CN100569509C - 一种碳纳米管阵列/层状材料复合物及其制备方法 - Google Patents
一种碳纳米管阵列/层状材料复合物及其制备方法 Download PDFInfo
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- CN100569509C CN100569509C CNB2007101189311A CN200710118931A CN100569509C CN 100569509 C CN100569509 C CN 100569509C CN B2007101189311 A CNB2007101189311 A CN B2007101189311A CN 200710118931 A CN200710118931 A CN 200710118931A CN 100569509 C CN100569509 C CN 100569509C
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- carbon nano
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- nano pipe
- laminated composite
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 181
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 146
- 239000002131 composite material Substances 0.000 title claims abstract description 67
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000003054 catalyst Substances 0.000 claims abstract description 91
- 239000000463 material Substances 0.000 claims abstract description 67
- 241000446313 Lamella Species 0.000 claims abstract description 43
- 238000000034 method Methods 0.000 claims abstract description 38
- 238000005229 chemical vapour deposition Methods 0.000 claims abstract description 27
- 150000001875 compounds Chemical class 0.000 claims abstract description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 50
- 239000010455 vermiculite Substances 0.000 claims description 31
- 229910052902 vermiculite Inorganic materials 0.000 claims description 31
- 235000019354 vermiculite Nutrition 0.000 claims description 31
- 239000007789 gas Substances 0.000 claims description 30
- 239000010445 mica Substances 0.000 claims description 30
- 229910052618 mica group Inorganic materials 0.000 claims description 30
- 238000001354 calcination Methods 0.000 claims description 26
- 229910052786 argon Inorganic materials 0.000 claims description 25
- 239000012159 carrier gas Substances 0.000 claims description 23
- 229910052751 metal Inorganic materials 0.000 claims description 23
- 239000002184 metal Substances 0.000 claims description 23
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 22
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 21
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 21
- 239000000470 constituent Substances 0.000 claims description 20
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 19
- 229910002804 graphite Inorganic materials 0.000 claims description 19
- 239000010439 graphite Substances 0.000 claims description 19
- 239000001257 hydrogen Substances 0.000 claims description 19
- 229910052739 hydrogen Inorganic materials 0.000 claims description 19
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 18
- 230000015572 biosynthetic process Effects 0.000 claims description 17
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 14
- 239000012530 fluid Substances 0.000 claims description 13
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 12
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 11
- 229910052757 nitrogen Inorganic materials 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 10
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 10
- 230000000694 effects Effects 0.000 claims description 9
- 239000000395 magnesium oxide Substances 0.000 claims description 9
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 9
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 9
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 8
- 239000005995 Aluminium silicate Substances 0.000 claims description 7
- 235000012211 aluminium silicate Nutrition 0.000 claims description 7
- 229910001593 boehmite Inorganic materials 0.000 claims description 7
- FAHBNUUHRFUEAI-UHFFFAOYSA-M hydroxidooxidoaluminium Chemical compound O[Al]=O FAHBNUUHRFUEAI-UHFFFAOYSA-M 0.000 claims description 7
- 229910052742 iron Inorganic materials 0.000 claims description 7
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims description 6
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 6
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000002243 precursor Substances 0.000 claims description 6
- 239000001307 helium Substances 0.000 claims description 5
- 229910052734 helium Inorganic materials 0.000 claims description 5
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 5
- 238000005470 impregnation Methods 0.000 claims description 5
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 3
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims description 3
- 229910002651 NO3 Inorganic materials 0.000 claims description 3
- 239000001273 butane Substances 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- -1 imvite Substances 0.000 claims description 3
- 229910052750 molybdenum Inorganic materials 0.000 claims description 3
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- NHNBFGGVMKEFGY-UHFFFAOYSA-N nitrate group Chemical group [N+](=O)([O-])[O-] NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 3
- 239000001294 propane Substances 0.000 claims description 3
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 3
- 229910052721 tungsten Inorganic materials 0.000 claims description 3
- 239000002041 carbon nanotube Substances 0.000 abstract description 23
- 229910021393 carbon nanotube Inorganic materials 0.000 abstract description 21
- 238000010923 batch production Methods 0.000 abstract description 2
