CA2783604C - Process for epoxidation start-up - Google Patents
Process for epoxidation start-up Download PDFInfo
- Publication number
- CA2783604C CA2783604C CA2783604A CA2783604A CA2783604C CA 2783604 C CA2783604 C CA 2783604C CA 2783604 A CA2783604 A CA 2783604A CA 2783604 A CA2783604 A CA 2783604A CA 2783604 C CA2783604 C CA 2783604C
- Authority
- CA
- Canada
- Prior art keywords
- ethylene
- temperature
- catalyst
- moderator
- epoxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C11/00—Aliphatic unsaturated hydrocarbons
- C07C11/02—Alkenes
- C07C11/04—Ethene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
- C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US28739309P | 2009-12-17 | 2009-12-17 | |
| US61/287,393 | 2009-12-17 | ||
| PCT/US2010/060769 WO2011084600A2 (en) | 2009-12-17 | 2010-12-16 | Process for epoxidation start-up |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2783604A1 CA2783604A1 (en) | 2011-07-14 |
| CA2783604C true CA2783604C (en) | 2018-05-01 |
Family
ID=44152004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2783604A Expired - Fee Related CA2783604C (en) | 2009-12-17 | 2010-12-16 | Process for epoxidation start-up |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US8530682B2 (enExample) |
| EP (2) | EP2778157A1 (enExample) |
| JP (1) | JP5946772B2 (enExample) |
| KR (1) | KR101790254B1 (enExample) |
| CN (1) | CN102666514B (enExample) |
| BR (1) | BR112012014695A2 (enExample) |
| CA (1) | CA2783604C (enExample) |
| IN (1) | IN2012DN05178A (enExample) |
| MX (1) | MX2012007043A (enExample) |
| MY (1) | MY157612A (enExample) |
| RU (1) | RU2542978C2 (enExample) |
| TW (1) | TWI485141B (enExample) |
| WO (1) | WO2011084600A2 (enExample) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2685512C (en) | 2007-05-09 | 2016-12-06 | Shell Internationale Research Maatschappij B.V. | An epoxidation catalyst, a process for preparing the catalyst, and a process for the production of an olefin oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine |
| EP2778157A1 (en) * | 2009-12-17 | 2014-09-17 | Scientific Design Company Inc. | Process for epoxidation start-up |
| US20110152073A1 (en) | 2009-12-23 | 2011-06-23 | Scientific Design Company, Inc. | Epoxidation process and microstructure |
| CN103547365B (zh) | 2011-04-11 | 2016-03-16 | 陶氏技术投资有限责任公司 | 调节高效环氧乙烷催化剂的方法 |
| EP3517245B1 (en) | 2011-12-30 | 2023-12-13 | Saint-Gobain Ceramics & Plastics Inc. | Shaped abrasive particle and method of forming same |
| EP2802436B1 (en) | 2012-01-10 | 2019-09-25 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive particles having complex shapes |
| EP2852473B1 (en) | 2012-05-23 | 2020-12-23 | Saint-Gobain Ceramics & Plastics Inc. | Shaped abrasive particles and methods of forming same |
| US9440332B2 (en) | 2012-10-15 | 2016-09-13 | Saint-Gobain Abrasives, Inc. | Abrasive particles having particular shapes and methods of forming such particles |
| KR102155068B1 (ko) | 2012-12-31 | 2020-09-11 | 사이언티픽 디자인 컴파니 인코포레이티드 | 고 선택성 산화에틸렌 촉매를 위한 스타트-업 공정 |
| KR102155073B1 (ko) * | 2013-01-11 | 2020-09-11 | 사이언티픽 디자인 컴파니 인코포레이티드 | 후-컨디셔닝 단계를 이용하는 에폭시화 공정 |
| MX378491B (es) | 2013-03-29 | 2025-03-11 | Saint Gobain Abrasives Inc | Particulas abrasivas con formas particulares y metodos para elaborar las particulas. |
| US9783718B2 (en) | 2013-09-30 | 2017-10-10 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particles and methods of forming same |
| WO2015100209A1 (en) * | 2013-12-23 | 2015-07-02 | Scientific Design Company, Inc. | Epoxidation process |
| WO2015102992A1 (en) | 2013-12-31 | 2015-07-09 | Saint-Gobain Abrasives, Inc. | Abrasive article including shaped abrasive particles |
| US9771507B2 (en) | 2014-01-31 | 2017-09-26 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particle including dopant material and method of forming same |
| EP3131706B8 (en) | 2014-04-14 | 2024-01-10 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive article including shaped abrasive particles |
| US9914864B2 (en) | 2014-12-23 | 2018-03-13 | Saint-Gobain Ceramics & Plastics, Inc. | Shaped abrasive particles and method of forming same |
