CN113388459B - 一种抗猫、狗过敏原整理组合物溶液的制备方法 - Google Patents

一种抗猫、狗过敏原整理组合物溶液的制备方法 Download PDF

Info

Publication number
CN113388459B
CN113388459B CN202110576495.2A CN202110576495A CN113388459B CN 113388459 B CN113388459 B CN 113388459B CN 202110576495 A CN202110576495 A CN 202110576495A CN 113388459 B CN113388459 B CN 113388459B
Authority
CN
China
Prior art keywords
parts
cat
finishing composition
composition solution
allergen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202110576495.2A
Other languages
English (en)
Other versions
CN113388459A (zh
Inventor
周剑
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningbo Ruisong Biological Technology Co ltd
Original Assignee
Ningbo Ruisong Biological Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ningbo Ruisong Biological Technology Co ltd filed Critical Ningbo Ruisong Biological Technology Co ltd
Priority to CN202110576495.2A priority Critical patent/CN113388459B/zh
Priority to US17/338,232 priority patent/US11541090B2/en
Priority to JP2021094316A priority patent/JP7224678B2/ja
Publication of CN113388459A publication Critical patent/CN113388459A/zh
Application granted granted Critical
Publication of CN113388459B publication Critical patent/CN113388459B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/86—Mixtures of anionic, cationic, and non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/046—Salts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/1233—Carbonates, e.g. calcite or dolomite
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2082—Polycarboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C11D3/227—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin with nitrogen-containing groups
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/384—Animal products
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38618—Protease or amylase in liquid compositions only
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38636—Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D06M13/148—Polyalcohols, e.g. glycerol or glucose
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • D06M13/238—Tannins, e.g. gallotannic acids
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10—Preparation or pretreatment of starting material
    • A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10—Preparation or pretreatment of starting material
    • A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50—Methods involving additional extraction steps
    • A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/04—Carboxylic acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C11D1/721—End blocked ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
    • C11D2111/40—Specific cleaning or washing processes
    • C11D2111/46—Specific cleaning or washing processes applying energy, e.g. irradiation
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Textile Engineering (AREA)
  • Emergency Medicine (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Biochemistry (AREA)
  • Medical Informatics (AREA)
  • Public Health (AREA)
  • Mycology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Veterinary Medicine (AREA)
  • Botany (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Zoology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)

Abstract

本发明公开了一种抗猫、狗过敏原整理组合物溶液的制备方法，其制备过程为：将日本天王柿子、依兰花瓣清洗3～5次、研碎，超声处理，制得悬浊液；将上述悬浊液微波处理，随后离心处理，制得淡黄色上清液；将上述淡黄色上清液膜分离处理，形成日本天王柿子、依兰混合提取液。将上述制备的日本天王柿子、依兰混合提取液2～5份、银离子化合物2～5份、桉树油5～30份、脂肪醇聚氧乙烯醚5～20份、十二烷基苯磺酸钠5～20份、月桂酸钠0.05～1份、硬脂酸钠0.05～1份、柠檬酸2～5份、丝氨酸蛋白酶0.5～1份、果胶酶0.5～1份、纤维素酶0.5～1份、木聚糖酶0.5～1份、β—葡聚糖酶0.5～1份、甘油20～40份、十六烷基二甲基苄基氯化铵0.05～1份、壳聚糖5～10份、色素0.1～0.5、植物香精2～3份、防腐剂0.2～1份、去离子水20～50份混合均匀，超声震荡、降温至室温，即制备得到抗猫、狗过敏原整理组合物溶液。该组合物制备方法简单、可用于日常的喷洒、擦拭，也可在洗衣或烘干过程中应用。

