ES2114688T3 - PROCEDURE AND INSTALLATION OF SOLVENT-FREE EXTRACTION OF NATURAL PRODUCTS BY MICROWAVE. - Google Patents

PROCEDURE AND INSTALLATION OF SOLVENT-FREE EXTRACTION OF NATURAL PRODUCTS BY MICROWAVE.

Info

Publication number
ES2114688T3
ES2114688T3 ES94915607T ES94915607T ES2114688T3 ES 2114688 T3 ES2114688 T3 ES 2114688T3 ES 94915607 T ES94915607 T ES 94915607T ES 94915607 T ES94915607 T ES 94915607T ES 2114688 T3 ES2114688 T3 ES 2114688T3
Authority
ES
Spain
Prior art keywords
microwave
solvent
procedure
installation
natural products
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94915607T
Other languages
Spanish (es)
Inventor
Philippe Mengal
Bernard Mompon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Archimex
Original Assignee
Archimex
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Archimex filed Critical Archimex
Application granted granted Critical
Publication of ES2114688T3 publication Critical patent/ES2114688T3/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/027—Recovery of volatiles by distillation or stripping

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Fats And Perfumes (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The microwave extraction method involves the steps of placing the biological material in an enclosure without any solvent whatsoever and exposing it to microwave radiation to free at least some of the natural product, and then separating the residual biological material from the extracted natural product. Additionally, it involves the steps of applying reduced pressure in said enclosure during said microwave radiation stage and heating the enclosure during at least most of the microwave radiation stage to compensate the temperature drop resulting from water evaporation from the biological material.
ES94915607T 1993-05-11 1994-05-10 PROCEDURE AND INSTALLATION OF SOLVENT-FREE EXTRACTION OF NATURAL PRODUCTS BY MICROWAVE. Expired - Lifetime ES2114688T3 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9305810A FR2705035B1 (en) 1993-05-11 1993-05-11 Process and installation for solvent-free extraction of natural products by microwave.

Publications (1)

Publication Number Publication Date
ES2114688T3 true ES2114688T3 (en) 1998-06-01

Family

ID=9447117

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94915607T Expired - Lifetime ES2114688T3 (en) 1993-05-11 1994-05-10 PROCEDURE AND INSTALLATION OF SOLVENT-FREE EXTRACTION OF NATURAL PRODUCTS BY MICROWAVE.

Country Status (16)

Country Link
EP (1) EP0698076B1 (en)
JP (1) JPH08512337A (en)
CN (1) CN1059920C (en)
AT (1) ATE162211T1 (en)
AU (1) AU682035B2 (en)
BG (1) BG62367B1 (en)
BR (1) BR9406717A (en)
CA (1) CA2161127C (en)
DE (1) DE69407965T2 (en)
DK (1) DK0698076T3 (en)
ES (1) ES2114688T3 (en)
FR (1) FR2705035B1 (en)
GR (1) GR3026603T3 (en)
HU (1) HU218708B (en)
RU (1) RU2115700C1 (en)
WO (1) WO1994026853A1 (en)

Families Citing this family (63)