- 239000012298 atmosphere Substances 0.000 description 32
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 21
- 239000008367 deionised water Substances 0.000 description 12
- 229910021641 deionized water Inorganic materials 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 239000012299 nitrogen atmosphere Substances 0.000 description 8
- 238000001816 cooling Methods 0.000 description 7
- 239000012265 solid product Substances 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- 230000005540 biological transmission Effects 0.000 description 5
- 239000012071 phase Substances 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 230000003197 catalytic effect Effects 0.000 description 3
- 239000003345 natural gas Substances 0.000 description 3
- 238000005554 pickling Methods 0.000 description 3
- 239000005977 Ethylene Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000011157 advanced composite material Substances 0.000 description 2
- 150000001721 carbon Chemical group 0.000 description 2
- UFMZWBIQTDUYBN-UHFFFAOYSA-N cobalt dinitrate Chemical compound [Co+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O UFMZWBIQTDUYBN-UHFFFAOYSA-N 0.000 description 2
- 229910001981 cobalt nitrate Inorganic materials 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000010335 hydrothermal treatment Methods 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 239000003915 liquefied petroleum gas Substances 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000012018 catalyst precursor Substances 0.000 description 1
- 238000004523 catalytic cracking Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229910021389 graphene Inorganic materials 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 230000002687 intercalation Effects 0.000 description 1
- 238000009830 intercalation Methods 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000007777 multifunctional material Substances 0.000 description 1
- CFYGEIAZMVFFDE-UHFFFAOYSA-N neodymium(3+);trinitrate Chemical compound [Nd+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O CFYGEIAZMVFFDE-UHFFFAOYSA-N 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
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CNB2007101189311A CN100569509C (zh) | 2007-06-15 | 2007-06-15 | 一种碳纳米管阵列/层状材料复合物及其制备方法 |
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CNB2007101189311A CN100569509C (zh) | 2007-06-15 | 2007-06-15 | 一种碳纳米管阵列/层状材料复合物及其制备方法 |
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CN101073934A CN101073934A (zh) | 2007-11-21 |
CN100569509C true CN100569509C (zh) | 2009-12-16 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10226756B2 (en) * | 2011-03-18 | 2019-03-12 | Nanocyl S.A. | Catalytic composition for synthesizing carbon nanotubes |
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CN101348249B (zh) * | 2008-09-05 | 2011-03-30 | 清华大学 | 一种在颗粒内表面制备碳纳米管阵列的方法 |
CN101837949A (zh) * | 2010-05-07 | 2010-09-22 | 南昌大学 | 原位碳纳米管/纳米石墨片复合粉体及制备方法 |
CN102351556B (zh) * | 2011-06-16 | 2013-06-05 | 西北工业大学 | 稀土增韧炭/炭复合材料的制备方法 |
CN102502593B (zh) * | 2011-10-11 | 2013-07-10 | 中国石油大学(北京) | 一种石墨烯、掺杂石墨烯或石墨烯复合物的制备方法 |
CN102502580B (zh) * | 2011-10-27 | 2014-08-27 | 清华大学 | 一种碳纳米管阵列及其制备方法与在制备超级电容器中的应用 |
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KR102276423B1 (ko) * | 2014-06-10 | 2021-07-12 | 삼성전자주식회사 | 복합체, 이를 이용한 전기화학적 활물질 복합체, 이를 포함한 전극, 리튬 전지, 전계 방출 소자, 바이오센서, 반도체 소자 및 열전소자 |
CN104961464B (zh) * | 2015-06-17 | 2017-06-06 | 天津大学 | 沿厚度方向具有高回弹性和高导热系数碳基复合材料及制备方法 |
TWI576864B (zh) * | 2015-08-12 | 2017-04-01 | 台灣奈米碳素股份有限公司 | 具結構方向性之奈米碳管複合線材的製作方法 |
JP6714616B2 (ja) * | 2015-12-28 | 2020-06-24 | 日立造船株式会社 | カーボンナノチューブ接合シートおよびカーボンナノチューブ接合シートの製造方法 |
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JP7201683B2 (ja) * | 2017-07-31 | 2023-01-10 | チャンスー シーナノ テクノロジー カンパニー リミテッド | 高さが制御されたカーボンナノチューブアレイを成長させる方法 |
CN109336088A (zh) * | 2018-12-19 | 2019-02-15 | 山东斯恩特纳米材料有限公司 | 一种制备垂直阵列碳纳米管的方法 |
CN109926050A (zh) * | 2019-04-18 | 2019-06-25 | 陕西延长石油(集团)有限责任公司 | 一种碳纳米管金属共生材料的制备方法 |
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CN111530462A (zh) * | 2020-04-20 | 2020-08-14 | 无锡东恒新能源科技有限公司 | 一种合成阵列型碳纳米管催化剂及其制备方法与应用 |
CN112250059B (zh) * | 2020-11-03 | 2022-06-17 | 宁波埃氪新材料科技有限公司 | 一种新能源汽车锂离子电池导电剂用小直径碳纳米管合成方法及其制成的碳纳米管 |
CN113471530B (zh) * | 2021-07-28 | 2022-10-25 | 西安交通大学 | 一种无机粘土阵列的制备方法及应用 |
CN114220954A (zh) * | 2021-12-02 | 2022-03-22 | 中国石油大学(北京) | 电极极片及其制备方法和电池 |
CN114029047A (zh) * | 2021-12-22 | 2022-02-11 | 长沙晟天新材料有限公司 | 一种阵列碳纳米管负载催化剂的制备方法 |
CN114713227B (zh) * | 2022-03-17 | 2024-01-05 | 无锡东恒新能源科技有限公司 | 一种流化床用层状催化剂的合成方法 |
CN114976085A (zh) * | 2022-03-29 | 2022-08-30 | 广东氢发新材料科技有限公司 | 一种气相沉积碳纳米纤维网络改性石墨复合双极板及其制备方法 |
CN114632521B (zh) * | 2022-04-08 | 2023-09-08 | 湖北冠毓新材料科技有限公司 | 基于蛭石的催化剂的制备方法和碳纳米管制备方法,以及由其制备的催化剂和碳纳米管 |
CN115637158A (zh) * | 2022-12-23 | 2023-01-24 | 华北理工大学 | 一种膨胀石墨/碳纳米管复合材料及其制备方法和应用 |
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2007
- 2007-06-15 CN CNB2007101189311A patent/CN100569509C/zh active Active
Non-Patent Citations (2)
Title |
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纳米碳管的制备. 吕德义,陈万喜,徐铸德.化学通报,第10期. 2000 |
纳米碳管的制备. 吕德义,陈万喜,徐铸德.化学通报,第10期. 2000 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10226756B2 (en) * | 2011-03-18 | 2019-03-12 | Nanocyl S.A. | Catalytic composition for synthesizing carbon nanotubes |
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