CN100413839C - 从水溶液中回收有机酸的方法 - Google Patents

从水溶液中回收有机酸的方法 Download PDF

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Publication number
CN100413839C
CN100413839C CNB018090400A CN01809040A CN100413839C CN 100413839 C CN100413839 C CN 100413839C CN B018090400 A CNB018090400 A CN B018090400A CN 01809040 A CN01809040 A CN 01809040A CN 100413839 C CN100413839 C CN 100413839C
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China
Prior art keywords
acid
mother liquor
klg
reclaim
proton
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Expired - Fee Related
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CNB018090400A
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English (en)
Chinese (zh)
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CN1427813A (zh
Inventor
N·A·科林斯
M·R·舍尔顿
G·W·廷达尔
S·T·佩里
R·S·奥梅德拉
C·W·辛克
B·K·阿鲁穆加姆
J·C·胡布斯
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Eastman Chemical Co
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Eastman Chemical Co
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Publication of CN1427813A publication Critical patent/CN1427813A/zh
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00Chemistry: molecular biology and microbiology
    • Y10S435/803Physical recovery methods, e.g. chromatography, grinding
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00Chemistry: molecular biology and microbiology
    • Y10S435/8215Microorganisms
    • Y10S435/822Microorganisms using bacteria or actinomycetales
    • Y10S435/874Pseudomonas
    • Y10S435/876Pseudomonas fluorescens
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00Chemistry: molecular biology and microbiology
    • Y10S435/8215Microorganisms
    • Y10S435/822Microorganisms using bacteria or actinomycetales
    • Y10S435/886Streptomyces
    • Y10S435/896Streptomyces fradiae

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
CNB018090400A 2000-03-07 2001-03-06 从水溶液中回收有机酸的方法 Expired - Fee Related CN100413839C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/519,936 US6670505B1 (en) 2000-03-07 2000-03-07 Process for the recovery of organic acids from aqueous solutions
US09/519,936 2000-03-07

Publications (2)

Publication Number Publication Date
CN1427813A CN1427813A (zh) 2003-07-02
CN100413839C true CN100413839C (zh) 2008-08-27

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CNB018090400A Expired - Fee Related CN100413839C (zh) 2000-03-07 2001-03-06 从水溶液中回收有机酸的方法

Country Status (8)