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FR2763795B1 (en) * 1997-05-30 1999-08-20 Archimex Pibs PROCESS FOR THE PREPARATION OF PLANTS SUCH AS SPICES, AROMATIC PLANTS AND AROMATOES
FR2793008B1 (en) 1999-04-30 2001-07-27 Valeurs Bois Ind PROCESS FOR THE EXTRACTION OF NATURAL JUICE FROM WOODY PLANT MATERIAL, DEVICE FOR CARRYING OUT THE PROCESS AND USE OF THE PROCESS FOR THE PRODUCTION OF DRY WOODY PLANT
FR2787347B1 (en) * 1998-12-17 2001-01-19 Gattefosse Ets Sa METHOD FOR MANUFACTURING AN EMULSION BASED ON AROMATIC PLANT MATERIAL, EMULSION LIKELY TO BE OBTAINED BY SAID METHOD AND USE OF SAID EMULSION
CN1112953C (en) * 1999-10-29 2003-07-02 汤大卫 Process for liquid/sodid extraction
CN1120736C (en) * 2000-09-14 2003-09-10 中国科学院山西煤炭化学研究所 Extraction process for industrial solid material
EP1439218B1 (en) * 2003-01-21 2004-07-28 Milestone S.r.l. Solvent-free microwave extraction of volatile natural compounds
EP1629725B1 (en) * 2004-07-20 2007-09-12 Milestone S.r.l. Microwave extraction of volatile natural substances
CN100379754C (en) * 2004-11-22 2008-04-09 王煊 Extraction of saponin by non-solvent microwave heat
CN100421759C (en) * 2006-03-10 2008-10-01 山东轻工业学院 Decompressed microwave extraction device and method for extracting plant effective ingredient
EP2011568B1 (en) * 2006-03-16 2016-08-24 Universidad Tecnica Federico Santa Maria (Usm) Device for extraction of organic chemical compounds with toxic properties that are present in atmospheric samples, using focused-microwave-heated solvents in open (non-pressurized) systems
CN101290277B (en) * 2007-04-20 2011-05-11 财团法人食品工业发展研究所 Rapid extraction method utilizing microwave radiation
TW200842336A (en) * 2007-04-26 2008-11-01 Food Industry Res & Dev Inst Microwave accelerating extraction equipment
FR2925898A1 (en) * 2007-12-28 2009-07-03 Jean Pierre Lablanchy Extracting an essential oil having high content of thymoquinone from a part of Nigella sativa plant, comprises extracting aromatic water comprising essential oil using combination of microwave and impulse vacuum
JP5508388B2 (en) * 2009-02-26 2014-05-28 エステー株式会社 High monoterpene component-containing essential oil, method for producing the same, and method for purifying environmental pollutants using the essential oil
RU2395766C1 (en) * 2009-05-25 2010-07-27 Закрытое Акционерное Общество "Твин Трейдинг Компани" Drying method of materials of vegetable, animal origin, fish and seafood, and device for its implementation
JP2011052086A (en) * 2009-08-31 2011-03-17 Actree Corp Method for extracting oil and fat from bryophyte
FR2955331B1 (en) * 2010-01-15 2012-05-11 Archimex Pibs MICROWAVE ASSISTED BIOMASS EXTRACTION PROCESS AND INSTALLATION
JP6087485B2 (en) * 2010-02-25 2017-03-01 エステー株式会社 Fragrance composition and fragrance, deodorant and antibacterial agent using the same
FR2966700B1 (en) * 2010-10-29 2013-01-11 Bernard Mompon PROCESS FOR THE PRODUCTION OF PLANT-ORIGIN ARTICLES IMPREGNATED WITH PLANT LIQUID SUBSTANCE
TWI468506B (en) * 2011-01-17 2015-01-11 Nat Univ Chung Hsing The method and application of microwave-assisted extraction for microalgae lipid
CN102252889A (en) * 2011-03-15 2011-11-23 重庆大学 Microwave-assisted solvent-free solid-phase headspace extraction device and extraction method thereof
FR2975020B1 (en) 2011-05-13 2015-03-13 Univ D Avignon Et Des Pays De Vaucluse OBTAINING PLANT EXTRACT USING MICROWAVE
LV14481B (en) * 2011-11-21 2012-06-20 Latvijas Valsts Mežzinātnes Institūts 'silava' Method of production of water soluble and non-soluble essential oils from plant origin raw material
RU2473356C1 (en) * 2011-12-07 2013-01-27 Общество с ограниченной ответственностью "Компания Клевер" Method for preparing aqueous extracts of crude drugs rich in active extractants
US9486716B2 (en) 2012-03-14 2016-11-08 State Of Oregon Acting By And Through The State Board Of Higher Education On Behalf Of Oregon State University Essential oil extraction apparatus
FR3003181B1 (en) * 2013-03-18 2021-04-02 Innovation & Dev Company Idco PROCESS AND INSTALLATION FOR EXTRACTION OF BIOLOGICAL PRODUCTS BY MICROWAVE.
CN103194312A (en) * 2013-03-24 2013-07-10 西北农林科技大学 Method for extracting essential oil from cypress leaves
FR3013563B1 (en) * 2013-11-28 2017-06-30 Finat Conseil & Distrib PROCESS FOR MANUFACTURING NATURAL AND STABLE AROMATIZING PREPARATIONS AND AROMATIZING PREPARATIONS OBTAINED BY SAID METHOD
CN103725420B (en) * 2013-12-20 2016-07-13 江南大学 A kind of extract the method for Nigella damascena L. platymiscium Volatile Oil from Seed, device and application
FR3017308B1 (en) 2014-02-10 2022-06-17 Idco DEVICE AND METHOD FOR EXTRACTION OF BIOLOGICAL PRODUCTS BY MICROWAVES AND ULTRASOUNDS
CN103820218A (en) * 2014-03-07 2014-05-28 张家界金绿油脂有限责任公司 Method for microwave extracting rapeseed grease
