CA2482113A1 - Process for the purification of thiophenes - Google Patents

Process for the purification of thiophenes Download PDF

Info

Publication number
CA2482113A1
CA2482113A1 CA002482113A CA2482113A CA2482113A1 CA 2482113 A1 CA2482113 A1 CA 2482113A1 CA 002482113 A CA002482113 A CA 002482113A CA 2482113 A CA2482113 A CA 2482113A CA 2482113 A1 CA2482113 A1 CA 2482113A1
Authority
CA
Canada
Prior art keywords
thiophene
solvent
optionally substituted
general formula
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA002482113A
Other languages
English (en)
French (fr)
Inventor
Lutz Brassat
Stephan Kirchmeyer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Heraeus Deutschland GmbH and Co KG
Original Assignee
H.C. Starck GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by H.C. Starck GmbH filed Critical H.C. Starck GmbH
Publication of CA2482113A1 publication Critical patent/CA2482113A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D495/00—Heterocyclic compounds containing in the condensed system at least one hetero ring having sulfur atoms as the only ring hetero atoms
    • C07D495/02—Heterocyclic compounds containing in the condensed system at least one hetero ring having sulfur atoms as the only ring hetero atoms in which the condensed system contains two hetero rings
    • C07D495/06—Peri-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D495/00—Heterocyclic compounds containing in the condensed system at least one hetero ring having sulfur atoms as the only ring hetero atoms
    • C07D495/02—Heterocyclic compounds containing in the condensed system at least one hetero ring having sulfur atoms as the only ring hetero atoms in which the condensed system contains two hetero rings
    • C07D495/04—Ortho-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D333/00—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom
    • C07D333/02—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings
    • C07D333/04—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom
    • C07D333/06—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to the ring carbon atoms
    • C07D333/14—Radicals substituted by singly bound hetero atoms other than halogen
    • C07D333/16—Radicals substituted by singly bound hetero atoms other than halogen by oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D333/00—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom
    • C07D333/02—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings
    • C07D333/04—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom
    • C07D333/26—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D333/30—Hetero atoms other than halogen
    • C07D333/32—Oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G61/12—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule
    • C08G61/122—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from five- or six-membered heterocyclic compounds, other than imides
    • C08G61/123—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from five- or six-membered heterocyclic compounds, other than imides derived from five-membered heterocyclic compounds
    • C08G61/126—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from five- or six-membered heterocyclic compounds, other than imides derived from five-membered heterocyclic compounds with a five-membered ring containing one sulfur atom in the ring
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22—Electrodes
    • H01G11/30—Electrodes characterised by their material
    • H01G11/48—Conductive polymers
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K3/00—Apparatus or processes for manufacturing printed circuits
    • H05K3/40—Forming printed elements for providing electric connections to or between printed circuits
    • H05K3/42—Plated through-holes or plated via connections
    • H05K3/423—Plated through-holes or plated via connections characterised by electroplating method
    • H05K3/424—Plated through-holes or plated via connections characterised by electroplating method by direct electroplating
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/13—Energy storage using capacitors

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Cephalosporin Compounds (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
CA002482113A 2003-09-23 2004-09-20 Process for the purification of thiophenes Abandoned CA2482113A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10343873.4 2003-09-23
DE10343873A DE10343873A1 (de) 2003-09-23 2003-09-23 Verfahren zur Reinigung von Thiophenen

Publications (1)

Publication Number Publication Date
CA2482113A1 true CA2482113A1 (en) 2005-03-23

Family

ID=34177890

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002482113A Abandoned CA2482113A1 (en) 2003-09-23 2004-09-20 Process for the purification of thiophenes

Country Status (14)

Country Link
US (2) US20050065352A1 (enExample)
EP (1) EP1518859B1 (enExample)
JP (1) JP4843207B2 (enExample)
KR (1) KR20050030118A (enExample)
CN (1) CN1616451B (enExample)
AT (1) ATE356132T1 (enExample)
CA (1) CA2482113A1 (enExample)
DE (2) DE10343873A1 (enExample)
DK (1) DK1518859T3 (enExample)
ES (1) ES2283917T3 (enExample)
MX (1) MXPA04009161A (enExample)
PT (1) PT1518859E (enExample)
RU (1) RU2379310C2 (enExample)
TW (1) TWI330182B (enExample)