| EP3277459B1 (en) | 2015-03-31 | 2023-08-16 | Saint-Gobain Abrasives, Inc. | Fixed abrasive articles and methods of forming same |
| TWI634200B (zh) | 2015-03-31 | 2018-09-01 | 聖高拜磨料有限公司 | 固定磨料物品及其形成方法 |
| CN108025978B (zh) * | 2015-06-02 | 2021-08-27 | 科学设计有限公司 | 具有增强的孔结构的多孔体 |
| KR102006615B1 (ko) | 2015-06-11 | 2019-08-02 | 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 | 형상화 연마 입자들을 포함하는 연마 물품 |
| WO2017197002A1 (en) | 2016-05-10 | 2017-11-16 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive particles and methods of forming same |
| KR102481559B1 (ko) | 2016-05-10 | 2022-12-28 | 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 | 연마 입자 및 이의 형성 방법 |
| WO2018064642A1 (en) | 2016-09-29 | 2018-04-05 | Saint-Gobain Abrasives, Inc. | Fixed abrasive articles and methods of forming same |
| US11801493B2 (en) | 2016-12-02 | 2023-10-31 | Shell Usa, Inc. | Methods for conditioning an ethylene epoxidation catalyst and associated methods for the production of ethylene oxide |
| US10563105B2 (en) | 2017-01-31 | 2020-02-18 | Saint-Gobain Ceramics & Plastics, Inc. | Abrasive article including shaped abrasive particles |
| EP3642293A4 (en) | 2017-06-21 | 2021-03-17 | Saint-Gobain Ceramics&Plastics, Inc. | PARTICULATE MATERIALS AND METHOD FOR MANUFACTURING THEREOF |
| US11059017B2 (en) | 2017-09-15 | 2021-07-13 | MultiPhase Solutions, Inc. | Halogen selective detection gas chromatography for the on-line analysis and control of selective oxidation chemical production processes |
| US12629664B2 (en) * | 2018-02-07 | 2026-05-19 | Basf Se | Method for preparing a silver impregnation solution |
| KR102719159B1 (ko) | 2019-12-27 | 2024-10-21 | 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. | 연마 물품 및 이의 형성 방법 |
| CN114846112A (zh) | 2019-12-27 | 2022-08-02 | 圣戈本陶瓷及塑料股份有限公司 | 磨料制品及其形成方法 |
| KR102765343B1 (ko) | 2019-12-27 | 2025-02-13 | 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. | 연마 물품 및 이의 형성 방법 |
| CN113121474A (zh) * | 2019-12-30 | 2021-07-16 | 中国石油化工股份有限公司 | 乙烯环氧化银催化剂的开车方法 |
| CN114057669B (zh) * | 2020-07-29 | 2023-12-08 | 中国石油化工股份有限公司 | 一种乙烯环氧化恒温开车方法 |
| CN114436998A (zh) * | 2020-11-05 | 2022-05-06 | 中国石油化工股份有限公司 | 一种乙烯环氧化开车方法 |
| EP4457055A4 (en) | 2021-12-30 | 2025-12-24 | Saint Gobain Abrasives Inc | ABRASIVE ARTICLES AND THEIR FORMATION PROCESSES |
| WO2023130051A1 (en) | 2021-12-30 | 2023-07-06 | Saint-Gobain Abrasives, Inc. | Abrasive articles and methods of forming same |
| WO2023130053A1 (en) | 2021-12-30 | 2023-07-06 | Saint-Gobain Abrasives, Inc. | Abrasive articles and methods of forming same |
| US11931725B2 (en) * | 2022-07-19 | 2024-03-19 | Scientific Design Company, Inc. | Ethylene oxide high selectivity catalyst conditioning process |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1170663A (en) | 1967-03-22 | 1969-11-12 | Shell Int Research | Process for preparing Silver Catalysts |
| US3702259A (en) | 1970-12-02 | 1972-11-07 | Shell Oil Co | Chemical production of metallic silver deposits |
| US4761394A (en) | 1986-10-31 | 1988-08-02 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4766105A (en) | 1986-10-31 | 1988-08-23 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
| US4908343A (en) | 1987-02-20 | 1990-03-13 | Union Carbide Chemicals And Plastics Company Inc. | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5057481A (en) | 1987-02-20 | 1991-10-15 | Union Carbide Chemicals And Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US4874879A (en) * | 1988-07-25 | 1989-10-17 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
| EP0357293B1 (en) | 1988-08-30 | 1996-02-28 | Union Carbide Corporation | Catalysts for the production of ethylene oxide and their preparation processes |
| US5187140A (en) | 1989-10-18 | 1993-02-16 | Union Carbide Chemicals & Plastics Technology Corporation | Alkylene oxide catalysts containing high silver content |
| US5102848A (en) | 1990-09-28 | 1992-04-07 | Union Carbide Chemicals & Plastics Technology Corporation | Catalyst composition for oxidation of ethylene to ethylene oxide |
