CA2560936C - Process for producing 5-hydroxy-4-thiomethylpyrazole compound - Google Patents

Process for producing 5-hydroxy-4-thiomethylpyrazole compound Download PDF

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Publication number
CA2560936C
CA2560936C CA2560936A CA2560936A CA2560936C CA 2560936 C CA2560936 C CA 2560936C CA 2560936 A CA2560936 A CA 2560936A CA 2560936 A CA2560936 A CA 2560936A CA 2560936 C CA2560936 C CA 2560936C
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CA
Canada
Prior art keywords
group
hydroxy
mmol
represented
reaction
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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CA2560936A
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English (en)
French (fr)
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CA2560936A1 (en
Inventor
Yukio Uchida
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ihara Chemical Industry Co Ltd
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Ihara Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Ihara Chemical Industry Co Ltd filed Critical Ihara Chemical Industry Co Ltd
Publication of CA2560936A1 publication Critical patent/CA2560936A1/en
Application granted granted Critical
Publication of CA2560936C publication Critical patent/CA2560936C/en
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Expired - Lifetime legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18One oxygen or sulfur atom
    • C07D231/20One oxygen atom attached in position 3 or 5
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/28Two oxygen or sulfur atoms
    • C07D231/30Two oxygen or sulfur atoms attached in positions 3 and 5
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D413/00Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
    • C07D413/02Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
    • C07D413/12Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA2560936A 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound Expired - Lifetime CA2560936C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2004-102963 2004-03-31
JP2004102963A JP4621939B2 (ja) 2004-03-31 2004-03-31 5−ヒドロキシ−4−チオメチルピラゾール化合物の製造方法
PCT/JP2005/006806 WO2005095352A1 (ja) 2004-03-31 2005-03-31 5-ヒドロキシ-4-チオメチルピラゾール化合物の製造方法

Publications (2)

Publication Number Publication Date
CA2560936A1 CA2560936A1 (en) 2005-10-13
CA2560936C true CA2560936C (en) 2013-01-08

Family

ID=35063690

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2560936A Expired - Lifetime CA2560936C (en) 2004-03-31 2005-03-31 Process for producing 5-hydroxy-4-thiomethylpyrazole compound

Country Status (19)

