CA2161127A1 - Method and plant for solvent-free microwave extraction of natural products - Google Patents

Method and plant for solvent-free microwave extraction of natural products

Info

Publication number
CA2161127A1
CA2161127A1 CA002161127A CA2161127A CA2161127A1 CA 2161127 A1 CA2161127 A1 CA 2161127A1 CA 002161127 A CA002161127 A CA 002161127A CA 2161127 A CA2161127 A CA 2161127A CA 2161127 A1 CA2161127 A1 CA 2161127A1
Authority
CA
Canada
Prior art keywords
solvent
plant
microwave extraction
natural products
biological material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002161127A
Other languages
French (fr)
Other versions
CA2161127C (en
Inventor
Philippe Mengal
Bernard Mompon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Archimex
Original Assignee
Philippe Mengal
Bernard Mompon
Archimex
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Philippe Mengal, Bernard Mompon, Archimex filed Critical Philippe Mengal
Publication of CA2161127A1 publication Critical patent/CA2161127A1/en
Application granted granted Critical
Publication of CA2161127C publication Critical patent/CA2161127C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/027—Recovery of volatiles by distillation or stripping

Abstract

The microwave extraction method involves the steps of placing the biological material in an enclosure without any solvent whatsoever and exposing it to microwave radiation to free at least some of the natural product, and then separating the residual biological material from the extracted natural product. Additionally, it involves the steps of applying reduced pressure in said enclosure during said microwave radiation stage and heating the enclosure during at least most of the microwave radiation stage to compensate the temperature drop resulting from water evaporation from the biological material.
CA002161127A 1993-05-11 1994-05-10 Method and plant for solvent-free microwave extraction of natural products Expired - Fee Related CA2161127C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR9305810A FR2705035B1 (en) 1993-05-11 1993-05-11 Process and installation for solvent-free extraction of natural products by microwave.
FR93/05810 1993-05-11
PCT/FR1994/000551 WO1994026853A1 (en) 1993-05-11 1994-05-10 Method and plant for solvent-free microwave extraction of natural products

Publications (2)

Publication Number Publication Date
CA2161127A1 true CA2161127A1 (en) 1994-11-24
CA2161127C CA2161127C (en) 2005-09-27

Family

ID=9447117

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002161127A Expired - Fee Related CA2161127C (en) 1993-05-11 1994-05-10 Method and plant for solvent-free microwave extraction of natural products

Country Status (16)

Country Link
EP (1) EP0698076B1 (en)
JP (1) JPH08512337A (en)
CN (1) CN1059920C (en)
AT (1) ATE162211T1 (en)
AU (1) AU682035B2 (en)
BG (1) BG62367B1 (en)
BR (1) BR9406717A (en)
CA (1) CA2161127C (en)
DE (1) DE69407965T2 (en)
DK (1) DK0698076T3 (en)
ES (1) ES2114688T3 (en)
FR (1) FR2705035B1 (en)
GR (1) GR3026603T3 (en)
HU (1) HU218708B (en)
RU (1) RU2115700C1 (en)
WO (1) WO1994026853A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11702615B1 (en) 2022-03-09 2023-07-18 Chemtech Services, Inc. Microwave extraction of essential oils