| US5155242A (en) | 1991-12-05 | 1992-10-13 | Shell Oil Company | Process for starting-up an ethylene oxide reactor |
| US5407888A (en) | 1992-05-12 | 1995-04-18 | Basf Aktiengesellschaft | Silver catalyst |
| US5856534A (en) * | 1997-12-18 | 1999-01-05 | Arco Chemical Technology, L.P. | Epoxidation process using supported silver catalysts treated with carbon dioxide |
| JP4042332B2 (ja) * | 2001-02-27 | 2008-02-06 | 三菱化学株式会社 | レニウム含有触媒を用いるオレフィンオキシドの製造方法 |
| RU2005102097A (ru) * | 2002-06-28 | 2005-08-27 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. (NL) | Способ введения в действие способа эпоксидирования и способ эпоксидирования олефина |
| BR0312244B1 (pt) | 2002-06-28 | 2013-06-25 | mÉtodo para melhorar a seletividade de um catalisador e um processo para a epoxidaÇço de uma olefina | |
| CN100376561C (zh) * | 2002-06-28 | 2008-03-26 | 国际壳牌研究有限公司 | 环氧化方法的开车方法、烯烃环氧化的催化剂和方法 |
| US7615655B2 (en) * | 2003-09-29 | 2009-11-10 | Dow Global Technologies, Inc. | Process for the production of alkylene oxide using a gas-phase promoter system |
| US8791280B2 (en) | 2005-08-10 | 2014-07-29 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for preparation of catalyst carrier and its use in catalyst preparation |
| CA2687234C (en) * | 2007-05-11 | 2016-04-19 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Start-up of high selectivity catalysts in olefin oxide plants |
| US7553980B2 (en) * | 2007-09-26 | 2009-06-30 | Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg | Process for initiating a highly selective ethylene oxide catalyst |
| WO2009137427A2 (en) * | 2008-05-07 | 2009-11-12 | Shell Oil Company | A process for the start-up of an epoxidation process, a process for the production of ethylene oxide, a 1,2-diol, a 1,2-diol ether, a 1,2-carbonate, or an alkanolamine |
| EP2778157A1 (en) * | 2009-12-17 | 2014-09-17 | Scientific Design Company Inc. | Process for epoxidation start-up |
| US20110152073A1 (en) * | 2009-12-23 | 2011-06-23 | Scientific Design Company, Inc. | Epoxidation process and microstructure |
-
2010
- 2010-12-16 EP EP20140171850 patent/EP2778157A1/en not_active Withdrawn
- 2010-12-16 CA CA2783604A patent/CA2783604C/en not_active Expired - Fee Related
- 2010-12-16 MX MX2012007043A patent/MX2012007043A/es active IP Right Grant
- 2010-12-16 BR BR112012014695A patent/BR112012014695A2/pt not_active IP Right Cessation
- 2010-12-16 RU RU2012130065/04A patent/RU2542978C2/ru not_active IP Right Cessation
- 2010-12-16 EP EP10842602.4A patent/EP2513077B1/en not_active Revoked
- 2010-12-16 WO PCT/US2010/060769 patent/WO2011084600A2/en not_active Ceased
- 2010-12-16 KR KR1020127018627A patent/KR101790254B1/ko not_active Expired - Fee Related
- 2010-12-16 IN IN5178DEN2012 patent/IN2012DN05178A/en unknown
- 2010-12-16 JP JP2012544826A patent/JP5946772B2/ja not_active Expired - Fee Related
- 2010-12-16 TW TW099144226A patent/TWI485141B/zh not_active IP Right Cessation
- 2010-12-16 MY MYPI2012002389A patent/MY157612A/en unknown
- 2010-12-16 CN CN201080057763.XA patent/CN102666514B/zh not_active Expired - Fee Related
- 2010-12-16 US US12/970,392 patent/US8530682B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| IN2012DN05178A (enExample) | 2015-10-23 |
| BR112012014695A2 (pt) | 2015-09-15 |
| MX2012007043A (es) | 2012-07-20 |
| EP2513077A2 (en) | 2012-10-24 |
| CN102666514B (zh) | 2015-11-25 |
| JP2013514387A (ja) | 2013-04-25 |
| MY157612A (en) | 2016-06-30 |
| CN102666514A (zh) | 2012-09-12 |
| WO2011084600A2 (en) | 2011-07-14 |
| KR20120106809A (ko) | 2012-09-26 |
| WO2011084600A3 (en) | 2011-11-17 |
| EP2778157A1 (en) | 2014-09-17 |
| US20110152548A1 (en) | 2011-06-23 |
| TW201136906A (en) | 2011-11-01 |
| EP2513077B1 (en) | 2014-06-11 |
| RU2542978C2 (ru) | 2015-02-27 |
| JP5946772B2 (ja) | 2016-07-06 |
| TWI485141B (zh) | 2015-05-21 |
| US8530682B2 (en) | 2013-09-10 |
| RU2012130065A (ru) | 2014-01-27 |
| EP2513077A4 (en) | 2013-05-22 |
| CA2783604A1 (en) | 2011-07-14 |
| KR101790254B1 (ko) | 2017-10-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20151113 |
|
| MKLA | Lapsed |
Effective date: 20191216 |