Country Link
US (1) US7488831B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
EP (1) EP1767528B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JP4621939B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
KR (1) KR101205731B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CN (1) CN1938278B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
AU (1) AU2005228017B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
BR (1) BRPI0509353B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CA (1) CA2560936C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CR (1) CR8640A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ES (1) ES2508765T3 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IL (1) IL178233A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IN (1) IN2006DE05581A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
MX (1) MX280092B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
NZ (1) NZ550143A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
PL (1) PL1767528T3 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
RU (1) RU2386619C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
TW (1) TWI357899B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
UA (1) UA83910C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
WO (1) WO2005095352A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006037945A1 (en) 2004-10-05 2006-04-13 Syngenta Limited Isoxazoline derivatives and their use as herbicides
PL1829868T3 (pl) * 2004-12-20 2015-03-31 Ihara Chemical Ind Co Sposób wytwarzania soli (4,5-dihydroizoksazol-3-ilo)tiokarboksyamidyny
JP2007031342A (ja) * 2005-07-27 2007-02-08 Ihara Chem Ind Co Ltd 5−ヒドロキシ−1−アルキルピラゾール誘導体の製造方法
WO2007094225A1 (ja) * 2006-02-14 2007-08-23 Ihara Chemical Industry Co., Ltd. 5-アルコキシ-4-ヒドロキシメチルピラゾール化合物の製造方法
EP2167464B1 (en) * 2007-05-25 2014-12-03 AbbVie Deutschland GmbH & Co KG Heterocyclic compounds as positive modulators of metabotropic glutamate receptor 2 (mglu2 receptor)
GB0916267D0 (en) 2009-09-16 2009-10-28 Syngenta Ltd Herbicidal compounds
MX2012005884A (es) * 2009-11-26 2012-06-19 Basf Se Metodo para producir sales de 4,5-dihidroisoxazol-3-tiocarboxamidi na 5,5-disustituida.
BR112012012449A2 (pt) 2009-11-26 2015-09-08 Basf Se "processo para preparar 2-isoxazolinas 5,5-dissubstituídas"
WO2011144549A1 (en) * 2010-05-20 2011-11-24 Bayer Cropscience Ag Method for manufacturing 1 - alkyl - 3 - difluormethyl - 5 - hydroxypyrazoles
CN103843198B (zh) 2011-07-29 2016-05-04 萨斯喀彻温大学 聚合物基谐振器天线
CN103387541B (zh) * 2012-05-10 2016-02-10 中国中化股份有限公司 一种取代吡唑醚类化合物的制备方法
US20180230103A1 (en) 2015-11-16 2018-08-16 Lonza Ltd Method for preparation of 1-methyl-3-(trifluoromethyl)-1h-pyrazol-5-ol
TW201835036A (zh) 2017-02-27 2018-10-01 瑞士商隆薩有限公司 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法
MX2020006837A (es) 2017-12-27 2020-09-03 Kumiai Chemical Industry Co Metodo para producir un compuesto de sal de tiocarboxamidina.
CN112135814B (zh) * 2018-05-31 2021-09-28 组合化学工业株式会社 含氟吡唑衍生物的制造方法及其中间体
AU2020319741A1 (en) 2019-07-30 2022-03-10 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone
AU2020300922C1 (en) 2019-10-31 2024-04-18 Kumiai Chemical Industry Co., Ltd. Process For Producing Herbicide And Intermediate Thereof
IL296145A (en) 2020-03-05 2022-11-01 Adama Agan Ltd A process for the preparation of pyroxasulfone and intermediates obtained in this process
CN111574511A (zh) * 2020-06-28 2020-08-25 安徽久易农业股份有限公司 一种砜吡草唑的合成方法及其应用
EP4177244A3 (en) 2020-07-10 2023-08-09 Adama Agan Ltd. Process and intermediates for the preparation of pyroxasulfone and fenoxasulfone
CN112110912B (zh) * 2020-07-31 2022-07-05 绍兴贝斯美化工股份有限公司 一种合成硫醚类中间体的方法
WO2023074828A1 (ja) 2021-10-29 2023-05-04 クミアイ化学工業株式会社 ジスルフィド化合物、ポリスルフィド化合物及びその用途
AR127776A1 (es) 2021-11-28 2024-02-28 Adama Agan Ltd Composiciones de concentrado en suspensión de alta carga
CN114716428B (zh) * 2022-05-06 2024-02-06 山东潍坊润丰化工股份有限公司 制备砜吡草唑中间体的方法
CN115850178B (zh) * 2022-12-28 2025-04-04 宁夏格瑞精细化工有限公司 一种1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的制备方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4918085A (en) * 1989-03-02 1990-04-17 Rhone-Poulenc Ag Company Pesticidal 3-cyano-5-alkoxy-1-arylpyrazoles, compositions and use
CO5221057A1 (es) * 2000-03-02 2002-11-28 Aventis Cropscience Sa Componentes y composiciones plagicidas
JP4465133B2 (ja) * 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
DE60238194D1 (de) * 2001-06-21 2010-12-16 Kumiai Chemical Industry Co Isoxazolinderivate und herbizide
RU2315758C2 (ru) * 2002-08-01 2008-01-27 Ихара Кемикал Индастри Ко., Лтд. Производные пиразола и способ их получения
UA78071C2 (en) * 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition

Also Published As

Publication number Publication date
BRPI0509353B1 (pt) 2019-01-02
BRPI0509353A (pt) 2007-09-11
BRPI0509353A8 (pt) 2017-09-19
CN1938278B (zh) 2012-12-12
EP1767528A4 (en) 2010-04-21
IL178233A0 (en) 2006-12-31
KR20070003964A (ko) 2007-01-05
TWI357899B (en) 2012-02-11
MXPA06011130A (es) 2007-01-25
RU2386619C2 (ru) 2010-04-20
CN1938278A (zh) 2007-03-28
RU2006138241A (ru) 2008-05-10
KR101205731B1 (ko) 2012-11-28
US7488831B2 (en) 2009-02-10
EP1767528A1 (en) 2007-03-28
AU2005228017B2 (en) 2010-09-30
CA2560936A1 (en) 2005-10-13
IL178233A (en) 2014-02-27
WO2005095352A1 (ja) 2005-10-13
JP2005289824A (ja) 2005-10-20
AU2005228017A1 (en) 2005-10-13
PL1767528T3 (pl) 2015-03-31
JP4621939B2 (ja) 2011-02-02
MX280092B (es) 2010-10-18
ES2508765T3 (es) 2014-10-16
NZ550143A (en) 2010-04-30
UA83910C2 (ru) 2008-08-26
EP1767528B1 (en) 2014-09-17
TW200536832A (en) 2005-11-16
CR8640A (es) 2007-08-28
IN2006DE05581A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 2007-08-31
US20070185334A1 (en) 2007-08-09

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