Description

一种抗猫、狗过敏原整理组合物溶液的制备方法
技术领域
本发明属于抗过敏源整理组合物领域，具体涉及一种抗猫、狗过敏原整理组合物溶液的制备方法。
背景技术
近年来，育儿式养育宠物已成为现代人的一种流行趋势。根据“天猫国际”发布的年度消费报告显示，宠物消费需求升级，宠物商品越来越丰富且出现细分化趋势，在宠物用品市场中，清洁护理类的需求量最大。然而，在养育宠物时，宠物的过敏原如皮屑、皮脂腺皮肤分泌物、唾液、尿液和鸟羽毛尘等，通过宠物脱落的毛发，被吸入肺部时，高达10％的普通人群和40％的过敏个体会产生过敏或哮喘反应，无法实现自由养育宠物的需求。尤其是猫的过敏原，体积极小，重量非常轻，在整个房子的气流中循环，可在空气中飘浮数小时最终进入地毯、床上用品、软垫家具、粗糙纹理织物、墙面、加热管道、空调以及它们接触到的任何其他东西。那么，发明一种制备方法简单、且对宠物身体与人类无任何副作用，既可用于宠物清洁护理又具备抗过敏原属性、可满足易敏人群养育宠物需求的产品具备广阔的市场前景。
发明内容
为了解决上述问题，本发明以日本天王柿子、依兰混合提取液、银离子化合物、桉树油等天然物质为主要成分，通过超声、微波、膜处理等先进技术手段，制备得到抗猫、狗过敏原整理组合物溶液。该组合物制备方法简单、可用于日常的喷洒、擦拭使用，也可在洗衣或烘干过程中应用。
本发明是一种抗猫、狗过敏原整理组合物溶液的制备方法，主要包括以下步骤：
(1)将日本天王柿子、依兰花瓣清洗3～5次、研碎，超声处理，制得悬浊液；
(2)将上述悬浊液微波处理，随后离心处理，制得淡黄色上清液；
(3)将上述淡黄色上清液膜分离处理，形成日本天王柿子提取液；
(4)将制得的日本天王柿子、依兰混合提取液2～5份、银离子化合物2～5份、桉树油5～30份、脂肪醇聚氧乙烯醚5～20份、十二烷基苯磺酸钠5～20份、月桂酸钠0.05～1份、硬脂酸钠0.05～1份、柠檬酸2～5份、丝氨酸蛋白酶0.5～1份、果胶酶0.5～1份、纤维素酶0.5～1份、木聚糖酶0.5～1份、β—葡聚糖酶0.5～1份、甘油20～40份、十六烷基二甲基苄基氯化铵0.05～1份、壳聚糖5～10份、色素0.1～0.5、植物香精2～3份、防腐剂0.2～1份、去离子水20～50份；优选日本天王柿提取液2～3份、长崎贝壳粉2～3份、银离子化合物2～3份、桉树油5～20份、脂肪醇聚氧乙烯醚5～10份、十二烷基苯磺酸钠5～15份、月桂酸钠0.05～0.5份、硬脂酸钠0.05～0.5份、柠檬酸4～5份、丝氨酸蛋白酶0.5～1份、果胶酶0.5～1份、纤维素酶0.5～1份、木聚糖酶0.5～1份、β—葡聚糖酶0.5～1份、甘油25～40份、十六烷基二甲基苄基氯化铵0.05～1份、壳聚糖8～10份、色素0.1～0.5、植物香精2～3份、防腐剂0.2～1份、去离子水20～40份，混合均匀，一定温度下超声震荡一定时间，降温至室温后即制得抗猫、狗过敏原整理组合物溶液。
所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(1)中所述，超声处理的条件为超声温度30～80℃，超声时间15～60min；优选超声温度40～60℃，超声时间30～60min。
所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(2)中所述，微波处理的条件为微波输出功率300～800W，时间20～45min，温度30～80℃；优选微波输出功率400～600W，时间25～45min，温度60～80℃。
所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(2)中所述，离心处理的条件为转速300～1500r/min，离心时间5～30min；优选转速800～1500r/min，离心时间5～15min。
所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(3)中所述，膜分离处理的条件为超滤膜操作压差0.1～5MPa，纳滤膜操作压力差0.1～5MPa，膜面流速0.5～5m/s，温度35～55℃；优选超滤膜操作压差0.1～3MPa，纳滤膜操作压力差0.1～3MPa，膜面流速0.5～2.5m/s，温度35～45℃。
