TWI485141B - 環氧化反應的起動方法 - Google Patents

環氧化反應的起動方法 Download PDF

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Publication number
TWI485141B
TWI485141B TW099144226A TW99144226A TWI485141B TW I485141 B TWI485141 B TW I485141B TW 099144226 A TW099144226 A TW 099144226A TW 99144226 A TW99144226 A TW 99144226A TW I485141 B TWI485141 B TW I485141B
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TW
Taiwan
Prior art keywords
catalyst
ethylene
temperature
moderator
silver
Prior art date
Application number
TW099144226A
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English (en)
Chinese (zh)
Other versions
TW201136906A (en
Inventor
Howard Sachs
Andrzej Rokicki
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Scient Design Co
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Publication of TW201136906A publication Critical patent/TW201136906A/zh
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00Aliphatic unsaturated hydrocarbons
    • C07C11/02Alkenes
    • C07C11/04Ethene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D303/00Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02Compounds containing oxirane rings
    • C07D303/04Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
TW099144226A 2009-12-17 2010-12-16 環氧化反應的起動方法 TWI485141B (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US28739309P 2009-12-17 2009-12-17

Publications (2)

Publication Number Publication Date
TW201136906A TW201136906A (en) 2011-11-01
TWI485141B true TWI485141B (zh) 2015-05-21

Family

ID=44152004

Family Applications (1)

Application Number Title Priority Date Filing Date
TW099144226A TWI485141B (zh) 2009-12-17 2010-12-16 環氧化反應的起動方法

Country Status (13)

