CA2161127C - Method and plant for solvent-free microwave extraction of natural products - Google Patents
Method and plant for solvent-free microwave extraction of natural products Download PDFInfo
- Publication number
- CA2161127C CA2161127C CA002161127A CA2161127A CA2161127C CA 2161127 C CA2161127 C CA 2161127C CA 002161127 A CA002161127 A CA 002161127A CA 2161127 A CA2161127 A CA 2161127A CA 2161127 C CA2161127 C CA 2161127C
- Authority
- CA
- Canada
- Prior art keywords
- enclosure
- biological material
- microwaves
- essential oil
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
- Compounds Of Unknown Constitution (AREA)
- Medicines Containing Plant Substances (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR93/05810 | 1993-05-11 | ||
FR9305810A FR2705035B1 (fr) | 1993-05-11 | 1993-05-11 | Procédé et installation d'extraction sans solvant de produits naturels par micro-ondes. |
PCT/FR1994/000551 WO1994026853A1 (fr) | 1993-05-11 | 1994-05-10 | Procede et installation d'extraction sans solvant de produits naturels par micro-ondes |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2161127A1 CA2161127A1 (en) | 1994-11-24 |
CA2161127C true CA2161127C (en) | 2005-09-27 |
Family
ID=9447117
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002161127A Expired - Fee Related CA2161127C (en) | 1993-05-11 | 1994-05-10 | Method and plant for solvent-free microwave extraction of natural products |
Country Status (16)
Country | Link |
---|---|
EP (1) | EP0698076B1 (el) |
JP (1) | JPH08512337A (el) |
CN (1) | CN1059920C (el) |
AT (1) | ATE162211T1 (el) |
AU (1) | AU682035B2 (el) |
BG (1) | BG62367B1 (el) |
BR (1) | BR9406717A (el) |
CA (1) | CA2161127C (el) |
DE (1) | DE69407965T2 (el) |
DK (1) | DK0698076T3 (el) |
ES (1) | ES2114688T3 (el) |
FR (1) | FR2705035B1 (el) |
GR (1) | GR3026603T3 (el) |
HU (1) | HU218708B (el) |
RU (1) | RU2115700C1 (el) |
WO (1) | WO1994026853A1 (el) |
Families Citing this family (63)
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FR2763795B1 (fr) * | 1997-05-30 | 1999-08-20 | Archimex Pibs | Procede de preparation de vegetaux tels que les epices, les plantes aromatiques et les aromates |
FR2793008B1 (fr) | 1999-04-30 | 2001-07-27 | Valeurs Bois Ind | Procede d'extraction de jus naturel de matieres vegetales ligneuses, dispositif permettant la mise en oeuvre du procede et utilisation du procede pour la production de vegetaux ligneux seches |
FR2787347B1 (fr) * | 1998-12-17 | 2001-01-19 | Gattefosse Ets Sa | Procede de fabrication d'une emulsion a base de materiel vegetal aromatique, emulsion susceptible d'etre obtenue par ledit procede et utilisation de ladite emulsion |
CN1112953C (zh) * | 1999-10-29 | 2003-07-02 | 汤大卫 | 一种液相/固相萃取的方法 |
CN1120736C (zh) * | 2000-09-14 | 2003-09-10 | 中国科学院山西煤炭化学研究所 | 工业用固体物料抽提法 |
EP1439218B1 (de) * | 2003-01-21 | 2004-07-28 | Milestone S.r.l. | Lösungsmittelfreie Mikrowellen-Extraktion von flüchtigen Naturstoffen |
EP1629725B1 (de) * | 2004-07-20 | 2007-09-12 | Milestone S.r.l. | Mikrowellen-unterstützte Extraktion von flüchtigen Naturstoffen |
CN100379754C (zh) * | 2004-11-22 | 2008-04-09 | 王煊 | 一种微波无溶剂加热萃取皂甙的方法 |
