CH184541A - Process for the preparation of a mixture of quaternary ammonium compounds. - Google Patents

Process for the preparation of a mixture of quaternary ammonium compounds.

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Publication number
CH184541A
CH184541A CH184541DA CH184541A CH 184541 A CH184541 A CH 184541A CH 184541D A CH184541D A CH 184541DA CH 184541 A CH184541 A CH 184541A
Authority
CH
Switzerland
Prior art keywords
mixture
preparation
quaternary ammonium
ammonium compounds
water
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH184541A publication Critical patent/CH184541A/en

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Description

  

  Verfahren zur Herstellung eines Gemisches von     quaternären        Ammoniumverbindungen.       Gegenstand des Hauptpatentes ist ein  Verfahren zur Herstellung einer     quaternären          Ammoniumverbindung    durch Einwirkenlassen  von     Benzylchlorid    auf     Diäthyldodecylamin.     



  Gegenstand des vorliegenden Patentes  ist ein Verfahren zur Herstellung eines     Ge-,          misches        quaternärer        Ammoniumverbindungen.     Das Verfahren ist dadurch gekennzeichnet,  dass man auf     Dimethylbenzylamin    ein Ge  misch von     Alkylbromiden    einwirken lässt,  wie es durch Einwirkung von Bromwasser  stoff auf das Alkoholgemenge erhältlich ist,  das durch Reduktion der bei der     Verseifung     von     Fetteil    entstehenden Fettsäuren erhalten  wird.

   Die Reaktion erfolgt zweckmässig unter  Erwärmen und kann in Gegenwart eines       Verdünnemittels,    wie Wasser oder Alkohol,  durchgeführt werden. Das bei der Reaktion  entstandene Produkt bildet eine zähe, gelb  liche Masse, die in Wasser zu einer klaren,  stark schäumenden Lösung löslich ist. Es  hat netzende und desinfizierende Eigenschaf-         ten    und soll für Desinfektionszwecke Ver  wendung finden.  



  <I>Beispiel:</I>       135    Gewichtsteile.     Dimethylbenzylamin     erwärmt man 12 Stunden auf 100   unter  Rühren mit 260 Gewichtsteilen eines Ge  misches von     Alkylbromiden,    wie es beispiels  weise entsteht durch Einwirkung von Brom  wasserstoff auf das Gemenge von Alkoholen,  das durch katalytische Hydrierung der aus  natürlichen Fetten durch     Verseifung    erhält  lichen Fettsäuren gewonnen werden kann.  Nach dem Erkalten erhält man als Reak  tionsprodukt eine zähe, gelbliche Masse, die  sich klar in Wasser löst und deren     wässrige     Lösungen stark schäumen.



  Process for the preparation of a mixture of quaternary ammonium compounds. The main patent relates to a process for the preparation of a quaternary ammonium compound by allowing benzyl chloride to act on diethyldodecylamine.



  The subject of the present patent is a process for the production of a mixture of quaternary ammonium compounds. The process is characterized in that a mixture of alkyl bromides is allowed to act on dimethylbenzylamine, as can be obtained by the action of hydrogen bromide on the alcohol mixture obtained by reducing the fatty acids formed during the saponification of the fatty portion.

   The reaction is conveniently carried out with heating and can be carried out in the presence of a diluent such as water or alcohol. The product formed during the reaction forms a viscous, yellowish mass that is soluble in water to form a clear, strongly foaming solution. It has wetting and disinfecting properties and should be used for disinfection purposes.



  <I> Example: </I> 135 parts by weight. Dimethylbenzylamine is heated to 100 for 12 hours while stirring with 260 parts by weight of a mixture of alkyl bromides, such as is produced, for example, by the action of hydrogen bromide on the mixture of alcohols that can be obtained by catalytic hydrogenation of the fatty acids obtained from natural fats by saponification . After cooling, the reaction product obtained is a tough, yellowish mass which dissolves clearly in water and whose aqueous solutions foam strongly.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines Gemisches von quaternären Ammoniumverbindun.gen, da durch gekennzeichnet, dass man auf Dimethyl- benzylamin ein Gemisch von Alkylbromiden einwirken lässt, wie es durch Einwirkung von Bromwasserstoff auf das Alkoholgemenge erhältlich ist, das durch Reduktion der bei der Verseifung von Fetteil entstehenden Fett säuren erhalten wird. Das neue Produkt bildet eine zähe, gelb liche Masse, die in Wasser zu einer klaren, stark schäumenden Lösung löslich ist. Es hat desinfizierende Eigenschaften. PATENT CLAIM: A process for the preparation of a mixture of quaternary Ammoniumverbindun.gen, characterized in that a mixture of alkyl bromides is allowed to act on dimethylbenzylamine, as can be obtained by the action of hydrogen bromide on the alcohol mixture obtained by reducing the amount during the saponification of Fette part of the resulting fatty acids is obtained. The new product forms a viscous, yellowish mass that is soluble in water to form a clear, strongly foaming solution. It has disinfecting properties. UNTERANSPRUCH: Verfahren nach Patentanspruch, dadurch gekennzeichnet, dass die Reaktion unter Er wärmen ausgeführt wird. SUBCLAIM: Method according to claim, characterized in that the reaction is carried out under He warm.
CH184541D 1933-04-13 1934-04-03 Process for the preparation of a mixture of quaternary ammonium compounds. CH184541A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE184541X 1933-04-13
CH175812T 1934-04-03

Publications (1)

Publication Number Publication Date
CH184541A true CH184541A (en) 1936-05-31

Family

ID=25719753

Family Applications (1)

Application Number Title Priority Date Filing Date
CH184541D CH184541A (en) 1933-04-13 1934-04-03 Process for the preparation of a mixture of quaternary ammonium compounds.

Country Status (1)

Country Link
CH (1) CH184541A (en)

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