Country Link
US (1) US8530682B2 (enExample)
EP (2) EP2513077B1 (enExample)
JP (1) JP5946772B2 (enExample)
KR (1) KR101790254B1 (enExample)
CN (1) CN102666514B (enExample)
BR (1) BR112012014695A2 (enExample)
CA (1) CA2783604C (enExample)
IN (1) IN2012DN05178A (enExample)
MX (1) MX2012007043A (enExample)
MY (1) MY157612A (enExample)
RU (1) RU2542978C2 (enExample)
TW (1) TWI485141B (enExample)
WO (1) WO2011084600A2 (enExample)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI446964B (zh) 2007-05-09 2014-08-01 Shell Int Research 環氧化催化劑,製備該催化劑之方法及製備烯烴氧化物、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或烷醇胺之方法
CA2783604C (en) * 2009-12-17 2018-05-01 Scientific Design Company, Inc. Process for epoxidation start-up
US20110152073A1 (en) 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure
WO2012141942A1 (en) 2011-04-11 2012-10-18 Dow Technology Investments Llc Process for conditioning a high efficiency ethylene oxide catalyst
KR20170018102A (ko) 2011-12-30 2017-02-15 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 형상화 연마입자 및 이의 형성방법
EP3705177A1 (en) 2012-01-10 2020-09-09 Saint-Gobain Ceramics & Plastics Inc. Abrasive particles having complex shapes and methods of forming same
KR102197361B1 (ko) 2012-05-23 2021-01-05 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 형상화 연마입자들 및 이의 형성방법
FI2906392T3 (fi) 2012-10-15 2025-06-20 Saint Gobain Abrasives Inc Hiomahiukkasia, joilla on erityisiä muotoja, ja menetelmiä tällaisten hiukkasten muodostamiseksi
CN104884443B (zh) * 2012-12-31 2017-07-04 科学设计公司 用于环氧乙烷催化剂的启动方法
CN105008339B (zh) * 2013-01-11 2017-09-12 科学设计公司 具有后调节步骤的环氧化工艺
CN105073343B (zh) 2013-03-29 2017-11-03 圣戈班磨料磨具有限公司 具有特定形状的磨粒、形成这种粒子的方法及其用途
RU2643004C2 (ru) 2013-09-30 2018-01-29 Сен-Гобен Серэмикс Энд Пластикс, Инк. Формованные абразивные частицы и способы их получения
EP3087061B1 (en) * 2013-12-23 2018-04-11 Scientific Design Company Inc. Epoxidation process
MX380754B (es) 2013-12-31 2025-03-12 Saint Gobain Abrasives Inc Artículo abrasivo que incluye partículas abrasivas perfiladas.
US9771507B2 (en) 2014-01-31 2017-09-26 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particle including dopant material and method of forming same
BR112016023838A2 (pt) 2014-04-14 2017-08-15 Saint Gobain Ceramics artigo abrasivo incluindo partículas abrasivas moldadas
US9914864B2 (en) 2014-12-23 2018-03-13 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particles and method of forming same
CN107636109A (zh) 2015-03-31 2018-01-26 圣戈班磨料磨具有限公司 固定磨料制品和其形成方法
TWI634200B (zh) 2015-03-31 2018-09-01 聖高拜磨料有限公司 固定磨料物品及其形成方法
US9776169B2 (en) * 2015-06-02 2017-10-03 Scientific Design Company, Inc. Porous bodies with enhanced pore architecture
EP3307483B1 (en) 2015-06-11 2020-06-17 Saint-Gobain Ceramics&Plastics, Inc. Abrasive article including shaped abrasive particles
PL3455321T3 (pl) 2016-05-10 2022-12-12 Saint-Gobain Ceramics&Plastics, Inc. Sposób formowania cząstek ściernych
WO2017197002A1 (en) 2016-05-10 2017-11-16 Saint-Gobain Ceramics & Plastics, Inc. Abrasive particles and methods of forming same
US11230653B2 (en) 2016-09-29 2022-01-25 Saint-Gobain Abrasives, Inc. Fixed abrasive articles and methods of forming same
EP3548471B1 (en) 2016-12-02 2021-05-19 Shell Internationale Research Maatschappij B.V. Methods for conditioning an ethylene epoxidation catalyst and associated methods for the production of ethylene oxide
US10563105B2 (en) 2017-01-31 2020-02-18 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
WO2018236989A1 (en) 2017-06-21 2018-12-27 Saint-Gobain Ceramics & Plastics, Inc. Particulate materials and methods of forming same
WO2019055773A1 (en) 2017-09-15 2019-03-21 MultiPhase Solutions, Inc. GAS PHASE CHROMATOGRAPHY OF SELECTIVE HALOGEN DETECTION FOR ONLINE ANALYSIS AND CONTROL OF SELECTIVE OXIDATION CHEMICAL PRODUCTION PROCESSES
CN111655368A (zh) * 2018-02-07 2020-09-11 巴斯夫欧洲公司 制备银浸渍溶液的方法
CN114845838B (zh) 2019-12-27 2024-10-25 圣戈本陶瓷及塑料股份有限公司 磨料制品及其形成方法
KR102765343B1 (ko) 2019-12-27 2025-02-13 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. 연마 물품 및 이의 형성 방법
US12129422B2 (en) 2019-12-27 2024-10-29 Saint-Gobain Ceramics & Plastics, Inc. Abrasive articles and methods of forming same
CN113121474A (zh) * 2019-12-30 2021-07-16 中国石油化工股份有限公司 乙烯环氧化银催化剂的开车方法
CN114057669B (zh) * 2020-07-29 2023-12-08 中国石油化工股份有限公司 一种乙烯环氧化恒温开车方法
CN114436998A (zh) * 2020-11-05 2022-05-06 中国石油化工股份有限公司 一种乙烯环氧化开车方法
WO2023130052A1 (en) 2021-12-30 2023-07-06 Saint-Gobain Abrasives, Inc. Abrasive articles and methods of forming same
CA3241421A1 (en) 2021-12-30 2023-07-06 Anthony MARTONE Abrasive articles and methods of forming same
EP4457054A4 (en) 2021-12-30 2026-01-14 Saint Gobain Abrasives Inc ABRASIVE ARTICLES AND THEIR FORMATION PROCESSES

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW200521121A (en) * 2003-09-29 2005-07-01 Union Carbide Chem Plastic A process for the production of alkylene oxide using a gas-phase promoter system
TWI283242B (en) * 2002-06-28 2007-07-01 Shell Int Research A method for the start-up of an epoxidation process and a process for the epoxidation of an olefin
TW200918513A (en) * 2007-09-26 2009-05-01 Sd Lizenzverwertungsgesell Mbh Process for initiating a highly selective ethylene oxide catalyst

