CN102639235B - 较高级氢化硅烷的制备方法 - Google Patents
较高级氢化硅烷的制备方法 Download PDFInfo
- Publication number
- CN102639235B CN102639235B CN201080044156.XA CN201080044156A CN102639235B CN 102639235 B CN102639235 B CN 102639235B CN 201080044156 A CN201080044156 A CN 201080044156A CN 102639235 B CN102639235 B CN 102639235B
- Authority
- CN
- China
- Prior art keywords
- hydrosilanes
- carrier
- catalyst
- reaction
- rudimentary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/755—Nickel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/24—Chromium, molybdenum or tungsten
- B01J23/26—Chromium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/75—Cobalt
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/78—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with alkali- or alkaline earth metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/85—Chromium, molybdenum or tungsten
- B01J23/86—Chromium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/85—Chromium, molybdenum or tungsten
- B01J23/86—Chromium
- B01J23/868—Chromium copper and chromium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/04—Hydrides of silicon
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02365—Forming inorganic semiconducting materials on a substrate
- H01L21/02518—Deposited layers
- H01L21/02521—Materials
- H01L21/02524—Group 14 semiconducting materials
- H01L21/02532—Silicon, silicon germanium, germanium
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02365—Forming inorganic semiconducting materials on a substrate
- H01L21/02612—Formation types
- H01L21/02617—Deposition types
- H01L21/0262—Reduction or decomposition of gaseous compounds, e.g. CVD
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102009048087A DE102009048087A1 (de) | 2009-10-02 | 2009-10-02 | Verfahren zur Herstellung höherer Hydridosilane |
| DE102009048087.0 | 2009-10-02 | ||
| PCT/EP2010/061825 WO2011038977A1 (de) | 2009-10-02 | 2010-08-13 | Verfahren zur herstellung höherer hydridosilane |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102639235A CN102639235A (zh) | 2012-08-15 |
| CN102639235B true CN102639235B (zh) | 2015-06-03 |
Family
ID=43063916
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201080044156.XA Expired - Fee Related CN102639235B (zh) | 2009-10-02 | 2010-08-13 | 较高级氢化硅烷的制备方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8709369B2 (enExample) |
| EP (1) | EP2482976B1 (enExample) |
| JP (1) | JP2013506541A (enExample) |
| KR (1) | KR20120081996A (enExample) |
| CN (1) | CN102639235B (enExample) |
| DE (1) | DE102009048087A1 (enExample) |
| TW (1) | TWI495613B (enExample) |
| WO (1) | WO2011038977A1 (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8669390B2 (en) * | 2009-04-13 | 2014-03-11 | Nippon Soda Co., Ltd. | Process for production of cyclic silane compound and/or cyclic carbosilane compound |
| DE102010040231A1 (de) | 2010-09-03 | 2012-03-08 | Evonik Degussa Gmbh | p-Dotierte Siliciumschichten |
| DE102010041842A1 (de) | 2010-10-01 | 2012-04-05 | Evonik Degussa Gmbh | Verfahren zur Herstellung höherer Hydridosilanverbindungen |
| DE102010062984A1 (de) | 2010-12-14 | 2012-06-14 | Evonik Degussa Gmbh | Verfahren zur Herstellung höherer Halogen- und Hydridosilane |
| DE102010063823A1 (de) | 2010-12-22 | 2012-06-28 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Hydridosilanen |
| CN105658330B (zh) * | 2013-10-21 | 2017-07-11 | 三井化学株式会社 | 高级硅烷的制造催化剂及高级硅烷的制造方法 |
