KR101790254B1 - 에폭시화 스타트업 방법 - Google Patents

에폭시화 스타트업 방법 Download PDF

Info

Publication number
KR101790254B1
KR101790254B1 KR1020127018627A KR20127018627A KR101790254B1 KR 101790254 B1 KR101790254 B1 KR 101790254B1 KR 1020127018627 A KR1020127018627 A KR 1020127018627A KR 20127018627 A KR20127018627 A KR 20127018627A KR 101790254 B1 KR101790254 B1 KR 101790254B1
Authority
KR
South Korea
Prior art keywords
ethylene
temperature
catalyst
volume
epoxidation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020127018627A
Other languages
English (en)
Korean (ko)
Other versions
KR20120106809A (ko
Inventor
하워드 삭스
안드르제이 로키키
Original Assignee
사이언티픽 디자인 컴파니 인코포레이티드
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=44152004&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=KR101790254(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 사이언티픽 디자인 컴파니 인코포레이티드 filed Critical 사이언티픽 디자인 컴파니 인코포레이티드
Publication of KR20120106809A publication Critical patent/KR20120106809A/ko
Application granted granted Critical
Publication of KR101790254B1 publication Critical patent/KR101790254B1/ko
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/04—Ethylene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
    • C07D303/02—Compounds containing oxirane rings
    • C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020127018627A 2009-12-17 2010-12-16 에폭시화 스타트업 방법 Expired - Fee Related KR101790254B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US28739309P 2009-12-17 2009-12-17
US61/287,393 2009-12-17
PCT/US2010/060769 WO2011084600A2 (en) 2009-12-17 2010-12-16 Process for epoxidation start-up

Publications (2)

Publication Number Publication Date
KR20120106809A KR20120106809A (ko) 2012-09-26
KR101790254B1 true KR101790254B1 (ko) 2017-10-26

Family

ID=44152004

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020127018627A Expired - Fee Related KR101790254B1 (ko) 2009-12-17 2010-12-16 에폭시화 스타트업 방법

Country Status (13)

Country Link
US (1) US8530682B2 (enExample)
EP (2) EP2778157A1 (enExample)
JP (1) JP5946772B2 (enExample)
KR (1) KR101790254B1 (enExample)
CN (1) CN102666514B (enExample)
BR (1) BR112012014695A2 (enExample)
CA (1) CA2783604C (enExample)
IN (1) IN2012DN05178A (enExample)
MX (1) MX2012007043A (enExample)
MY (1) MY157612A (enExample)
RU (1) RU2542978C2 (enExample)
TW (1) TWI485141B (enExample)
WO (1) WO2011084600A2 (enExample)