所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(4)中所述一定温度为45～65℃；所述一定时间为2～10h。优选一定温度为55～65℃；一定时间为6～8h。
本发明以日本天王柿子、依兰混合提取液、桉树油、银离子化合物等物质为主要原材料，通过超声、微波、膜处理等先进技术手段，利用日本天王柿子中提取的胆碱、芦丁、单宁等，依兰中提取的依兰精油，桉树油，银离子等抗菌成分与猫、狗中主要的过敏原蛋白质作用，从而起到抗过敏原的功效。该组合物制备方法简单、可用于日常的喷洒、擦拭使用，也可在洗衣或烘干过程中应用。
附图说明
图1为本发明实施例1-5中不同质量配比的整理组合物溶液对猫过敏原Fel d1的抗过敏效果图；
图2为本发明实施例1-5中不同质量配比的整理组合物溶液对狗过敏原为Can f1的抗过敏效果图；
图3为本发明实施例3在不同反应时间下对猫过敏原Fel d1的抗过敏效果图；
图4为本发明实施例3在不同反应时间下对狗过敏原Can f1的抗过敏效果图。
具体实施方式
下面结合具体实施例对本发明方法作详细说明，本实施例在以本发明技术方案为前提下进行实施，但本发明的保护范围不限于下述的实施例。
实施例1
将日本天王柿子、依兰花瓣清洗3～5次、研碎，40℃超声30min制得悬浊液；将上述悬浊液置于60℃微波25min，微波输出功率设定为400W；随后，1500r/min离心5min，制得淡黄色上清液；将上述淡黄色上清液55℃下膜分离处理，超滤膜操作压差为0.5MPa，纳滤膜操作压力差0.5MPa，膜面流速为0.5m/s，形成日本天王柿子、依兰混合提取液；按质量份数为日本天王柿、依兰混合提取液2份、银离子化合物2份、桉树油5份、脂肪醇聚氧乙烯醚15份、十二烷基苯磺酸钠15份、月桂酸钠1份、硬脂酸钠1份、柠檬酸5份、丝氨酸蛋白酶1份、纤维素酶1份、果胶酶1份、纤维素酶1份、木聚糖酶1份、β—葡聚糖酶1份、甘油35份、十六烷基二甲基苄基氯化铵1份、壳聚糖8份、色素0.1份、植物香精2份、防腐剂0.2份、去离子水35份，65℃下超声震荡6h，降温至室温后，即制得抗猫、狗过敏原整理组合物溶液。
实施例2
将日本天王柿子、依兰花瓣清洗3～5次、研碎，40℃超声30min制得悬浊液；将上述悬浊液置于60℃微波25min，微波输出功率设定为400W；随后，1500r/min离心5min，制得淡黄色上清液；将上述淡黄色上清液55℃下膜分离处理，超滤膜操作压差为0.5MPa，纳滤膜操作压力差0.5MPa，膜面流速为0.5m/s，形成日本天王柿子、依兰混合提取液；按质量份数为日本天王柿、依兰混合提取液3份、银离子化合物2份、桉树油5份、脂肪醇聚氧乙烯醚15份、十二烷基苯磺酸钠15份、月桂酸钠1份、硬脂酸钠1份、柠檬酸5份、丝氨酸蛋白酶1份、纤维素酶1份、果胶酶1份、纤维素酶1份、木聚糖酶1份、β—葡聚糖酶1份、甘油35份、十六烷基二甲基苄基氯化铵1份、壳聚糖8份、色素0.1份、植物香精2份、防腐剂0.2份、去离子水35份，65℃下超声震荡6h，降温至室温后，即制得抗猫、狗过敏原整理组合物溶液。
实施例3
将日本天王柿子、依兰花瓣清洗3～5次、研碎，40℃超声30min制得悬浊液；将上述悬浊液置于60℃微波25min，微波输出功率设定为400W；随后，1500r/min离心5min，制得淡黄色上清液；将上述淡黄色上清液55℃下膜分离处理，超滤膜操作压差为0.5MPa，纳滤膜操作压力差0.5MPa，膜面流速为0.5m/s，形成日本天王柿子、依兰混合提取液；按质量份数为日本天王柿、依兰混合提取液5份、银离子化合物2份、桉树油5份、脂肪醇聚氧乙烯醚15份、十二烷基苯磺酸钠15份、月桂酸钠1份、硬脂酸钠1份、柠檬酸5份、丝氨酸蛋白酶1份、纤维素酶1份、果胶酶1份、纤维素酶1份、木聚糖酶1份、β—葡聚糖酶1份、甘油35份、十六烷基二甲基苄基氯化铵1份、壳聚糖8份、色素0.1份、植物香精2份、防腐剂0.2份、去离子水35份，65℃下超声震荡6h，降温至室温后，即制得抗猫、狗过敏原整理组合物溶液。