| KR101970138B1 (ko) | 2014-08-20 | 2019-04-18 | 쇼와 덴코 가부시키가이샤 | 올리고실란의 제조 방법 |
| KR102164914B1 (ko) | 2016-06-10 | 2020-10-13 | 쇼와 덴코 가부시키가이샤 | 올리고실란의 제조 방법 |
| WO2018056250A1 (ja) | 2016-09-23 | 2018-03-29 | 昭和電工株式会社 | オリゴシランの製造方法 |
| WO2018079484A1 (ja) | 2016-10-27 | 2018-05-03 | 昭和電工株式会社 | オリゴシランの製造方法及びオリゴシランの製造装置 |
| US11401166B2 (en) * | 2018-10-11 | 2022-08-02 | L'Air Liaquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Process for producing isomer enriched higher silanes |
| US11097953B2 (en) | 2018-10-11 | 2021-08-24 | L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Process for producing liquid polysilanes and isomer enriched higher silanes |
| US11230474B2 (en) * | 2018-10-11 | 2022-01-25 | L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Process for producing isomer enriched higher silanes |
| US10752507B2 (en) * | 2018-10-11 | 2020-08-25 | L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Process for producing liquid polysilanes and isomer enriched higher silanes |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5700400A (en) * | 1993-06-15 | 1997-12-23 | Nippon Oil Co., Ltd. | Method for producing a semiconducting material |
| US6027705A (en) * | 1998-01-08 | 2000-02-22 | Showa Denko K.K. | Method for producing a higher silane |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2077710B (en) | 1980-06-11 | 1983-10-12 | Nat Res Dev | Synthesising a polysilane |
| DE3886891T2 (de) * | 1987-10-09 | 1994-06-16 | Mitsui Petrochemical Ind | Verfahren zur Herstellung von Polysilanverbindungen. |
| JPH02184513A (ja) | 1989-01-11 | 1990-07-19 | Tonen Sekiyukagaku Kk | ジシランおよびトリシランの製造方法 |
| JPH03183613A (ja) * | 1989-12-08 | 1991-08-09 | Showa Denko Kk | ジシランの製造法 |
| US4965386A (en) | 1990-03-26 | 1990-10-23 | E. I. Du Pont De Nemours And Company | Hydrosilation, and dehydrocondensation of silicon hydrides, catalyzed by scandium, yttrium and rare earth metal compounds |
| US5252766A (en) | 1990-09-14 | 1993-10-12 | Director-General Of Agency Of Industrial Science | Method for producing polysilanes |
| JP3621131B2 (ja) * | 1993-06-15 | 2005-02-16 | 新日本石油株式会社 | 半導体材料の製造法 |
| JP3183613B2 (ja) | 1994-09-20 | 2001-07-09 | カルソニックカンセイ株式会社 | 一体型熱交換器用タンク |
| JPH11260729A (ja) * | 1998-01-08 | 1999-09-24 | Showa Denko Kk | 高次シランの製造法 |
| DE60038931D1 (de) | 1999-03-30 | 2008-07-03 | Seiko Epson Corp | Verfahren zur Herstellung einer Siliziumschicht und Tintenstrahlzusammensetzung für Tintenstrahldrucker |
| KR100627203B1 (ko) | 2001-08-14 | 2006-09-22 | 제이에스알 가부시끼가이샤 | 실란 조성물, 실리콘막의 형성법 및 태양 전지의 제조법 |
| US8163261B2 (en) * | 2005-04-05 | 2012-04-24 | Voltaix, Llc | System and method for making Si2H6 and higher silanes |
| DE102007023762A1 (de) | 2006-08-10 | 2008-02-14 | Evonik Degussa Gmbh | Anlage und Verfahren zur kontinuierlichen industriellen Herstellung von 3-Glycidyloxypropylalkoxysilanen |
| DE102007023759A1 (de) | 2006-08-10 | 2008-02-14 | Evonik Degussa Gmbh | Anlage und Verfahren zur kontinuierlichen industriellen Herstellung von Fluoralkylchlorsilan |
| DE102007023763A1 (de) | 2006-08-10 | 2008-02-14 | Evonik Degussa Gmbh | Anlage, Reaktor und Verfahren zur kontinuierlichen industriellen Herstellung von Polyetheralkylalkoxysilanen |
| DE102007023760A1 (de) | 2006-08-10 | 2008-02-14 | Evonik Degussa Gmbh | Anlage, Reaktor und Verfahren zur kontinuierlichen industriellen Herstellung von 3-Methacryloxypropylalkoxysilanen |