Families Citing this family (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR066468A1 (es) 2007-05-09 2009-08-19 Shell Int Research Un catalizador de epoxidacion, un proceso para preparar el mismo, y un proceso para producir un oxido de olefina , un 1,2- diol, un 1,2 - diol eter, un 1,2- carbonato, o una alcanolamina
RU2542978C2 (ru) * 2009-12-17 2015-02-27 Сайентифик Дизайн Компани, Инк. Способ запуска эпоксидирования
US20110152073A1 (en) 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure
WO2012141942A1 (en) 2011-04-11 2012-10-18 Dow Technology Investments Llc Process for conditioning a high efficiency ethylene oxide catalyst
CN104125875B (zh) 2011-12-30 2018-08-21 圣戈本陶瓷及塑料股份有限公司 成形磨粒及其形成方法
AU2013207946B2 (en) 2012-01-10 2016-07-07 Saint-Gobain Ceramics & Plastics, Inc. Abrasive particles having complex shapes and methods of forming same
KR20150020199A (ko) 2012-05-23 2015-02-25 생-고뱅 세라믹스 앤드 플라스틱스, 인코포레이티드 형상화 연마입자들 및 이의 형성방법
KR101736085B1 (ko) 2012-10-15 2017-05-16 생-고뱅 어브레이시브즈, 인코포레이티드 특정한 형태들을 가진 연마 입자들 및 이러한 입자들을 형성하는 방법들
KR102155068B1 (ko) * 2012-12-31 2020-09-11 사이언티픽 디자인 컴파니 인코포레이티드 고 선택성 산화에틸렌 촉매를 위한 스타트-업 공정
CN105008339B (zh) * 2013-01-11 2017-09-12 科学设计公司 具有后调节步骤的环氧化工艺
CA2907372C (en) 2013-03-29 2017-12-12 Saint-Gobain Abrasives, Inc. Abrasive particles having particular shapes and methods of forming such particles
JP2016538149A (ja) 2013-09-30 2016-12-08 サン−ゴバン セラミックス アンド プラスティクス，インコーポレイティド 形状化研磨粒子及び形状化研磨粒子を形成する方法
CN105980368B (zh) * 2013-12-23 2019-02-19 科学设计有限公司 环氧化方法
CN106029301B (zh) 2013-12-31 2018-09-18 圣戈班磨料磨具有限公司 包括成形磨粒的研磨制品
US9771507B2 (en) 2014-01-31 2017-09-26 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particle including dopant material and method of forming same
WO2015160854A1 (en) 2014-04-14 2015-10-22 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
US9914864B2 (en) 2014-12-23 2018-03-13 Saint-Gobain Ceramics & Plastics, Inc. Shaped abrasive particles and method of forming same
TWI634200B (zh) 2015-03-31 2018-09-01 聖高拜磨料有限公司 固定磨料物品及其形成方法
CN116967949A (zh) 2015-03-31 2023-10-31 圣戈班磨料磨具有限公司 固定磨料制品和其形成方法
WO2016196767A1 (en) * 2015-06-02 2016-12-08 Scientific Design Company, Inc. Epoxidation process
CA2988012C (en) 2015-06-11 2021-06-29 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
PL3455321T3 (pl) 2016-05-10 2022-12-12 Saint-Gobain Ceramics&Plastics, Inc. Sposób formowania cząstek ściernych
CN109462993A (zh) 2016-05-10 2019-03-12 圣戈本陶瓷及塑料股份有限公司 磨料颗粒及其形成方法
EP3519134B1 (en) 2016-09-29 2024-01-17 Saint-Gobain Abrasives, Inc. Fixed abrasive articles and methods of forming same
KR102449657B1 (ko) 2016-12-02 2022-09-29 쉘 인터내셔날 리써취 마트샤피지 비.브이. 에틸렌 에폭시화 촉매를 컨디셔닝하는 방법 및 에틸렌 옥사이드의 생산을 위한 관련된 방법
US10563105B2 (en) 2017-01-31 2020-02-18 Saint-Gobain Ceramics & Plastics, Inc. Abrasive article including shaped abrasive particles
US10865148B2 (en) 2017-06-21 2020-12-15 Saint-Gobain Ceramics & Plastics, Inc. Particulate materials and methods of forming same
US11059017B2 (en) 2017-09-15 2021-07-13 MultiPhase Solutions, Inc. Halogen selective detection gas chromatography for the on-line analysis and control of selective oxidation chemical production processes
DK3749449T3 (da) * 2018-02-07 2022-04-19 Basf Se Fremgangsmåde til fremstilling af en sølvimprægnerings-opløsning
KR102765343B1 (ko) 2019-12-27 2025-02-13 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. 연마 물품 및 이의 형성 방법
CN114845838B (zh) 2019-12-27 2024-10-25 圣戈本陶瓷及塑料股份有限公司 磨料制品及其形成方法
KR102877276B1 (ko) 2019-12-27 2025-10-28 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. 연마 물품 및 이의 형성 방법
CN113121474A (zh) * 2019-12-30 2021-07-16 中国石油化工股份有限公司 乙烯环氧化银催化剂的开车方法
CN114057669B (zh) * 2020-07-29 2023-12-08 中国石油化工股份有限公司 一种乙烯环氧化恒温开车方法
CN114436998A (zh) * 2020-11-05 2022-05-06 中国石油化工股份有限公司 一种乙烯环氧化开车方法
CN118541241A (zh) 2021-12-30 2024-08-23 圣戈班磨料磨具有限公司 磨料制品及其形成方法
MX2024007593A (es) 2021-12-30 2024-08-20 Saint Gobain Abrasives Inc Artículos abrasivos y métodos de formación de los mismos.

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002248351A (ja) 2001-02-27 2002-09-03 Mitsubishi Chemicals Corp レニウム含有触媒を用いるオレフィンオキシドの製造方法
US20070032670A1 (en) 2003-09-29 2007-02-08 Liping Zhang Process for the production of alkylene oxide using a gas-phase promoter system
WO2008140714A1 (en) 2007-05-11 2008-11-20 Billig Barry J Start-up of high selectivity catalysts in olefin oxide plants
WO2009042300A1 (en) * 2007-09-26 2009-04-02 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for initiating a highly selective ethylene oxide catalyst