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1170663A (en) 1967-03-22 1969-11-12 Shell Int Research Process for preparing Silver Catalysts
US3702259A (en) 1970-12-02 1972-11-07 Shell Oil Co Chemical production of metallic silver deposits
US4766105A (en) 1986-10-31 1988-08-23 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4761394A (en) 1986-10-31 1988-08-02 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4908343A (en) 1987-02-20 1990-03-13 Union Carbide Chemicals And Plastics Company Inc. Catalyst composition for oxidation of ethylene to ethylene oxide
US5057481A (en) 1987-02-20 1991-10-15 Union Carbide Chemicals And Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US4874879A (en) * 1988-07-25 1989-10-17 Shell Oil Company Process for starting-up an ethylene oxide reactor
DE68925767T2 (de) 1988-08-30 1996-08-14 Union Carbide Corp Katalysatoren für die Herstellung von Ethylenoxid und Verfahren zur deren Herstellung
US5187140A (en) 1989-10-18 1993-02-16 Union Carbide Chemicals & Plastics Technology Corporation Alkylene oxide catalysts containing high silver content
US5102848A (en) 1990-09-28 1992-04-07 Union Carbide Chemicals & Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US5155242A (en) 1991-12-05 1992-10-13 Shell Oil Company Process for starting-up an ethylene oxide reactor
US5407888A (en) 1992-05-12 1995-04-18 Basf Aktiengesellschaft Silver catalyst
US5856534A (en) * 1997-12-18 1999-01-05 Arco Chemical Technology, L.P. Epoxidation process using supported silver catalysts treated with carbon dioxide
JP4042332B2 (ja) 2001-02-27 2008-02-06 三菱化学株式会社 レニウム含有触媒を用いるオレフィンオキシドの製造方法
AU2003243757A1 (en) 2002-06-28 2004-01-19 Shell Oil Company A method for improving the selectivity of a catalyst and a process for the epoxidation of an olefin
MX257124B (es) * 2002-06-28 2008-05-14 Shell Int Research Metodo para iniciar un proceso de epoxidacion, catalizador y proceso de epoxidacion de una olefina.
US8791280B2 (en) 2005-08-10 2014-07-29 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for preparation of catalyst carrier and its use in catalyst preparation
US7696368B2 (en) * 2007-05-11 2010-04-13 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Start-up of high selectivity catalysts in olefin oxide plants
CN102056909B (zh) * 2008-05-07 2014-03-05 国际壳牌研究有限公司 环氧化工艺的开车方法及环氧乙烷、1,2-二醇、1,2-二醇醚、1,2-碳酸酯或链烷醇胺的制备方法
CA2783604C (en) * 2009-12-17 2018-05-01 Scientific Design Company, Inc. Process for epoxidation start-up
US20110152073A1 (en) 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI283242B (en) * 2002-06-28 2007-07-01 Shell Int Research A method for the start-up of an epoxidation process and a process for the epoxidation of an olefin
TW200521121A (en) * 2003-09-29 2005-07-01 Union Carbide Chem Plastic A process for the production of alkylene oxide using a gas-phase promoter system
TW200918513A (en) * 2007-09-26 2009-05-01 Sd Lizenzverwertungsgesell Mbh Process for initiating a highly selective ethylene oxide catalyst

Also Published As

Publication number Publication date
MY157612A (en) 2016-06-30
CA2783604C (en) 2018-05-01
KR20120106809A (ko) 2012-09-26
EP2513077B1 (en) 2014-06-11
CN102666514A (zh) 2012-09-12
TW201136906A (en) 2011-11-01
EP2778157A1 (en) 2014-09-17
KR101790254B1 (ko) 2017-10-26
RU2542978C2 (ru) 2015-02-27
US8530682B2 (en) 2013-09-10
CA2783604A1 (en) 2011-07-14
EP2513077A2 (en) 2012-10-24
MX2012007043A (es) 2012-07-20
JP2013514387A (ja) 2013-04-25
WO2011084600A3 (en) 2011-11-17
CN102666514B (zh) 2015-11-25
IN2012DN05178A (enExample) 2015-10-23
WO2011084600A2 (en) 2011-07-14
JP5946772B2 (ja) 2016-07-06
EP2513077A4 (en) 2013-05-22
BR112012014695A2 (pt) 2015-09-15
US20110152548A1 (en) 2011-06-23
RU2012130065A (ru) 2014-01-27

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