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ATE272103T1 (en) * 2003-01-21 2004-08-15 Milestone Srl SOLVENT-FREE MICROWAVE EXTRACTION OF VOLATILE NATURAL SUBSTANCES
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WO2010098440A1 (en) * 2009-02-26 2010-09-02 日本かおり研究所株式会社 Monoterpene component-rich essential oil, method for producing same and method for remediating environmental pollutants using the essential oil
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JP2011052086A (en) * 2009-08-31 2011-03-17 Actree Corp Method for extracting oil and fat from bryophyte
FR2955331B1 (en) * 2010-01-15 2012-05-11 Archimex Pibs MICROWAVE ASSISTED BIOMASS EXTRACTION PROCESS AND INSTALLATION
JP6087485B2 (en) * 2010-02-25 2017-03-01 エステー株式会社 Fragrance composition and fragrance, deodorant and antibacterial agent using the same
FR2966700B1 (en) * 2010-10-29 2013-01-11 Bernard Mompon PROCESS FOR THE PRODUCTION OF PLANT-ORIGIN ARTICLES IMPREGNATED WITH PLANT LIQUID SUBSTANCE
TWI468506B (en) * 2011-01-17 2015-01-11 Nat Univ Chung Hsing The method and application of microwave-assisted extraction for microalgae lipid
CN102252889A (en) * 2011-03-15 2011-11-23 重庆大学 Microwave-assisted solvent-free solid-phase headspace extraction device and extraction method thereof
FR2975020B1 (en) 2011-05-13 2015-03-13 Univ D Avignon Et Des Pays De Vaucluse OBTAINING PLANT EXTRACT USING MICROWAVE
LV14481B (en) * 2011-11-21 2012-06-20 Latvijas Valsts Mežzinātnes Institūts 'silava' Method of production of water soluble and non-soluble essential oils from plant origin raw material
RU2473356C1 (en) * 2011-12-07 2013-01-27 Общество с ограниченной ответственностью "Компания Клевер" Method for preparing aqueous extracts of crude drugs rich in active extractants
US9486716B2 (en) * 2012-03-14 2016-11-08 State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University Essential oil extraction apparatus
FR3003181B1 (en) * 2013-03-18 2021-04-02 Innovation & Dev Company Idco PROCESS AND INSTALLATION FOR EXTRACTION OF BIOLOGICAL PRODUCTS BY MICROWAVE.
CN103194312A (en) * 2013-03-24 2013-07-10 西北农林科技大学 Method for extracting essential oil from cypress leaves
FR3013563B1 (en) * 2013-11-28 2017-06-30 Finat Conseil & Distrib PROCESS FOR MANUFACTURING NATURAL AND STABLE AROMATIZING PREPARATIONS AND AROMATIZING PREPARATIONS OBTAINED BY SAID METHOD
CN103725420B (en) * 2013-12-20 2016-07-13 江南大学 A kind of extract the method for Nigella damascena L. platymiscium Volatile Oil from Seed, device and application
FR3017308B1 (en) 2014-02-10 2022-06-17 Idco DEVICE AND METHOD FOR EXTRACTION OF BIOLOGICAL PRODUCTS BY MICROWAVES AND ULTRASOUNDS
CN103820218A (en) * 2014-03-07 2014-05-28 张家界金绿油脂有限责任公司 Method for microwave extracting rapeseed grease
JP5899604B2 (en) * 2014-03-24 2016-04-06 兼松エンジニアリング株式会社 Biomass recycling system using microwaves
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RO130896A0 (en) * 2015-01-19 2016-02-26 Mariana Pătraşcu Continuous flow reactor for microwave- and ultrasound-assisted extraction of biologically active compounds from plants
CN104711121A (en) * 2015-02-28 2015-06-17 湖北中烟工业有限责任公司 Method for extracting chrysanthemum indicum essential oil in ultrasonic-assisted solvent-free microwave extraction manner
CN104784965B (en) * 2015-04-20 2016-10-05 张新泉 A kind of microwave extracting device for Chinese medicine
RU2582292C1 (en) * 2015-05-07 2016-04-20 федеральное государственное автономное образовательное учреждение высшего образования "Российский университет дружбы народов" (РУДН) Method of extracting essential oil from medicinal plant material
CN105219526A (en) * 2015-09-25 2016-01-06 四川省林业科学研究院 A kind of yusho oil microwave extraction device and method
CN105213273B (en) * 2015-11-09 2018-11-13 北京工商大学 A kind of fresh and alive water of lemon and the preparation method and application thereof
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CN105713726A (en) * 2016-03-31 2016-06-29 李颖 Method and device for rapidly extracting natural plant essential oil and hydrolat without solvents
CN106190574A (en) * 2016-07-28 2016-12-07 河南科技学院 A kind of Atractylodes lancea (Thunb.) DC. volatile oil and preparation method thereof
JP2017008111A (en) * 2016-10-17 2017-01-12 エステー株式会社 Aromatic composition and aromatic agent using the same, deodorant and antibacterial agent
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US20200347318A1 (en) * 2017-08-31 2020-11-05 Firmenich Sa Microwave assisted extraction of essential oils from plant biomass
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FR3113248B1 (en) 2020-08-04 2022-08-05 Soc De Courtage Et De Diffusion Codif International Lavandula stoechas cell extract, compositions comprising it, cosmetic uses and method for culturing Lavandula stoechas cells.
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* Cited by examiner, † Cited by third party
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CA1336968C (en) * 1989-05-16 1995-09-12 J. R. Jocelyn Pare Microwave-assisted natural products extraction
SE9003593D0 (en) * 1990-11-12 1990-11-12 T G Owe Berg PROCEDURE FOR CONVERSION OF HEATS TO WORK
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11702615B1 (en) 2022-03-09 2023-07-18 Chemtech Services, Inc. Microwave extraction of essential oils

Also Published As

Publication number Publication date
AU682035B2 (en) 1997-09-18
BG100187A (en) 1996-05-31
DE69407965D1 (en) 1998-02-19
AU6725194A (en) 1994-12-12
CA2161127C (en) 2005-09-27
FR2705035B1 (en) 1995-08-04
FR2705035A1 (en) 1994-11-18
EP0698076B1 (en) 1998-01-14
HUT75578A (en) 1997-05-28
JPH08512337A (en) 1996-12-24
RU2115700C1 (en) 1998-07-20
CN1125461A (en) 1996-06-26
DK0698076T3 (en) 1998-09-14
DE69407965T2 (en) 1998-09-10
HU9503230D0 (en) 1996-01-29
GR3026603T3 (en) 1998-07-31
BR9406717A (en) 1996-02-06
BG62367B1 (en) 1999-09-30
ES2114688T3 (en) 1998-06-01
WO1994026853A1 (en) 1994-11-24
EP0698076A1 (en) 1996-02-28
HU218708B (en) 2000-11-28
ATE162211T1 (en) 1998-01-15
CN1059920C (en) 2000-12-27

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