-12-18 2001-01-31 阿科化学技术公司 采用以二氧化碳处理的载体上的银催化剂的环氧化方法
CN1665797A (zh) * 2002-06-28 2005-09-07 国际壳牌研究有限公司 环氧化方法的开车方法和烯烃环氧化方法
CN1860109A (zh) * 2003-09-29 2006-11-08 联合碳化化学及塑料技术公司 使用气相助催化剂系统制备烯化氧的方法
US20090082584A1 (en) * 2007-09-26 2009-03-26 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for initiating a highly selective ethylene oxide catalyst

Also Published As

Publication number Publication date
RU2012130065A (ru) 2014-01-27
CA2783604A1 (en) 2011-07-14
RU2542978C2 (ru) 2015-02-27
IN2012DN05178A (enExample) 2015-10-23
JP2013514387A (ja) 2013-04-25
CN102666514A (zh) 2012-09-12
MY157612A (en) 2016-06-30
WO2011084600A3 (en) 2011-11-17
US8530682B2 (en) 2013-09-10
TW201136906A (en) 2011-11-01
US20110152548A1 (en) 2011-06-23
WO2011084600A2 (en) 2011-07-14
TWI485141B (zh) 2015-05-21
JP5946772B2 (ja) 2016-07-06
MX2012007043A (es) 2012-07-20
EP2778157A1 (en) 2014-09-17
EP2513077B1 (en) 2014-06-11
KR20120106809A (ko) 2012-09-26
EP2513077A4 (en) 2013-05-22
KR101790254B1 (ko) 2017-10-26
EP2513077A2 (en) 2012-10-24
BR112012014695A2 (pt) 2015-09-15
CA2783604C (en) 2018-05-01

Similar Documents

Publication Publication Date Title
CN102666514B (zh) 用于环氧化启动的方法
TWI393712B (zh) 啟動高選擇性環氧乙烷觸媒之方法
US9096563B2 (en) Start-up process for high selectivity ethylene oxide catalysts
CN101711239B (zh) 烯烃氧化装置中高选择性催化剂的启动
CN102665898B (zh) 环氧化方法和显微结构
CN105008339B (zh) 具有后调节步骤的环氧化工艺
US8624045B2 (en) Process for olefin oxide production
CN104203931A (zh) 具有添加缓和剂的环氧化方法
CN109689633B (zh) 环氧化方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151125

Termination date: 20191216