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US (2) US6670505B1 (https=)
EP (1) EP1261574B1 (https=)
JP (1) JP2003525923A (https=)
CN (1) CN100413839C (https=)
AT (1) ATE344225T1 (https=)
BR (1) BR0109005A (https=)
DE (1) DE60124229T2 (https=)
WO (1) WO2001066508A2 (https=)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10007702A1 (de) 2000-02-19 2001-08-23 Sueddeutsche Kalkstickstoff Verfahren zur Herstellung von N-(Phosphonomethyl)glycin
DE60115019T2 (de) 2000-05-22 2006-08-03 Monsanto Technology Llc. Reaktionssysteme zur herstellung von n-(phosphonomethyl)glyzin verbindungen
WO2004056841A1 (de) * 2002-12-19 2004-07-08 Basf Aktiengesellschaft Verfahren zum extrahieren von 2-keto-l-gulonsäure (kgs) aus einem polaren, vorzugsweise wässrigen lösungsmittel
DE10308045B3 (de) * 2003-02-26 2004-06-17 Lurgi Ag Verfahren und Vorrichtung zur kontinuierlichen Gewinnung freier Weinsäure aus Kaliumhydrogentartrat enthaltenden Rohstoffen
JP4469568B2 (ja) 2003-07-09 2010-05-26 三菱化学株式会社 有機酸の製造方法
CN100575496C (zh) 2003-08-28 2009-12-30 三菱化学株式会社 产生琥珀酸的方法
EP1672067B1 (en) 2003-09-17 2015-11-11 Mitsubishi Chemical Corporation Process for producing non-amino organic acid
CN100534972C (zh) * 2003-09-30 2009-09-02 味之素株式会社 从发酵液中纯化琥珀酸的方法
EP1760143B1 (en) 2004-05-20 2012-05-16 Ajinomoto Co., Inc. Succinic acid-producing bacterium and process for producing succinic acid
CN100389075C (zh) * 2004-08-10 2008-05-21 株式会社神钢环境舒立净 排水处理方法和排水处理装置
JP2008514695A (ja) * 2004-10-01 2008-05-08 ジーイー・ヘルスケア・アクスイェ・セルスカプ ピルビン酸の製造方法
JP5088136B2 (ja) 2005-10-18 2012-12-05 味の素株式会社 コハク酸の製造方法
JP5180060B2 (ja) 2006-02-24 2013-04-10 三菱化学株式会社 有機酸生産菌及び有機酸の製造法
CN101906032A (zh) * 2010-07-14 2010-12-08 华东理工大学 回收和循环使用l-(+)-酒石酸的方法
WO2013025105A1 (en) 2011-08-16 2013-02-21 /Purac Biochem B.V. Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up
EA027342B1 (ru) * 2011-08-16 2017-07-31 Пурак Биокем Б.В. Извлечение карбоновой кислоты из ее магниевых солей путем осаждения c применением хлористо-водородной кислоты, пригодное для выделения продукта реакции из ферментативного бульона
EP3845486A1 (en) * 2011-08-16 2021-07-07 Purac Biochem B.V. Recovery of carboxylic acid from their magnesium salts by precipitation using hydrochloric acid, useful for fermentation broth work-up
CN108148027A (zh) * 2011-08-16 2018-06-12 普拉克生化公司 可用于发酵液处理的通过用盐酸沉淀从羧酸镁盐中回收羧酸的方法
US9480574B2 (en) 2013-03-14 2016-11-01 Benvenue Medical, Inc. Spinal fusion implants and devices and methods for deploying such implants
CN103450007B (zh) * 2013-09-02 2015-06-17 西安通鑫半导体辅料有限公司 一种从硅片脱胶工序产生的废乳酸中回收乳酸的方法
US9422398B2 (en) 2014-05-30 2016-08-23 Industrial Technology Research Institute Copolymer, and method for preparing a monomer used to form the copolymer
US10314605B2 (en) 2014-07-08 2019-06-11 Benvenue Medical, Inc. Apparatus and methods for disrupting intervertebral disc tissue
CN104447529B (zh) * 2014-11-25 2017-05-24 利尔化学股份有限公司 3,6‑二氯吡啶甲酸的提取纯化方法
CN104672078B (zh) * 2015-02-02 2017-05-24 江苏索普(集团)有限公司 一种羰基合成醋酸副产物提纯制丙酸的工艺
US10022243B2 (en) 2015-02-06 2018-07-17 Benvenue Medical, Inc. Graft material injector system and method
US10758286B2 (en) 2017-03-22 2020-09-01 Benvenue Medical, Inc. Minimal impact access system to disc space
WO2019148083A1 (en) 2018-01-29 2019-08-01 Benvenue Medical, Inc. Minimally invasive interbody fusion
WO2019178575A1 (en) 2018-03-16 2019-09-19 Benvenue Medical, Inc. Articulated instrumentation and methods of using the same
CN108314164B (zh) * 2018-03-27 2020-06-19 浙江大学 回收废水中钡的方法
CN108947066A (zh) * 2018-07-13 2018-12-07 宁波永顺精细化工有限公司 羧酸钡废水中羧酸及钡盐的回收方法
NZ777498A (en) * 2018-12-19 2024-11-29 Basf Se Method for separating biomass from a solution comprising biomass and at least one oligosaccharide
KR102520535B1 (ko) * 2018-12-24 2023-04-11 안형일 미네랄을 포함하는 사료 첨가 조성물
CN111943836A (zh) * 2019-05-16 2020-11-17 帝斯曼知识产权资产管理有限公司 回收2-酮-l-古洛糖酸的改进方法
CN111978202B (zh) * 2020-08-12 2022-08-05 浙江理工大学上虞工业技术研究院有限公司 可碱洗分散染料水解产物的回收方法
CN112552164B (zh) * 2020-12-08 2022-12-09 日照金禾博源生化有限公司 一种从不合格柠檬酸钠母液中提取苹果酸的工艺方法
WO2023076622A1 (en) * 2021-10-29 2023-05-04 Alliance For Sustainable Energy, Llc Process for the recovery of monopotassium glucarate and glucaric acid

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4990441A (en) * 1988-09-13 1991-02-05 Rhone-Poulenc Sante Process for separating 2-keto-L-gulonic acid from a fermented medium
US5245078A (en) * 1990-11-02 1993-09-14 Mitsubishi Kasei Corporation Process for separating an organic acid or acids from an organic acid-containing solution