JP5899604B2 (en) * 2014-03-24 2016-04-06 兼松エンジニアリング株式会社 Biomass recycling system using microwaves
TWI601565B (en) * 2014-06-05 2017-10-11 Timing Pharmaceutical Co Ltd Essential oil extraction device
CN104327951A (en) * 2014-10-23 2015-02-04 郑州工业应用技术学院 Hot air essential oil extraction device
CN104872605B (en) * 2014-12-08 2018-02-06 中国热带农业科学院南亚热带作物研究所 The method and liquid fumet of preparation solution fumet
RO130896A0 (en) * 2015-01-19 2016-02-26 Mariana Pătraşcu Continuous flow reactor for microwave- and ultrasound-assisted extraction of biologically active compounds from plants
CN104711121A (en) * 2015-02-28 2015-06-17 湖北中烟工业有限责任公司 Method for extracting chrysanthemum indicum essential oil in ultrasonic-assisted solvent-free microwave extraction manner
CN104784965B (en) * 2015-04-20 2016-10-05 张新泉 A kind of microwave extracting device for Chinese medicine
RU2582292C1 (en) * 2015-05-07 2016-04-20 федеральное государственное автономное образовательное учреждение высшего образования "Российский университет дружбы народов" (РУДН) Method of extracting essential oil from medicinal plant material
CN105219526A (en) * 2015-09-25 2016-01-06 四川省林业科学研究院 A kind of yusho oil microwave extraction device and method
CN105232782B (en) * 2015-11-09 2019-11-22 北京工商大学 A kind of fresh and alive water of fresh tea and the preparation method and application thereof
CN105213273B (en) * 2015-11-09 2018-11-13 北京工商大学 A kind of fresh and alive water of lemon and the preparation method and application thereof
CN105213272B (en) * 2015-11-09 2019-02-01 北京工商大学 A kind of fresh and alive water of lavender and the preparation method and application thereof
CN105232400B (en) * 2015-11-09 2018-11-02 北京工商大学 A kind of fresh and alive water of jasmine and the preparation method and application thereof
CN105250180B (en) * 2015-11-09 2018-11-27 北京工商大学 A kind of fresh and alive water of rose and the preparation method and application thereof
CN105713726A (en) * 2016-03-31 2016-06-29 李颖 Method and device for rapidly extracting natural plant essential oil and hydrolat without solvents
CN106190574A (en) * 2016-07-28 2016-12-07 河南科技学院 A kind of Atractylodes lancea (Thunb.) DC. volatile oil and preparation method thereof
JP2017008111A (en) * 2016-10-17 2017-01-12 エステー株式会社 Aromatic composition and aromatic agent using the same, deodorant and antibacterial agent
RU2636155C1 (en) * 2016-12-20 2017-11-21 Федеральное Государственное Бюджетное Образовательное Учреждение Высшего Образования "Нижегородская Государственная Сельскохозяйственная Академия" (ФГБОУ ВО НГСХА) Microwave technology for extracting fat from fat-containing raw materials
RU2649024C1 (en) * 2017-01-10 2018-03-29 Федеральное государственное бюджетное образовательное учреждение высшего образования "Кубанский государственный технологический университет" (ФГБОУ ВО "КубГТУ") Method for obtaining the essential peppermint oil
FR3066703B1 (en) * 2017-05-24 2020-10-16 Erpim SOLID / LIQUID BACK-CURRENT EXTRACTION PROCESS AND DEVICE INCLUDING A DRYING STAGE
WO2019043058A1 (en) 2017-08-31 2019-03-07 Firmenich Sa Microwave assisted extraction of essential oils from plant biomass
FR3074425B1 (en) 2017-12-01 2020-09-04 Univ D'avignon Et Des Pays De Vaucluse DEVICE FOR EXTRACTION AND SEPARATION OF VOLATILE AND NON-VOLATILE COMPOUNDS OF A BIOLOGICAL MATERIAL AND ASSOCIATED PROCESS
JP6359752B1 (en) * 2017-12-22 2018-07-18 日本フレーバー工業株式会社 Manufacturing method of vanilla extract and vanilla extract
FR3099991B1 (en) 2019-08-22 2023-12-22 Soc De Courtage Et De Diffusion Codif International Cosmetic composition ingredient for sensitive scalp
CN110747060A (en) * 2019-10-21 2020-02-04 华侨大学 Method for extracting melaleuca alternifolia essential oil by ultrasonic-assisted solvent-free microwave
FR3113248B1 (en) 2020-08-04 2022-08-05 Soc De Courtage Et De Diffusion Codif International Lavandula stoechas cell extract, compositions comprising it, cosmetic uses and method for culturing Lavandula stoechas cells.
FR3115694B3 (en) 2020-10-30 2022-10-28 Soc De Courtage Et De Diffusion Codif International Active ingredient consisting of a bitter apple extract activating Tas2Rs bitterness receptors present on human skin and corresponding cosmetic and dermato-cosmetic uses.
CN116528664A (en) * 2020-12-08 2023-08-01 艾饰庭株式会社 Excrement treatment material and method for deodorizing excrement using same
CN112760166A (en) * 2021-01-08 2021-05-07 四川轻化工大学 Rattan pepper oil production facility
WO2022163063A1 (en) * 2021-01-28 2022-08-04 エステー株式会社 Excrement treatment material and excrement deodorization method using same
CN113388459B (en) * 2021-05-26 2022-03-01 宁波芮颂生物科技有限公司 Preparation method of anti-cat and dog allergen finishing composition solution
US11702615B1 (en) 2022-03-09 2023-07-18 Chemtech Services, Inc. Microwave extraction of essential oils