CN100421759C (zh) * | 2006-03-10 | 2008-10-01 | 山东轻工业学院 | 一种用于植物有效成分提取的减压微波萃取装置和方法 |
EP2011568B1 (en) * | 2006-03-16 | 2016-08-24 | Universidad Tecnica Federico Santa Maria (Usm) | Device for extraction of organic chemical compounds with toxic properties that are present in atmospheric samples, using focused-microwave-heated solvents in open (non-pressurized) systems |
CN101290277B (zh) * | 2007-04-20 | 2011-05-11 | 财团法人食品工业发展研究所 | 利用微波辐射的快速提取方法 |
TW200842336A (en) * | 2007-04-26 | 2008-11-01 | Food Industry Res & Dev Inst | Microwave accelerating extraction equipment |
FR2925898A1 (fr) * | 2007-12-28 | 2009-07-03 | Jean Pierre Lablanchy | Procede et systeme d'extraction d'huile essentielle a forte teneur en thymoquinone a partir de la plante de nigella sativa |
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JP2011052086A (ja) * | 2009-08-31 | 2011-03-17 | Actree Corp | 蘚苔類からの油脂類抽出方法 |
FR2955331B1 (fr) * | 2010-01-15 | 2012-05-11 | Archimex Pibs | Procede et installation d'extraction de biomasse assistee par micro-onde |
JP6087485B2 (ja) * | 2010-02-25 | 2017-03-01 | エステー株式会社 | 芳香組成物およびこれを利用した芳香剤、消臭剤並びに抗菌剤 |
FR2966700B1 (fr) * | 2010-10-29 | 2013-01-11 | Bernard Mompon | Procede de fabrication d?articles d?origine vegetale impregnes de substance liquide vegetale |
TWI468506B (zh) * | 2011-01-17 | 2015-01-11 | Nat Univ Chung Hsing | 微波輔助萃取微藻油脂方法及其應用 |
CN102252889A (zh) * | 2011-03-15 | 2011-11-23 | 重庆大学 | 微波辅助无溶剂固相顶空提取装置及其提取方法 |
FR2975020B1 (fr) | 2011-05-13 | 2015-03-13 | Univ D Avignon Et Des Pays De Vaucluse | Obtention d'un extrait vegetal a l'aide de micro-ondes |
LV14481B (lv) * | 2011-11-21 | 2012-06-20 | Latvijas Valsts Mežzinātnes Institūts 'silava' | Ūdenī nešķīstošu un ūdenī šķīstošu ēterisko eļļu iegūšanas paņēmiens no augu izejvielām |
RU2473356C1 (ru) * | 2011-12-07 | 2013-01-27 | Общество с ограниченной ответственностью "Компания Клевер" | Способ получения водных экстрактов из растительного сырья с повышенным содержанием извлекаемых активных веществ |
US9486716B2 (en) | 2012-03-14 | 2016-11-08 | State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University | Essential oil extraction apparatus |
FR3003181B1 (fr) * | 2013-03-18 | 2021-04-02 | Innovation & Dev Company Idco | Procede et installation d'extraction de produits biologiques par micro-ondes. |
CN103194312A (zh) * | 2013-03-24 | 2013-07-10 | 西北农林科技大学 | 一种从柏叶中提取挥发油的方法 |
FR3013563B1 (fr) * | 2013-11-28 | 2017-06-30 | Finat Conseil & Distrib | Procede de fabrication de preparations aromatisantes naturelles et stables et preparations aromatisantes obtenues par le dit procede |
CN103725420B (zh) * | 2013-12-20 | 2016-07-13 | 江南大学 | 一种提取黑种草属植物种子挥发油的方法、装置及应用 |
FR3017308B1 (fr) | 2014-02-10 | 2022-06-17 | Idco | Dispositif et procede d'extraction de produits biologiques par micro-ondes et ultrasons |
CN103820218A (zh) * | 2014-03-07 | 2014-05-28 | 张家界金绿油脂有限责任公司 | 一种油菜籽微波提取油脂的方法 |
JP5899604B2 (ja) * | 2014-03-24 | 2016-04-06 | 兼松エンジニアリング株式会社 | マイクロ波を利用したバイオマス再資源化装置 |
TWI601565B (zh) * | 2014-06-05 | 2017-10-11 | Timing Pharmaceutical Co Ltd | Essential oil extraction device |
