ATE162211T1 - METHOD AND DEVICE FOR SOLVENT-FREE EXTRACTION OF NATURAL SUBSTANCES USING MICROWAVES - Google Patents

METHOD AND DEVICE FOR SOLVENT-FREE EXTRACTION OF NATURAL SUBSTANCES USING MICROWAVES

Info

Publication number
ATE162211T1
ATE162211T1 AT94915607T AT94915607T ATE162211T1 AT E162211 T1 ATE162211 T1 AT E162211T1 AT 94915607 T AT94915607 T AT 94915607T AT 94915607 T AT94915607 T AT 94915607T AT E162211 T1 ATE162211 T1 AT E162211T1
Authority
AT
Austria
Prior art keywords
solvent
biological material
microwaves
microwave radiation
natural substances
Prior art date
Application number
AT94915607T
Other languages
German (de)
Inventor
Philippe Mengal
Bernard Mompon
Original Assignee
Archimex Pibs
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Archimex Pibs filed Critical Archimex Pibs
Application granted granted Critical
Publication of ATE162211T1 publication Critical patent/ATE162211T1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/027—Recovery of volatiles by distillation or stripping

Abstract

The microwave extraction method involves the steps of placing the biological material in an enclosure without any solvent whatsoever and exposing it to microwave radiation to free at least some of the natural product, and then separating the residual biological material from the extracted natural product. Additionally, it involves the steps of applying reduced pressure in said enclosure during said microwave radiation stage and heating the enclosure during at least most of the microwave radiation stage to compensate the temperature drop resulting from water evaporation from the biological material.
AT94915607T 1993-05-11 1994-05-10 METHOD AND DEVICE FOR SOLVENT-FREE EXTRACTION OF NATURAL SUBSTANCES USING MICROWAVES ATE162211T1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9305810A FR2705035B1 (en) 1993-05-11 1993-05-11 Process and installation for solvent-free extraction of natural products by microwave.

Publications (1)

Publication Number Publication Date
ATE162211T1 true ATE162211T1 (en) 1998-01-15

Family

ID=9447117

Family Applications (1)

Application Number Title Priority Date Filing Date
AT94915607T ATE162211T1 (en) 1993-05-11 1994-05-10 METHOD AND DEVICE FOR SOLVENT-FREE EXTRACTION OF NATURAL SUBSTANCES USING MICROWAVES

Country Status (16)

Country Link
EP (1) EP0698076B1 (en)
JP (1) JPH08512337A (en)
CN (1) CN1059920C (en)
AT (1) ATE162211T1 (en)
AU (1) AU682035B2 (en)
BG (1) BG62367B1 (en)
BR (1) BR9406717A (en)
CA (1) CA2161127C (en)
DE (1) DE69407965T2 (en)
DK (1) DK0698076T3 (en)
ES (1) ES2114688T3 (en)
FR (1) FR2705035B1 (en)
GR (1) GR3026603T3 (en)
HU (1) HU218708B (en)
RU (1) RU2115700C1 (en)
WO (1) WO1994026853A1 (en)