实施例4
将日本天王柿子、依兰花瓣清洗3～5次、研碎，40℃超声30min制得悬浊液；将上述悬浊液置于60℃微波25min，微波输出功率设定为400W；随后，1500r/min离心5min，制得淡黄色上清液；将上述淡黄色上清液55℃下膜分离处理，超滤膜操作压差为0.5MPa，纳滤膜操作压力差0.5MPa，膜面流速为0.5m/s，形成日本天王柿子、依兰混合提取液；按质量份数为日本天王柿、依兰混合提取液2份、银离子化合物3份、桉树油5份、脂肪醇聚氧乙烯醚15份、十二烷基苯磺酸钠15份、月桂酸钠1份、硬脂酸钠1份、柠檬酸5份、丝氨酸蛋白酶1份、纤维素酶1份、果胶酶1份、纤维素酶1份、木聚糖酶1份、β—葡聚糖酶1份、甘油35份、十六烷基二甲基苄基氯化铵1份、壳聚糖8份、色素0.1份、植物香精2份、防腐剂0.2份、去离子水35份，65℃下超声震荡6h，降温至室温后，即制得抗猫、狗过敏原整理组合物溶液。
实施例5
将日本天王柿子、依兰花瓣清洗3～5次、研碎，40℃超声30min制得悬浊液；将上述悬浊液置于60℃微波25min，微波输出功率设定为400W；随后，1500r/min离心5min，制得淡黄色上清液；将上述淡黄色上清液55℃下膜分离处理，超滤膜操作压差为0.5MPa，纳滤膜操作压力差0.5MPa，膜面流速为0.5m/s，形成日本天王柿子、依兰混合提取液；按质量份数为日本天王柿、依兰混合提取液5份、长崎贝壳粉5份、银离子化合物3份、桉树油5份、脂肪醇聚氧乙烯醚15份、十二烷基苯磺酸钠15份、月桂酸钠1份、硬脂酸钠1份、柠檬酸5份、丝氨酸蛋白酶1份、纤维素酶1份、果胶酶1份、纤维素酶1份、木聚糖酶1份、β—葡聚糖酶1份、甘油35份、十六烷基二甲基苄基氯化铵1份、壳聚糖8份、色素0.1份、植物香精2份、防腐剂0.2份、去离子水35份，65℃下超声震荡6h，降温至室温后，即制得抗猫、狗过敏原整理组合物溶液。
性能测试
猫的主要过敏原为Feld1，一种由皮脂腺分泌的糖蛋白，主要存在于其皮屑、唾液、尿液中；狗的主要过敏原为Canf1，主要存在于其皮屑、唾液、尿液、血清中。
测试一
取质地、尺寸完全相同的两块棉布编号为A、B分别置于浓度为5000ng/mL的猫过敏原提取物Fel d1、狗过敏原提取物Can f1中，室温下浸泡24h。将上述的两块棉布分别六等分，分别编号为a1、a2、a3、a4、a5、a6，b1、b2、b3、b4、b5、b6。
将编号为a1、a2、a3、a4、a5的棉布分别用实施例1-5中制备的抗猫、狗过敏原整理组合物溶液浸泡45min，a6浸泡于纯净水中45min，采用
Figure GDA0003477513620000061
(Multiplex Array forindoor Allergens)方法检测制备的不同质量配比的整理组合物溶液对猫过敏原Fel d1的抗过敏效果，检测结果如图1所示。
将编号为b1、b2、b3、b4、b5的棉布分别用实施例1-5中制备的抗猫、狗过敏原整理组合物溶液浸泡45min，b6浸泡于纯净水中45min，采用MARIATM技术检测制备的不同质量配比的整理组合物溶液对狗过敏原Can f1的抗过敏效果，检测结果如图2所示。
测试二
将与上述a1、a2、a3、a4、a5、a6同样处理的棉布用实施例3中制备的抗猫、狗过敏原整理组合物溶液浸泡15min、30min、45min、60min、90min、120min，采用
Figure GDA0003477513620000071
(Multiplex Array for indoor Allergens)方法检测不同的反应时间对猫过敏原Fel d1的抗过敏效果，检测结果如图3所示。
将与上述b1、b2、b3、b4、b5、b6同样处理的棉布用实施例3中制备的抗猫、狗过敏原整理组合物溶液浸泡15min、30min、45min、60min、90min、120min，采用
Figure GDA0003477513620000072
(Multiplex Array for indoor Allergens)方法检测不同反应时间对狗过敏原Can f1的抗过敏效果，检测结果如图4所示。