CN104327951A (zh) * | 2014-10-23 | 2015-02-04 | 郑州工业应用技术学院 | 一种热空气精油提取装置 |
CN104872605B (zh) * | 2014-12-08 | 2018-02-06 | 中国热带农业科学院南亚热带作物研究所 | 制备液熏香料的方法和液熏香料 |
RO130896A0 (ro) * | 2015-01-19 | 2016-02-26 | Mariana Pătraşcu | Reactor continuu pentru extracţia asistată de microunde şi ultrasunete a compuşilor biologic activi din plante |
CN104711121A (zh) * | 2015-02-28 | 2015-06-17 | 湖北中烟工业有限责任公司 | 一种超声辅助无溶剂微波萃取野菊花精油的方法 |
CN104784965B (zh) * | 2015-04-20 | 2016-10-05 | 张新泉 | 一种中药微波萃取装置 |
RU2582292C1 (ru) * | 2015-05-07 | 2016-04-20 | федеральное государственное автономное образовательное учреждение высшего образования "Российский университет дружбы народов" (РУДН) | Способ выделения эфирного масла из лекарственного растительного сырья |
CN105219526A (zh) * | 2015-09-25 | 2016-01-06 | 四川省林业科学研究院 | 一种油樟油微波提取装置及方法 |
CN105232782B (zh) * | 2015-11-09 | 2019-11-22 | 北京工商大学 | 一种鲜茶鲜活水及其制备方法与应用 |
CN105213273B (zh) * | 2015-11-09 | 2018-11-13 | 北京工商大学 | 一种柠檬鲜活水及其制备方法与应用 |
CN105213272B (zh) * | 2015-11-09 | 2019-02-01 | 北京工商大学 | 一种薰衣草鲜活水及其制备方法与应用 |
CN105232400B (zh) * | 2015-11-09 | 2018-11-02 | 北京工商大学 | 一种茉莉鲜活水及其制备方法与应用 |
CN105250180B (zh) * | 2015-11-09 | 2018-11-27 | 北京工商大学 | 一种玫瑰鲜活水及其制备方法与应用 |
CN105713726A (zh) * | 2016-03-31 | 2016-06-29 | 李颖 | 一种快速无溶剂萃取天然植物精油和纯露的方法及装置 |
CN106190574A (zh) * | 2016-07-28 | 2016-12-07 | 河南科技学院 | 一种茅苍术挥发油及其制备方法 |
JP2017008111A (ja) * | 2016-10-17 | 2017-01-12 | エステー株式会社 | 芳香組成物およびこれを利用した芳香剤、消臭剤並びに抗菌剤 |
RU2636155C1 (ru) * | 2016-12-20 | 2017-11-21 | Федеральное Государственное Бюджетное Образовательное Учреждение Высшего Образования "Нижегородская Государственная Сельскохозяйственная Академия" (ФГБОУ ВО НГСХА) | Микроволновая технология извлечения жира из жиросодержащего сырья |
RU2649024C1 (ru) * | 2017-01-10 | 2018-03-29 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Кубанский государственный технологический университет" (ФГБОУ ВО "КубГТУ") | Способ получения эфирного масла мяты перечной |
FR3066703B1 (fr) * | 2017-05-24 | 2020-10-16 | Erpim | Procede et dispositif d’extraction solide/liquide a contre-courant comportant une etape de sechage |
WO2019043058A1 (en) | 2017-08-31 | 2019-03-07 | Firmenich Sa | EXTRACTION OF ESSENTIAL OILS FROM MICROWAVE ASSISTED PLANT BIOMASS |
FR3074425B1 (fr) | 2017-12-01 | 2020-09-04 | Univ D'avignon Et Des Pays De Vaucluse | Dispositif d’extraction et de separation de composes volatiles et non-volatiles d’une matiere biologique et procede associe |
JP6359752B1 (ja) * | 2017-12-22 | 2018-07-18 | 日本フレーバー工業株式会社 | バニラエキストラクトの製造方法及びバニラエキストラクト |
FR3099991B1 (fr) | 2019-08-22 | 2023-12-22 | Soc De Courtage Et De Diffusion Codif International | Ingrédient de composition cosmétique pour cuir chevelu sensible |
CN110747060A (zh) * | 2019-10-21 | 2020-02-04 | 华侨大学 | 一种超声辅助无溶剂微波萃取互叶白千层精油的方法 |
FR3113248B1 (fr) | 2020-08-04 | 2022-08-05 | Soc De Courtage Et De Diffusion Codif International | Extrait de cellules de Lavandula stoechas, compositions le comprenant, utilisations cosmétiques et procédé de culture des cellules de Lavandula stoechas. |