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA1336968C (en) * 1989-05-16 1995-09-12 J. R. Jocelyn Pare Microwave-assisted natural products extraction
SE9003593D0 (en) * 1990-11-12 1990-11-12 T G Owe Berg PROCEDURE FOR CONVERSION OF HEATS TO WORK
EP0485668B1 (en) * 1990-11-16 1996-01-17 Her Majesty The Queen In Right Of Canada As Represented By The Minister Of The Environment Microwave extraction of volatile oils and apparatus therefor

Also Published As

Publication number Publication date
BR9406717A (en) 1996-02-06
RU2115700C1 (en) 1998-07-20
HU9503230D0 (en) 1996-01-29
FR2705035A1 (en) 1994-11-18
JPH08512337A (en) 1996-12-24
BG100187A (en) 1996-05-31
EP0698076B1 (en) 1998-01-14
DK0698076T3 (en) 1998-09-14
DE69407965D1 (en) 1998-02-19
GR3026603T3 (en) 1998-07-31
AU682035B2 (en) 1997-09-18
EP0698076A1 (en) 1996-02-28
AU6725194A (en) 1994-12-12
HUT75578A (en) 1997-05-28
HU218708B (en) 2000-11-28
FR2705035B1 (en) 1995-08-04
CN1125461A (en) 1996-06-26
CN1059920C (en) 2000-12-27
DE69407965T2 (en) 1998-09-10
WO1994026853A1 (en) 1994-11-24
CA2161127C (en) 2005-09-27
ATE162211T1 (en) 1998-01-15
CA2161127A1 (en) 1994-11-24
BG62367B1 (en) 1999-09-30

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