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CN1681869B (zh) 2002-09-24 2010-05-26 E.I.内穆尔杜邦公司 用于电子器件用聚合物酸胶体制成的可水分散的聚苯胺
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US7390438B2 (en) 2003-04-22 2008-06-24 E.I. Du Pont De Nemours And Company Water dispersible substituted polydioxythiophenes made with fluorinated polymeric sulfonic acid colloids
US7351358B2 (en) 2004-03-17 2008-04-01 E.I. Du Pont De Nemours And Company Water dispersible polypyrroles made with polymeric acid colloids for electronics applications
WO2006073968A2 (en) * 2004-12-30 2006-07-13 E. I. Dupont De Nemours And Company Derivatized 3,4-alkylenedioxythiophene monomers, methods of making them, and use thereof
WO2006074063A2 (en) * 2004-12-30 2006-07-13 E.I. Dupont De Nemours And Company Electrically conductive polymers
KR101356296B1 (ko) 2005-06-28 2014-02-06 이 아이 듀폰 디 네모아 앤드 캄파니 높은 일 함수의 투명한 도체
US8049205B2 (en) * 2006-04-06 2011-11-01 Xerox Corporation Poly(alkynylthiophene)s and electronic devices generated therefrom
DE102006020744A1 (de) * 2006-05-04 2007-11-08 H. C. Starck Gmbh & Co. Kg Verfahren zur Stabilisierung von Thiophenderivaten
US8153029B2 (en) 2006-12-28 2012-04-10 E.I. Du Pont De Nemours And Company Laser (230NM) ablatable compositions of electrically conducting polymers made with a perfluoropolymeric acid applications thereof
US20080191172A1 (en) 2006-12-29 2008-08-14 Che-Hsiung Hsu High work-function and high conductivity compositions of electrically conducting polymers
DE102007052522A1 (de) * 2007-11-01 2009-05-07 H.C. Starck Gmbh Verfahren zur Beschichtung von unpolaren Polyaromaten enthaltenden Schichten
US8094434B2 (en) 2008-04-01 2012-01-10 Avx Corporation Hermetically sealed capacitor assembly
JP2009256276A (ja) * 2008-04-21 2009-11-05 Tayca Corp ３，４−アルキレンジオキシチオフェンの製造方法
US8194395B2 (en) 2009-10-08 2012-06-05 Avx Corporation Hermetically sealed capacitor assembly
US8279584B2 (en) 2010-08-12 2012-10-02 Avx Corporation Solid electrolytic capacitor assembly
US8824122B2 (en) 2010-11-01 2014-09-02 Avx Corporation Solid electrolytic capacitor for use in high voltage and high temperature applications
US8848342B2 (en) 2010-11-29 2014-09-30 Avx Corporation Multi-layered conductive polymer coatings for use in high voltage solid electrolytic capacitors
US8576543B2 (en) 2010-12-14 2013-11-05 Avx Corporation Solid electrolytic capacitor containing a poly(3,4-ethylenedioxythiophene) quaternary onium salt
US8493713B2 (en) 2010-12-14 2013-07-23 Avx Corporation Conductive coating for use in electrolytic capacitors
JP5745881B2 (ja) * 2011-02-14 2015-07-08 テイカ株式会社 固体電解コンデンサ
US8451588B2 (en) 2011-03-11 2013-05-28 Avx Corporation Solid electrolytic capacitor containing a conductive coating formed from a colloidal dispersion
US8947857B2 (en) 2011-04-07 2015-02-03 Avx Corporation Manganese oxide capacitor for use in extreme environments
US9767964B2 (en) 2011-04-07 2017-09-19 Avx Corporation Multi-anode solid electrolytic capacitor assembly
US8379372B2 (en) 2011-04-07 2013-02-19 Avx Corporation Housing configuration for a solid electrolytic capacitor