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2318500A (en) * 1935-10-21 1943-05-04 Parke Davis & Co Preparation of ascorbic acid and 1-gulosone
US2421611A (en) * 1945-05-04 1947-06-03 Byron E Gray Preparation of 2-keto gulonic acid and its salts
US2421612A (en) 1945-05-04 1947-06-03 Byron E Gray Preparation of 2-keto gulonic acid and its salts
US2462251A (en) 1945-05-16 1949-02-22 Merck & Co Inc Process for preparing ascorbic acids
US2918492A (en) * 1956-08-24 1959-12-22 Miles Lab Method of preparing methyl 2-ketogluconate
US3043749A (en) * 1960-07-28 1962-07-10 Pfizer & Co C Preparation of 2-keto-l-gulonic acid
US3234105A (en) * 1962-09-20 1966-02-08 Takeda Chemical Industries Ltd Method for producing 2-keto-lgulonic acid
US3381027A (en) * 1964-04-22 1968-04-30 Hoffmann La Roche Preparation and recovery of methyl 2-ketogluconate
US4113771A (en) 1971-04-07 1978-09-12 Ethyl Corporation Process for the purification of citric acid
US4202828A (en) 1978-01-10 1980-05-13 Kawasaki Kasei Chemicals Limited Process for separation of naphthoquinone and phthalic acid
FR2421864A1 (fr) 1978-04-05 1979-11-02 Hoechst France Procede de fabrication de l'acide hydroxy-4, dimethoxy-3,5 benzoique a partir de l'acide trimethoxy-3,4,5 benzoique
US4334074A (en) 1981-02-02 1982-06-08 The Dow Chemical Company Method of recovering 3,6-dichloropicolinic acid from basic aqueous solutions of salts thereof
DE3345411A1 (de) 1983-12-15 1985-06-27 Dynamit Nobel Ag, 5210 Troisdorf Verfahren zur reindarstellung von carbonsaeuren
US4771001A (en) 1986-03-27 1988-09-13 Neurex Corp. Production of lactic acid by continuous fermentation using an inexpensive raw material and a simplified method of lactic acid purification
US5168055A (en) 1986-06-11 1992-12-01 Rathin Datta Fermentation and purification process for succinic acid
US5202476A (en) * 1988-04-29 1993-04-13 Takeda Chemical Industries, Ltd. Purification of 2-keto-L-gulonic acid
FR2648136B1 (fr) 1989-06-12 1994-06-17 Rhone Poulenc Sante Procede de preparation de l'acide ascorbique
CH678057A5 (de) 1989-06-26 1991-07-31 Enco Eng Ag Verfahren zur herstellung von natrium- oder kalium-l-ascorbat.
US5202475A (en) 1990-09-27 1993-04-13 Eastman Kodak Company Process for preparation of cyclohexanedicarboxylic acid
US5210296A (en) 1990-11-19 1993-05-11 E. I. Du Pont De Nemours And Company Recovery of lactate esters and lactic acid from fermentation broth
US5159110A (en) 1991-05-16 1992-10-27 W. R. Grace & Co.-Conn. Process for recovering n-methyliminodiacetic acid from sodium sulfate
IT1254254B (it) 1992-03-11 1995-09-14 Erregierre Ind Chim Procedimento per la preparazione di acido iodesossicolico ad elevata purezza per impiego farmaceutico
US5352825A (en) 1993-07-06 1994-10-04 Hoarmann & Reimer Corp. Recovery of organic acid salts from impure process streams by addition of bases
CA2126365C (en) 1993-07-06 1999-08-24 Steven W. Felman Recovery of citric acid from impure process streams by addition of strong acids and salts thereof
US5426219A (en) 1993-07-26 1995-06-20 A.E. Staley Manufacturing Co. Process for recovering organic acids
US5410076A (en) 1993-11-12 1995-04-25 Lever Brothers Company, Division Of Conopco, Inc. Process for the preparation of bis(amidocarboxylic acid)
US5741681A (en) 1994-12-09 1998-04-21 Mitsubishi Chemical Corporation Method for producing L-aspartic acid
US5522995A (en) 1995-02-28 1996-06-04 Cockrem; Michael C. M. Process for recovering organic acids from aqueous salt solutions
JP3976832B2 (ja) 1996-04-30 2007-09-19 ディーエスエム アイピー アセッツ ビー.ブイ. 2−ケト−l−グロン酸の単離方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4990441A (en) * 1988-09-13 1991-02-05 Rhone-Poulenc Sante Process for separating 2-keto-L-gulonic acid from a fermented medium
US5245078A (en) * 1990-11-02 1993-09-14 Mitsubishi Kasei Corporation Process for separating an organic acid or acids from an organic acid-containing solution

Also Published As

Publication number Publication date
EP1261574A2 (en) 2002-12-04
CN1427813A (zh) 2003-07-02
JP2003525923A (ja) 2003-09-02
US6670505B1 (en) 2003-12-30
US20020026077A1 (en) 2002-02-28
DE60124229D1 (de) 2006-12-14
WO2001066508A3 (en) 2002-05-02
BR0109005A (pt) 2003-06-03
DE60124229T2 (de) 2007-02-15
ATE344225T1 (de) 2006-11-15
EP1261574B1 (en) 2006-11-02
WO2001066508A2 (en) 2001-09-13

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