Claims (6)

1.一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：该制备方法主要包括以下步骤：
(1)将日本天王柿子、依兰花瓣清洗3～5次、研碎，超声处理，制得悬浊液；
(2)将上述悬浊液微波处理，随后离心处理，制得淡黄色上清液；
(3)将上述淡黄色上清液膜分离处理，形成日本天王柿子、依兰混合提取液；
(4)将制得的日本天王柿子、依兰混合提取液2～5份、银离子化合物2～5份、桉树油5～30份、脂肪醇聚氧乙烯醚5～20份、十二烷基苯磺酸钠5～20份、月桂酸钠0.05～1份、硬脂酸钠0.05～1份、柠檬酸2～5份、丝氨酸蛋白酶0.5～1份、果胶酶0.5～1份、纤维素酶0.5～1份、木聚糖酶0.5～1份、β—葡聚糖酶0.5～1份、甘油20～40份、十六烷基二甲基苄基氯化铵0.05～1份、壳聚糖5～10份、色素0.1～0.5、植物香精2～3份、防腐剂0.2～1份、去离子水20～50份混合均匀，一定温度下超声震荡一定时间，降温至室温后即制得抗猫、狗过敏原整理组合物溶液。
2.根据权利要求1所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(1)中所述超声处理的条件为超声温度为30～80℃，超声时间为15～60min。
3.根据权利要求1所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(2)中所述微波处理的条件为微波输出功率300～800W，时间20～45min，温度30～80℃。
4.根据权利要求1所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(2)中所述离心处理的条件为转速300～1500r/min，离心时间5～30min。
5.根据权利要求1所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(3)中所述膜分离处理的条件为超滤膜操作压差0.1～5MPa，纳滤膜操作压力差0.1～5MPa，膜面流速0.5～5m/s，温度35～55℃。
6.根据权利要求1所述一种抗猫、狗过敏原整理组合物溶液的制备方法，其特征在于：步骤(4)中所述一定温度为45～65℃；所述一定时间为2～10h。
CN202110576495.2A 2021-05-26 2021-05-26 一种抗猫、狗过敏原整理组合物溶液的制备方法 Active CN113388459B (zh)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN202110576495.2A CN113388459B (zh) 2021-05-26 2021-05-26 一种抗猫、狗过敏原整理组合物溶液的制备方法
US17/338,232 US11541090B2 (en) 2021-05-26 2021-06-03 Composition for eliminating household pet allergens
JP2021094316A JP7224678B2 (ja) 2021-05-26 2021-06-04 抗猫・犬アレルゲン仕上げ組成物溶液の調製方法及びその使用

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110576495.2A CN113388459B (zh) 2021-05-26 2021-05-26 一种抗猫、狗过敏原整理组合物溶液的制备方法

Publications (2)

Publication Number Publication Date
CN113388459A CN113388459A (zh) 2021-09-14
CN113388459B true CN113388459B (zh) 2022-03-01

Family

ID=77619129

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110576495.2A Active CN113388459B (zh) 2021-05-26 2021-05-26 一种抗猫、狗过敏原整理组合物溶液的制备方法

Country Status (3)

Country Link
US (1) US11541090B2 (zh)
JP (1) JP7224678B2 (zh)
CN (1) CN113388459B (zh)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115844776A (zh) * 2022-10-24 2023-03-28 宁波芮颂生物科技有限公司 一种长效、持久宠物抗过敏毛发护理液的制备方法