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JP2011052086A (en) * 2009-08-31 2011-03-17 Actree Corp Method for extracting oil and fat from bryophyte
FR2955331B1 (en) * 2010-01-15 2012-05-11 Archimex Pibs MICROWAVE ASSISTED BIOMASS EXTRACTION PROCESS AND INSTALLATION
JP6087485B2 (en) * 2010-02-25 2017-03-01 エステー株式会社 Fragrance composition and fragrance, deodorant and antibacterial agent using the same
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TWI468506B (en) * 2011-01-17 2015-01-11 Nat Univ Chung Hsing The method and application of microwave-assisted extraction for microalgae lipid
CN102252889A (en) * 2011-03-15 2011-11-23 重庆大学 Microwave-assisted solvent-free solid-phase headspace extraction device and extraction method thereof
FR2975020B1 (en) 2011-05-13 2015-03-13 Univ D Avignon Et Des Pays De Vaucluse OBTAINING PLANT EXTRACT USING MICROWAVE
LV14481B (en) * 2011-11-21 2012-06-20 Latvijas Valsts Mežzinātnes Institūts 'silava' Method of production of water soluble and non-soluble essential oils from plant origin raw material
RU2473356C1 (en) * 2011-12-07 2013-01-27 Общество с ограниченной ответственностью "Компания Клевер" Method for preparing aqueous extracts of crude drugs rich in active extractants
US9486716B2 (en) * 2012-03-14 2016-11-08 State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University Essential oil extraction apparatus
FR3003181B1 (en) * 2013-03-18 2021-04-02 Innovation & Dev Company Idco PROCESS AND INSTALLATION FOR EXTRACTION OF BIOLOGICAL PRODUCTS BY MICROWAVE.
CN103194312A (en) * 2013-03-24 2013-07-10 西北农林科技大学 Method for extracting essential oil from cypress leaves
FR3013563B1 (en) * 2013-11-28 2017-06-30 Finat Conseil & Distrib PROCESS FOR MANUFACTURING NATURAL AND STABLE AROMATIZING PREPARATIONS AND AROMATIZING PREPARATIONS OBTAINED BY SAID METHOD
CN103725420B (en) * 2013-12-20 2016-07-13 江南大学 A kind of extract the method for Nigella damascena L. platymiscium Volatile Oil from Seed, device and application
FR3017308B1 (en) 2014-02-10 2022-06-17 Idco DEVICE AND METHOD FOR EXTRACTION OF BIOLOGICAL PRODUCTS BY MICROWAVES AND ULTRASOUNDS
CN103820218A (en) * 2014-03-07 2014-05-28 张家界金绿油脂有限责任公司 Method for microwave extracting rapeseed grease
JP5899604B2 (en) * 2014-03-24 2016-04-06 兼松エンジニアリング株式会社 Biomass recycling system using microwaves
TWI601565B (en) * 2014-06-05 2017-10-11 Timing Pharmaceutical Co Ltd Essential oil extraction device
CN104327951A (en) * 2014-10-23 2015-02-04 郑州工业应用技术学院 Hot air essential oil extraction device
CN104872605B (en) * 2014-12-08 2018-02-06 中国热带农业科学院南亚热带作物研究所 The method and liquid fumet of preparation solution fumet
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CN104711121A (en) * 2015-02-28 2015-06-17 湖北中烟工业有限责任公司 Method for extracting chrysanthemum indicum essential oil in ultrasonic-assisted solvent-free microwave extraction manner
CN104784965B (en) * 2015-04-20 2016-10-05 张新泉 A kind of microwave extracting device for Chinese medicine
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CN105713726A (en) * 2016-03-31 2016-06-29 李颖 Method and device for rapidly extracting natural plant essential oil and hydrolat without solvents
CN106190574A (en) * 2016-07-28 2016-12-07 河南科技学院 A kind of Atractylodes lancea (Thunb.) DC. volatile oil and preparation method thereof
JP2017008111A (en) * 2016-10-17 2017-01-12 エステー株式会社 Aromatic composition and aromatic agent using the same, deodorant and antibacterial agent
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RU2649024C1 (en) * 2017-01-10 2018-03-29 Федеральное государственное бюджетное образовательное учреждение высшего образования "Кубанский государственный технологический университет" (ФГБОУ ВО "КубГТУ") Method for obtaining the essential peppermint oil
FR3066703B1 (en) * 2017-05-24 2020-10-16 Erpim SOLID / LIQUID BACK-CURRENT EXTRACTION PROCESS AND DEVICE INCLUDING A DRYING STAGE
US20200347318A1 (en) * 2017-08-31 2020-11-05 Firmenich Sa Microwave assisted extraction of essential oils from plant biomass
FR3074425B1 (en) 2017-12-01 2020-09-04 Univ D'avignon Et Des Pays De Vaucluse DEVICE FOR EXTRACTION AND SEPARATION OF VOLATILE AND NON-VOLATILE COMPOUNDS OF A BIOLOGICAL MATERIAL AND ASSOCIATED PROCESS
JP6359752B1 (en) * 2017-12-22 2018-07-18 日本フレーバー工業株式会社 Manufacturing method of vanilla extract and vanilla extract
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CN110747060A (en) * 2019-10-21 2020-02-04 华侨大学 Method for extracting melaleuca alternifolia essential oil by ultrasonic-assisted solvent-free microwave
FR3113248B1 (en) 2020-08-04 2022-08-05 Soc De Courtage Et De Diffusion Codif International Lavandula stoechas cell extract, compositions comprising it, cosmetic uses and method for culturing Lavandula stoechas cells.
FR3115694B3 (en) 2020-10-30 2022-10-28 Soc De Courtage Et De Diffusion Codif International Active ingredient consisting of a bitter apple extract activating Tas2Rs bitterness receptors present on human skin and corresponding cosmetic and dermato-cosmetic uses.
CN116528664A (en) * 2020-12-08 2023-08-01 艾饰庭株式会社 Excrement treatment material and method for deodorizing excrement using same
CN116709910A (en) * 2021-01-28 2023-09-05 艾饰庭株式会社 Excrement treatment material and method for deodorizing excrement using same
CN113388459B (en) * 2021-05-26 2022-03-01 宁波芮颂生物科技有限公司 Preparation method of anti-cat and dog allergen finishing composition solution
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SE9003593D0 (en) * 1990-11-12 1990-11-12 T G Owe Berg PROCEDURE FOR CONVERSION OF HEATS TO WORK
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Also Published As

Publication number Publication date
AU682035B2 (en) 1997-09-18
BG100187A (en) 1996-05-31
DE69407965D1 (en) 1998-02-19
CA2161127A1 (en) 1994-11-24
AU6725194A (en) 1994-12-12
CA2161127C (en) 2005-09-27
FR2705035B1 (en) 1995-08-04
FR2705035A1 (en) 1994-11-18
EP0698076B1 (en) 1998-01-14
HUT75578A (en) 1997-05-28
JPH08512337A (en) 1996-12-24
RU2115700C1 (en) 1998-07-20
CN1125461A (en) 1996-06-26
DK0698076T3 (en) 1998-09-14
DE69407965T2 (en) 1998-09-10
HU9503230D0 (en) 1996-01-29
GR3026603T3 (en) 1998-07-31
BR9406717A (en) 1996-02-06
BG62367B1 (en) 1999-09-30
ES2114688T3 (en) 1998-06-01
WO1994026853A1 (en) 1994-11-24
EP0698076A1 (en) 1996-02-28
HU218708B (en) 2000-11-28
CN1059920C (en) 2000-12-27

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