| DE102007007185A1 (de) | 2007-02-09 | 2008-08-14 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Glycidyloxyalkyltrialkoxysilanen |
| DE102007014107A1 (de) | 2007-03-21 | 2008-09-25 | Evonik Degussa Gmbh | Aufarbeitung borhaltiger Chlorsilanströme |
| EP2135844A1 (de) | 2008-06-17 | 2009-12-23 | Evonik Degussa GmbH | Verfahren zur Herstellung höherer Hydridosilane |
| DE102008043422B3 (de) | 2008-11-03 | 2010-01-07 | Evonik Degussa Gmbh | Verfahren zur Aufreinigung niedermolekularer Hydridosilane |
| DE102009002758A1 (de) | 2009-04-30 | 2010-11-11 | Evonik Degussa Gmbh | Bandgap Tailoring von Solarzellen aus Flüssigsilan mittels Germanium-Zugabe |
| DE102009053804B3 (de) | 2009-11-18 | 2011-03-17 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Hydridosilanen |
| DE102010000979A1 (de) | 2010-01-18 | 2011-07-21 | Evonik Degussa GmbH, 45128 | Verwendung eines druckbetriebenen keramischen Wärmetauschers als integraler Bestandteil einer Anlage zur Umsetzung von Siliciumtetrachlorid zu Trichlorsilan |
| DE102010000978A1 (de) | 2010-01-18 | 2011-07-21 | Evonik Degussa GmbH, 45128 | Strömungsrohrreaktor zur Umsetzung von Siliciumtetrachlorid zu Trichlorsilan |
| DE102010000981A1 (de) | 2010-01-18 | 2011-07-21 | Evonik Degussa GmbH, 45128 | Closed loop-Verfahren zur Herstellung von Trichlorsilan aus metallurgischem Silicium |
| DE102010002405A1 (de) | 2010-02-26 | 2011-09-01 | Evonik Degussa Gmbh | Verfahren zur Oligomerisierung von Hydridosilanen, die mit dem Verfahren herstellbaren Oligomerisate und ihre Verwendung |
| DE102010040231A1 (de) | 2010-09-03 | 2012-03-08 | Evonik Degussa Gmbh | p-Dotierte Siliciumschichten |
-
2009
- 2009-10-02 DE DE102009048087A patent/DE102009048087A1/de not_active Ceased
-
2010
- 2010-08-13 WO PCT/EP2010/061825 patent/WO2011038977A1/de not_active Ceased
- 2010-08-13 CN CN201080044156.XA patent/CN102639235B/zh not_active Expired - Fee Related
- 2010-08-13 EP EP20100742002 patent/EP2482976B1/de not_active Not-in-force
- 2010-08-13 JP JP2012531295A patent/JP2013506541A/ja active Pending
- 2010-08-13 US US13/498,206 patent/US8709369B2/en not_active Expired - Fee Related
- 2010-08-13 KR KR1020127008245A patent/KR20120081996A/ko not_active Withdrawn
- 2010-09-29 TW TW099133065A patent/TWI495613B/zh not_active IP Right Cessation
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5700400A (en) * | 1993-06-15 | 1997-12-23 | Nippon Oil Co., Ltd. | Method for producing a semiconducting material |
| US6027705A (en) * | 1998-01-08 | 2000-02-22 | Showa Denko K.K. | Method for producing a higher silane |
Also Published As
| Publication number | Publication date |
|---|---|
| US20120263639A1 (en) | 2012-10-18 |
| WO2011038977A1 (de) | 2011-04-07 |
| US8709369B2 (en) | 2014-04-29 |
| KR20120081996A (ko) | 2012-07-20 |
| EP2482976B1 (de) | 2015-05-06 |
| CN102639235A (zh) | 2012-08-15 |
| DE102009048087A1 (de) | 2011-04-07 |
| JP2013506541A (ja) | 2013-02-28 |
| EP2482976A1 (de) | 2012-08-08 |
| TWI495613B (zh) | 2015-08-11 |
| TW201129502A (en) | 2011-09-01 |
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| C14 | Grant of patent or utility model | ||
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150603 Termination date: 20150813 |
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| EXPY | Termination of patent right or utility model |