FR3115694B3 (fr) | 2020-10-30 | 2022-10-28 | Soc De Courtage Et De Diffusion Codif International | Principe actif constitué d’un extrait de pomme amère activant des récepteurs à l’amertume Tas2Rs présents sur la peau humaine et utilisations cosmétiques et dermato-cosmétiques correspondantes. |
CN116528664A (zh) * | 2020-12-08 | 2023-08-01 | 艾饰庭株式会社 | 排泄物处理材料和利用其的排泄物的除臭方法 |
CN112760166A (zh) * | 2021-01-08 | 2021-05-07 | 四川轻化工大学 | 藤椒油生产设备 |
WO2022163063A1 (ja) * | 2021-01-28 | 2022-08-04 | エステー株式会社 | 排泄物処理材およびこれを利用した排泄物の消臭方法 |
CN113388459B (zh) * | 2021-05-26 | 2022-03-01 | 宁波芮颂生物科技有限公司 | 一种抗猫、狗过敏原整理组合物溶液的制备方法 |
US11702615B1 (en) | 2022-03-09 | 2023-07-18 | Chemtech Services, Inc. | Microwave extraction of essential oils |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA1336968C (en) * | 1989-05-16 | 1995-09-12 | J. R. Jocelyn Pare | Microwave-assisted natural products extraction |
SE9003593D0 (sv) * | 1990-11-12 | 1990-11-12 | T G Owe Berg | Foerfarande foer omvandling av vaerme till arbete |
EP0485668B1 (en) * | 1990-11-16 | 1996-01-17 | Her Majesty The Queen In Right Of Canada As Represented By The Minister Of The Environment | Microwave extraction of volatile oils and apparatus therefor |
-
1993
- 1993-05-11 FR FR9305810A patent/FR2705035B1/fr not_active Expired - Fee Related
-
1994
- 1994-05-10 CA CA002161127A patent/CA2161127C/en not_active Expired - Fee Related
- 1994-05-10 WO PCT/FR1994/000551 patent/WO1994026853A1/fr active IP Right Grant
- 1994-05-10 ES ES94915607T patent/ES2114688T3/es not_active Expired - Lifetime
- 1994-05-10 BR BR9406717A patent/BR9406717A/pt not_active IP Right Cessation
- 1994-05-10 CN CN94192507A patent/CN1059920C/zh not_active Expired - Fee Related
- 1994-05-10 HU HU9503230A patent/HU218708B/hu not_active IP Right Cessation
- 1994-05-10 AT AT94915607T patent/ATE162211T1/de not_active IP Right Cessation
- 1994-05-10 DK DK94915607T patent/DK0698076T3/da active
- 1994-05-10 RU RU95122234A patent/RU2115700C1/ru active
- 1994-05-10 JP JP6525060A patent/JPH08512337A/ja not_active Ceased
- 1994-05-10 EP EP94915607A patent/EP0698076B1/fr not_active Expired - Lifetime
- 1994-05-10 AU AU67251/94A patent/AU682035B2/en not_active Ceased
- 1994-05-10 DE DE69407965T patent/DE69407965T2/de not_active Expired - Lifetime
-
1995
- 1995-12-04 BG BG100187A patent/BG62367B1/bg unknown
-
1998
- 1998-04-10 GR GR980400799T patent/GR3026603T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
BR9406717A (pt) | 1996-02-06 |
RU2115700C1 (ru) | 1998-07-20 |
HU9503230D0 (en) | 1996-01-29 |
FR2705035A1 (fr) | 1994-11-18 |
JPH08512337A (ja) | 1996-12-24 |
BG100187A (bg) | 1996-05-31 |
EP0698076B1 (fr) | 1998-01-14 |
DK0698076T3 (da) | 1998-09-14 |
DE69407965D1 (de) | 1998-02-19 |
GR3026603T3 (en) | 1998-07-31 |
AU682035B2 (en) | 1997-09-18 |
ES2114688T3 (es) | 1998-06-01 |
EP0698076A1 (fr) | 1996-02-28 |
AU6725194A (en) | 1994-12-12 |
HUT75578A (en) | 1997-05-28 |
HU218708B (hu) | 2000-11-28 |
FR2705035B1 (fr) | 1995-08-04 |
CN1125461A (zh) | 1996-06-26 |
CN1059920C (zh) | 2000-12-27 |
DE69407965T2 (de) | 1998-09-10 |
WO1994026853A1 (fr) | 1994-11-24 |
ATE162211T1 (de) | 1998-01-15 |
CA2161127A1 (en) | 1994-11-24 |
BG62367B1 (bg) | 1999-09-30 |
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