US8300387B1 (en) 2011-04-07 2012-10-30 Avx Corporation Hermetically sealed electrolytic capacitor with enhanced mechanical stability
DE102013101443B4 (de) 2012-03-01 2025-05-28 KYOCERA AVX Components Corporation (n. d. Ges. d. Staates Delaware) Verfahren zum Ausbilden eines Ultrahochspannungs-Festelektrolytkondensators
US8971019B2 (en) 2012-03-16 2015-03-03 Avx Corporation Wet capacitor cathode containing an alkyl-substituted poly(3,4-ethylenedioxythiophene)
JP2013219362A (ja) 2012-04-11 2013-10-24 Avx Corp 過酷な条件下で強化された機械的安定性を有する固体電解コンデンサ
JP5933397B2 (ja) 2012-08-30 2016-06-08 エイヴィーエックス コーポレイション 固体電解コンデンサの製造方法および固体電解コンデンサ
US9324503B2 (en) 2013-03-15 2016-04-26 Avx Corporation Solid electrolytic capacitor
US9472350B2 (en) 2013-05-13 2016-10-18 Avx Corporation Solid electrolytic capacitor containing a multi-layered adhesion coating
GB2517019B (en) 2013-05-13 2018-08-29 Avx Corp Solid electrolytic capacitor containing conductive polymer particles
GB2514486B (en) 2013-05-13 2018-08-29 Avx Corp Solid electrolytic capacitor containing a pre-coat layer
FR3005894B1 (fr) * 2013-05-23 2020-12-25 Centre Nat Rech Scient Materiau superoleophobe et/ou superhydrophobe, son procede de preparation et ses applications
US10297393B2 (en) 2015-03-13 2019-05-21 Avx Corporation Ultrahigh voltage capacitor assembly
US9928963B2 (en) 2015-03-13 2018-03-27 Avx Corporation Thermally conductive encapsulant material for a capacitor assembly
US9754730B2 (en) 2015-03-13 2017-09-05 Avx Corporation Low profile multi-anode assembly in cylindrical housing
US10014108B2 (en) 2015-03-13 2018-07-03 Avx Corporation Low profile multi-anode assembly
US10431389B2 (en) 2016-11-14 2019-10-01 Avx Corporation Solid electrolytic capacitor for high voltage environments
KR102659642B1 (ko) 2018-08-10 2024-04-22 교세라 에이브이엑스 컴포넌츠 코포레이션 고유 전도성 중합체를 포함하는 고체 전해 커패시터
US11114250B2 (en) 2018-08-10 2021-09-07 Avx Corporation Solid electrolytic capacitor formed from conductive polymer particles
JP7426986B2 (ja) 2018-08-10 2024-02-02 キョーセラ・エイブイエックス・コンポーネンツ・コーポレーション ポリアニリンを含む固体電解キャパシタ
US11081288B1 (en) 2018-08-10 2021-08-03 Avx Corporation Solid electrolytic capacitor having a reduced anomalous charging characteristic
US11380492B1 (en) 2018-12-11 2022-07-05 KYOCERA AVX Components Corporation Solid electrolytic capacitor
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Also Published As

Publication number Publication date
TWI330182B (en) 2010-09-11
EP1518859A1 (de) 2005-03-30
MXPA04009161A (es) 2005-04-05
RU2379310C2 (ru) 2010-01-20
US20050065352A1 (en) 2005-03-24
DE10343873A1 (de) 2005-04-21
CN1616451B (zh) 2011-06-15
DK1518859T3 (da) 2007-05-07
PT1518859E (pt) 2007-05-31
RU2004127972A (ru) 2006-03-10
CN1616451A (zh) 2005-05-18
ES2283917T3 (es) 2007-11-01
EP1518859B1 (de) 2007-03-07
JP4843207B2 (ja) 2011-12-21
JP2005097305A (ja) 2005-04-14
US20090318710A1 (en) 2009-12-24
DE502004003113D1 (de) 2007-04-19
ATE356132T1 (de) 2007-03-15
TW200526617A (en) 2005-08-16
US7994345B2 (en) 2011-08-09
KR20050030118A (ko) 2005-03-29

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