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1170663A (en) * 1967-03-22 1969-11-12 Shell Int Research Process for preparing Silver Catalysts
US3702259A (en) * 1970-12-02 1972-11-07 Shell Oil Co Chemical production of metallic silver deposits
US4761394A (en) * 1986-10-31 1988-08-02 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4766105A (en) 1986-10-31 1988-08-23 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US5057481A (en) * 1987-02-20 1991-10-15 Union Carbide Chemicals And Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US4908343A (en) * 1987-02-20 1990-03-13 Union Carbide Chemicals And Plastics Company Inc. Catalyst composition for oxidation of ethylene to ethylene oxide
US4874879A (en) * 1988-07-25 1989-10-17 Shell Oil Company Process for starting-up an ethylene oxide reactor
DE68925767T2 (de) 1988-08-30 1996-08-14 Union Carbide Corp Katalysatoren für die Herstellung von Ethylenoxid und Verfahren zur deren Herstellung
US5187140A (en) * 1989-10-18 1993-02-16 Union Carbide Chemicals & Plastics Technology Corporation Alkylene oxide catalysts containing high silver content
US5102848A (en) 1990-09-28 1992-04-07 Union Carbide Chemicals & Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
US5155242A (en) * 1991-12-05 1992-10-13 Shell Oil Company Process for starting-up an ethylene oxide reactor
US5407888A (en) * 1992-05-12 1995-04-18 Basf Aktiengesellschaft Silver catalyst
US5856534A (en) * 1997-12-18 1999-01-05 Arco Chemical Technology, L.P. Epoxidation process using supported silver catalysts treated with carbon dioxide
WO2004002971A1 (en) * 2002-06-28 2004-01-08 Shell Internationale Research Maatschappij B.V. A method for the start-up of an epoxidation process, a catalyst and a process for the epoxidation of an olefin
WO2004002972A2 (en) * 2002-06-28 2004-01-08 Shell Internationale Research Maatschappij B.V. A method for the start-up of an epoxidation process and a process for the epoxidation of an olefin
BR0312244B1 (pt) 2002-06-28 2013-06-25 mÉtodo para melhorar a seletividade de um catalisador e um processo para a epoxidaÇço de uma olefina
US8791280B2 (en) 2005-08-10 2014-07-29 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for preparation of catalyst carrier and its use in catalyst preparation
KR101629037B1 (ko) * 2008-05-07 2016-06-09 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 에폭시화 방법의 스타트업 방법, 산화에틸렌, 1,2-디올, 1,2-디올 에테르, 1,2-카보네이트 또는 알칸올아민의 생산방법
RU2542978C2 (ru) * 2009-12-17 2015-02-27 Сайентифик Дизайн Компани, Инк. Способ запуска эпоксидирования
US20110152073A1 (en) * 2009-12-23 2011-06-23 Scientific Design Company, Inc. Epoxidation process and microstructure

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002248351A (ja) 2001-02-27 2002-09-03 Mitsubishi Chemicals Corp レニウム含有触媒を用いるオレフィンオキシドの製造方法
US20070032670A1 (en) 2003-09-29 2007-02-08 Liping Zhang Process for the production of alkylene oxide using a gas-phase promoter system
WO2008140714A1 (en) 2007-05-11 2008-11-20 Billig Barry J Start-up of high selectivity catalysts in olefin oxide plants
WO2009042300A1 (en) * 2007-09-26 2009-04-02 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for initiating a highly selective ethylene oxide catalyst

Also Published As

Publication number Publication date
EP2513077A4 (en) 2013-05-22
MY157612A (en) 2016-06-30
JP2013514387A (ja) 2013-04-25
EP2778157A1 (en) 2014-09-17
CA2783604A1 (en) 2011-07-14
WO2011084600A2 (en) 2011-07-14
CN102666514A (zh) 2012-09-12
JP5946772B2 (ja) 2016-07-06
WO2011084600A3 (en) 2011-11-17
EP2513077A2 (en) 2012-10-24
KR20120106809A (ko) 2012-09-26
BR112012014695A2 (pt) 2015-09-15
TWI485141B (zh) 2015-05-21
RU2012130065A (ru) 2014-01-27
CA2783604C (en) 2018-05-01
CN102666514B (zh) 2015-11-25
IN2012DN05178A (enExample) 2015-10-23
RU2542978C2 (ru) 2015-02-27
TW201136906A (en) 2011-11-01
US20110152548A1 (en) 2011-06-23
US8530682B2 (en) 2013-09-10
EP2513077B1 (en) 2014-06-11
MX2012007043A (es) 2012-07-20

Similar Documents

Publication Publication Date Title
KR101790254B1 (ko) 에폭시화 스타트업 방법
KR102155068B1 (ko) 고 선택성 산화에틸렌 촉매를 위한 스타트-업 공정
CN102665898B (zh) 环氧化方法和显微结构
CN102892503B (zh) 用于制造高选择性环氧乙烷催化剂的方法
CN105008339B (zh) 具有后调节步骤的环氧化工艺
US8624045B2 (en) Process for olefin oxide production
CN104203931A (zh) 具有添加缓和剂的环氧化方法

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

D13-X000 Search requested

St.27 status event code: A-1-2-D10-D13-srh-X000

D14-X000 Search report completed

St.27 status event code: A-1-2-D10-D14-srh-X000

PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20201020

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20201020

R18 Changes to party contact information recorded

Free format text: ST27 STATUS EVENT CODE: A-5-5-R10-R18-OTH-X000 (AS PROVIDED BY THE NATIONAL OFFICE)

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000