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2705035B1 (fr) * 1993-05-11 1995-08-04 Archimex Pibs Procédé et installation d'extraction sans solvant de produits naturels par micro-ondes.
JP2001129349A (ja) 1999-11-08 2001-05-15 Mimasukashichi Shoten:Kk 脱臭方法および脱臭装置
US20020022043A1 (en) 1999-12-28 2002-02-21 Miller Jeffrey D. Method for killing house dust mites in clothing and other soft materials
JP4478370B2 (ja) 2000-04-04 2010-06-09 ライオン株式会社 繊維製品用液体仕上げ剤組成物
US6395394B1 (en) 2000-04-17 2002-05-28 Twaron Products B.V. Finish composition for treating yarns
US7008457B2 (en) 2001-10-18 2006-03-07 Mark Robert Sivik Textile finishing composition and methods for using same
US6989035B2 (en) 2001-10-18 2006-01-24 The Procter & Gamble Company Textile finishing composition and methods for using same
US20050054702A1 (en) 2002-09-09 2005-03-10 Lonza Inc. Method of controlling allergens
JP4000038B2 (ja) 2002-10-11 2007-10-31 東レ・ダウコーニング株式会社 繊維糸状物用ストレート油剤組成物
JP3650388B2 (ja) 2002-10-29 2005-05-18 花王株式会社 アレルゲン除去剤
US7037535B2 (en) 2002-11-19 2006-05-02 Kimberly-Clark Worldwide, Inc. Method and composition for neutralizing house dust mite feces
JP4044080B2 (ja) * 2003-12-02 2008-02-06 花王株式会社 アレルゲン除去剤
US7381231B2 (en) 2004-01-29 2008-06-03 3M Innovative Properties Company Finishing compositions with reduced volatile organic compounds
CN101008120A (zh) 2006-01-23 2007-08-01 张文琪 防过敏原编织布
US20100209530A1 (en) 2007-10-01 2010-08-19 Yoshinao Yamada Anti-allergen agent
DE102008044700A1 (de) * 2008-08-15 2010-02-18 Dr. Scheller Cosmetics Ag Zusammensetzungen für die topische Anwendung in der Hautpflege mit verbessertem Wirkprofil
CN103261357B (zh) 2010-10-14 2014-12-31 东亚合成株式会社 抗变应原剂
JP2012153739A (ja) 2011-01-21 2012-08-16 Tanning Co Ltd 花粉アレルゲン不活性化方法および不活性化剤
CN104478950B (zh) * 2014-12-19 2017-04-05 桂林得坤生物科技股份有限公司 一种从柿子中提取小分子单宁含量多的柿单宁的方法
DE102014119332A1 (de) 2014-12-22 2016-06-23 Schill + Seilacher Gmbh Zusammensetzung zur permanent-hydrophilen Ausrüstung von Textilfasern und Textilerzeugnissen
US10155692B2 (en) 2015-03-13 2018-12-18 United States Gypsum Company Hydrophobic finish compositions with extended flow time retention and building products made thereof
CN105623929B (zh) 2016-01-06 2018-04-27 中华全国供销合作总社南京野生植物综合利用研究院 一种除菌抗敏的青花椒护肤皂及其制备方法
US11466400B2 (en) 2018-06-19 2022-10-11 Hexcel Corporation Finish composition
CN111440674A (zh) * 2020-05-13 2020-07-24 杭州炫墨生物科技有限公司 一种具有除螨效果的液体洗涤剂

Also Published As

Publication number Publication date
JP2022182905A (ja) 2022-12-08
JP7224678B2 (ja) 2023-02-20
CN113388459A (zh) 2021-09-14
US11541090B2 (en) 2023-01-03
US20220378860A1 (en) 2022-12-01

Similar Documents

Publication Publication Date Title
CN104997206B (zh) 一种具有抑菌作用的竹纤维服装面料
EP2823714B1 (en) Method for producing low-ash poultry plasma protein powder by utilizing poultry blood
CN108456966B (zh) 一种环保亲柔天丝面料的制备方法
CN113388459B (zh) 一种抗猫、狗过敏原整理组合物溶液的制备方法
CN108786967B (zh) 一种营养大米的加工方法
CN103355672A (zh) 一种竹笋膳食纤维超微粉冲剂的制备方法
CN109385457A (zh) 一种具有抗氧化活性的大鲵美拉德肽的制备方法
CN102260933B (zh) 牛奶蛋白共混再生纤维素纤维及其制备工艺与应用
CN104894202A (zh) 一种从兔皮中提取胶原蛋白的方法
CN103960457A (zh) 一种具有高溶解度的低植酸大豆分离蛋白的制备方法
CN107174559A (zh) 一种抗雾霾面膜
CN108587818B (zh) 牡丹籽油抑菌护肤香皂及其制备方法
CN111455657B (zh) 一种假发用牛毛纤维及其制备方法
CN112021408A (zh) 一种改善奶粉致敏性的加工方法
CN103772511A (zh) 芋头淀粉的生产工艺
CN105820731A (zh) 一种含超细羽绒纤维-壳聚糖微球的水性聚氨酯涂层剂
CN100352839C (zh) 具有降血脂功能的昆虫蛋白的制备方法
CN106082752B (zh) 一种酶交联混合水解蛋白水泥发泡剂的制备方法
CN113445311A (zh) 一种抗菌、抗过敏环保纺织品整理剂的制备方法
JP3964201B2 (ja) 木質繊維材料の製造方法
TR202020490A2 (tr) Vegan deri̇ ve üreti̇m yöntemi̇
CN106010300B (zh) 一种河豚鱼鱼皮明胶的制备方法
CN111234008A (zh) 去除抗原性的i型胶原蛋白及其制备方法和应用和椰子糖及其制备方法
CN103469544A (zh) 天丝混纺保健内衣面料
CN110893020A (zh) 一种低成本滋养型儿童内衣面料的制备方法

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant