CN105213272B - A kind of fresh and alive water of lavender and the preparation method and application thereof - Google Patents
A kind of fresh and alive water of lavender and the preparation method and application thereof Download PDFInfo
- Publication number
- CN105213272B CN105213272B CN201510755241.1A CN201510755241A CN105213272B CN 105213272 B CN105213272 B CN 105213272B CN 201510755241 A CN201510755241 A CN 201510755241A CN 105213272 B CN105213272 B CN 105213272B
- Authority
- CN
- China
- Prior art keywords
- lavender
- fresh
- water
- preparation
- product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 244000178870 Lavandula angustifolia Species 0.000 title claims abstract description 82
- 235000010663 Lavandula angustifolia Nutrition 0.000 title claims abstract description 82
- 239000001102 lavandula vera Substances 0.000 title claims abstract description 82
- 235000018219 lavender Nutrition 0.000 title claims abstract description 82
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 241000628997 Flos Species 0.000 claims abstract description 17
- 239000002537 cosmetic Substances 0.000 claims abstract description 14
- 230000036541 health Effects 0.000 claims abstract description 12
- 235000013305 food Nutrition 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 11
- 230000002087 whitening effect Effects 0.000 claims abstract description 9
- 102000003425 Tyrosinase Human genes 0.000 claims abstract description 8
- 108060008724 Tyrosinase Proteins 0.000 claims abstract description 8
- 150000003254 radicals Chemical class 0.000 claims abstract description 7
- 230000003712 anti-aging effect Effects 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims description 27
- 238000005292 vacuum distillation Methods 0.000 claims description 8
- 239000000470 constituent Substances 0.000 claims description 6
- 230000001815 facial effect Effects 0.000 claims description 5
- 238000009499 grossing Methods 0.000 claims description 4
- 239000000126 substance Substances 0.000 abstract description 13
- 239000003960 organic solvent Substances 0.000 abstract description 6
- 230000003078 antioxidant effect Effects 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 5
- 239000012752 auxiliary agent Substances 0.000 abstract description 3
- 239000000284 extract Substances 0.000 description 8
- 238000004821 distillation Methods 0.000 description 7
- 239000011149 active material Substances 0.000 description 6
- 230000001954 sterilising effect Effects 0.000 description 6
- 125000003118 aryl group Chemical group 0.000 description 5
- 238000009835 boiling Methods 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 238000005165 17O NMR spectroscopy Methods 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 230000007760 free radical scavenging Effects 0.000 description 4
- 230000005764 inhibitory process Effects 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 238000004321 preservation Methods 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- DOUMFZQKYFQNTF-WUTVXBCWSA-N (R)-rosmarinic acid Chemical compound C([C@H](C(=O)O)OC(=O)\C=C\C=1C=C(O)C(O)=CC=1)C1=CC=C(O)C(O)=C1 DOUMFZQKYFQNTF-WUTVXBCWSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 238000005481 NMR spectroscopy Methods 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 235000013334 alcoholic beverage Nutrition 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 235000015203 fruit juice Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000004089 microcirculation Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 238000000194 supercritical-fluid extraction Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 1
- 208000000059 Dyspnea Diseases 0.000 description 1
- 206010013975 Dyspnoeas Diseases 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 description 1
- 235000002997 Lavandula Nutrition 0.000 description 1
- 241001529749 Lavandula Species 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- 206010033557 Palpitations Diseases 0.000 description 1
- 241001529246 Platymiscium Species 0.000 description 1
- ZZAFFYPNLYCDEP-HNNXBMFYSA-N Rosmarinsaeure Natural products OC(=O)[C@H](Cc1cccc(O)c1O)OC(=O)C=Cc2ccc(O)c(O)c2 ZZAFFYPNLYCDEP-HNNXBMFYSA-N 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- -1 alcohol ester Chemical class 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 125000006267 biphenyl group Chemical group 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000001819 mass spectrum Methods 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- DOUMFZQKYFQNTF-MRXNPFEDSA-N rosemarinic acid Natural products C([C@H](C(=O)O)OC(=O)C=CC=1C=C(O)C(O)=CC=1)C1=CC=C(O)C(O)=C1 DOUMFZQKYFQNTF-MRXNPFEDSA-N 0.000 description 1
- TVHVQJFBWRLYOD-UHFFFAOYSA-N rosmarinic acid Natural products OC(=O)C(Cc1ccc(O)c(O)c1)OC(=Cc2ccc(O)c(O)c2)C=O TVHVQJFBWRLYOD-UHFFFAOYSA-N 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 208000013220 shortness of breath Diseases 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Food Science & Technology (AREA)
- Birds (AREA)
- Botany (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Genetics & Genomics (AREA)
- Microbiology (AREA)
- Epidemiology (AREA)
- Biotechnology (AREA)
- Zoology (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Polymers & Plastics (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses fresh and alive water of a kind of lavender and the preparation method and application thereof.The preparation method of the fresh and alive water of lavender of the present invention, includes the following steps: for lavandulae flos to be placed in reactor, vacuumize；Then it is evaporated under reduced pressure, collects condensate liquid to get the fresh and alive water of lavender is arrived.Application of the fresh and alive water of lavender of the present invention in the product that preparation has following at least one functions: 1) whitening；2) anti-aging；3) free radical is removed；4) inhibit tyrosinase.Natural lavender bud is used only in preparation method raw material of the present invention, and water is not added in preparation process, any chemical organic solvent and auxiliary agent is not added, the fresh and alive water pure in smell of obtained lavender of the present invention, strong not to be pungent, safety, antioxidant activity is strong, can apply in food, health care product and cosmetics.
Description
Technical field
The present invention relates to fresh and alive water of a kind of lavender and the preparation method and application thereof, belong to food, health care product and cosmetics
Field.
Background technique
Lavender (Lavender) is Chun Xing section lavender platymiscium, is perennial undershrub.China lavender it is main
There are the ground such as Xinjiang, Shaanxi in cultivation area.Lavender is precious Chinese medicine and food flavor.Some researches show that narrow-leaved lavenders to mention
Take object that can inhibit the peroxidating of lipid, wherein phenols component Rosmarinic acid is anti-oxidation active substance.Lavender or Xinjiang
Traditional medication of Uygur medicine, tie up it is medical it come treat chest and abdomen swelling and pain, flu cough and asthma, dizziness headache, shortness of breath and palpitation, joint ostalgia
Deng.
However, currently, current slave aromatics plant extract active material in the world, such as extract and smoke from lavandulae flos
The method of clothing showy flowers of herbaceous plants extract, substantially there are three types of: the most-often used method in the first and this field is " water-boiling method ", will be new
Fresh lavandulae flos are packed into distillation still, and a certain proportion of water is added, bottom is passed through the water boiling being steam heated in kettle, spend
Aromatic substance evaporates together with water vapour, is imported by conduit cooling in condenser.Main problem existing for water-boiling method is long-time
Thermophilic digestion, so that the fragrant alcohol ester of lavandulae flos morphs, extracted active material, not no natural scents of fresh flower,
But giving off a strong fragrance is pungent, smell is impure, and in production process, equipment is more, and energy consumption is high, and operator is more, low efficiency, the pollution of raffinate residue
Discharge amount is big, need to consume a large amount of steam and cooling water.Second is " solvent extraction ", using organic solvent, such as alcohol, ether
Or liquefied butane etc., by organic solvent, sprinkle dissolves in the aromatic substance in spending described molten on fresh lavandulae flos repeatedly
In agent, the method for then using low temperature distillation extracts the aromatic substance in lavandulae flos.Main problem existing for solvent extraction
It is equipment, complex process, also needs consumption steam and cooling water, due to using organic solvent, investment is big, low output, and easily to work
Property substance pollutes, and oil yield is low, and the active material isolated is impure.The third is " carbon dioxide supercritical extraction method ",
Extraction process is to utilize CO2In low temperature critical environment, the aromatic substance in lavandulae flos is extracted, technique adaptation smokes
The cryogenic aroma characteristic of the clothing showy flowers of herbaceous plants, the active material of extraction, fragrance is pure, closely similar with fresh flower.CO 2 supercritical extraction
The main problem followed the example of is that equipment, technique are extremely complex, and working ability is low, and equipment investment is expensive, and there is also waste sludge discharge pollutions
Environment, the method only exists in laboratory stage at present, and enterprise there is no to use the precedent of this method batch production.
Summary of the invention
The object of the present invention is to provide fresh and alive water of a kind of lavender and the preparation method and application thereof.Preparation method of the present invention is former
Natural lavender bud is used only in material, and water is not added in preparation process, any chemical organic solvent and auxiliary agent is not added, obtained sheet
The fresh and alive water pure in smell of invention lavender, strong not to be pungent, safety, antioxidant activity is strong, can be in food, health care product and cosmetics
Middle application.
The preparation method of the fresh and alive water of lavender provided by the invention, includes the following steps: lavandulae flos being placed in reactor
In, it vacuumizes；Then it is evaporated under reduced pressure, collects condensate liquid to get the fresh and alive water of lavender is arrived.
In above-mentioned method, the temperature of the vacuum distillation is 65~75 DEG C, concretely 65 DEG C, 70 DEG C or 75 DEG C；
The time of the vacuum distillation is 1.5~2.5h, concretely 2h, 2.5h or 2~2.5h.
In above-mentioned method, the vacuum degree of the vacuum distillation is 60~100Pa, concretely 60Pa, 75Pa or
100Pa；
The reactor is Rotary Evaporators.
In the present invention, the lavandulae flos are lavender flower and/or lavender bud.
The present invention also provides the fresh and alive water of the lavender of above-mentioned method preparation.
Invention further provides the fresh and alive water of above-mentioned lavender in the product that preparation has following at least one functions
Application:
1) whitening；
2) anti-aging；
3) free radical is removed；
4) inhibit tyrosinase.
In above-mentioned application, the product is at least one of cosmetics, food and health care product.
In above-mentioned application, the cosmetics are any one of facial mask, Essence, toner and smoothing toner.
The present invention also provides the product with following at least one functions, the active constituent of the product is the lavender
Fresh and alive water:
1) whitening；
2) anti-aging；
3) free radical is removed；
4) inhibit tyrosinase.
In above-mentioned product, the product is at least one of cosmetics, food and health care product；
The cosmetics are any one of facial mask, Essence, toner and smoothing toner.
In above-mentioned product, the mass percentage of the addition of the lavender active water in said products is 1~
100%.
Concrete application of the fresh and alive water of lavender of the present invention in cosmetics, food and health care product is as follows:
1, as drink, the effect of long-term drinking can increase skin vitality, color spot of dispelling, dispersing stagnated hepatoqi, activating microcirculation and removing stasis medicinal；
2, the effect of pure milk is drunk, can reach fragrant body, color spot of dispelling, dispersing stagnated hepatoqi, activating microcirculation and removing stasis medicinal is added；
3, the fresh and alive water of lavender of the present invention and its drinks cooperate, and make lavender alcoholic drink mixed with fruit juice, can effectively improve lavender alcoholic drink mixed with fruit juice
In beneficial human health microelement, the especially content of strontium, metasilicic acid；As Tonic liquor, effect is more preferable.
4, lavipeditum: the fresh and alive water of lavender and water quality ratio are 1: 100, can steep foot every night；
5, it can be used as the ingredient of facial mask, Essence, toner, smoothing toner, effect on the skin, can effectively provide body institute
The element of several beneficial human healths of ten needed.
The invention has the following advantages that
The raw material that preparation method of the present invention uses is natural lavender bud, does not add water in preparation process, spy is not added
Any chemical organic solvent and auxiliary agent, the fresh and alive water security nonhazardous of the lavender of extraction is not added in different gas；Using Rotary Evaporators
The method of vacuum distillation, the bioactive substance that can be extracted from lavender bud, the fresh and alive water of obtained lavender keep it
Naturally fragrance, and pure in smell is strong not to be pungent, and process equipment is small in size, simple process, high-efficient, low in energy consumption, automation
Degree is high, and operator is few, easy to operate, and the rate of output is high, without any disposal of pollutants, does not need to build boiler etc., passes through the party
The fresh and alive water active material of lavender that method is extracted is more.The antioxidant activity of the fresh and alive water of lavender of the present invention is strong, and white-skinned face function is good, energy
Play the role of health care, beauty, improves the immunity of body；Without additive (such as pigment), safety meets green food, protects
The requirement of strong product and cosmetics can be used as food, health care product and cosmetics, be the extraction of lavandulae flos active constituent and opened
Hair, which utilizes, provides a kind of new approach.
Detailed description of the invention
Fig. 1 is lavandulae flos extract DPPH free radical scavenging activity in the embodiment of the present invention 1.
Fig. 2 is lavandulae flos extract DPPH free radical scavenging activity in the embodiment of the present invention 2.
Fig. 3 is lavandulae flos extract DPPH free radical scavenging activity in the embodiment of the present invention 3.
Fig. 4 is the lavandulae flos extract that different preparation methods obtain17O-NMR detects spectrogram, and Fig. 4 (a) is commonly to distill
Lavender liquid17O-NMR spectrogram (Hw=71.66Hz)；Fig. 4 (b) is the fresh and alive water of lavender in the embodiment of the present invention 117O-NMR inspection
It surveys spectrogram (Hw=63.76Hz).
Fig. 5 is extract mass spectrum test map in lavandulae flos in the embodiment of the present invention 1.
Specific embodiment
Experimental method used in following embodiments is conventional method unless otherwise specified.
The materials, reagents and the like used in the following examples is commercially available unless otherwise specified.
The fresh and alive water of embodiment 1, lavender
The present invention is made of the raw material of following weight: 1 kilogram of the fresh flower flower bud of lavender, carries out according to following technique:
The fresh flower flower bud of lavender is put into Rotary Evaporators, is vacuumized (vacuum degree 75Pa), 70 DEG C, distillation 2.5 is small
When, obtain 0.8 kilogram of the fresh and alive water of lavender.
The sterilization of the fresh and alive water of lavender of the present invention and preservation: held by being stored in stainless steel after ultraviolet-ray sterilizing
In device or edible plastic containers, it is protected from light, low temperature, is sealed.
The fresh and alive water of embodiment 2, lavender
The present invention is made of the raw material of following weight: 1 kilogram of the fresh flower flower bud of lavender, carries out according to following technique:
The fresh flower flower bud of lavender is put into Rotary Evaporators, is vacuumized (vacuum degree 60Pa), 65 DEG C, is distilled 2 hours,
Obtain 0.78 kilogram of the fresh and alive water of lavender.
The sterilization of the fresh and alive water of lavender of the present invention and preservation: held by being stored in stainless steel after ultraviolet-ray sterilizing
In device or edible plastic containers, it is protected from light, low temperature, is sealed.
The fresh and alive water of embodiment 3, lavender
The present invention is made of the raw material of following weight: 1 kilogram of the fresh flower piece of lavender, carries out according to following technique:
The fresh flower piece of lavender is put into Rotary Evaporators, is vacuumized (vacuum degree 100Pa), 75 DEG C, distillation 1.5 is small
When, obtain 0.76 kilogram of the fresh and alive water of lavender.
The sterilization of the fresh and alive water of lavender of the present invention and preservation: held by being stored in stainless steel after ultraviolet-ray sterilizing
In device or edible plastic containers, it is protected from light, low temperature, is sealed.
The outer whitening experiment of the fresh and alive water body of embodiment 4, lavender
The external whitening experiment of the fresh and alive water of lavender of 1-3 of embodiment of the present invention preparation is carried out using inhibition tyrosine enzyme process
Measurement, measurement result are as shown in table 1.As shown in Table 1, the tyrosinase inhibition rate of the fresh and alive water of lavender of the present invention be 12.64~
15.96%, than the tyrosinase inhibition rate 4.38% for commonly distilling lavender liquid in comparative example, 8.26~11.58% are improved,
Illustrate that the fresh and alive water of lavender of the present invention improves three times than commonly distilling the external whitening effect of lavender liquid.
1 whitening function of table analysis -- tyrosinase Inhibition test
The fresh and alive water Antioxidation in vitro of embodiment 5, lavender
The measurement that the fresh and alive water of lavender of 1-3 of embodiment of the present invention preparation acts on DPPH radicals scavenging, DPPH (1,1-
Disphenyl-2-picry1-hydrazy1), chemical name 1,1 diphenyl -2- trinitrophenyl-hydrazine, molecular formula are (C6H5)2N-NC6H5(NO2)3, there is not pairs of valence electron in this compound on an atom of nitrogen bridge, and the track of this electronics
Movement is almost offset by molecular structure, usually to capture DPPH free radical as the index of evaluation oxidation resistance, measurement knot
Measurement result in fruit such as table 2 and embodiment 1-3 respectively is as shown in Figs. 1-3.By table 2 and Fig. 1-3 it is found that lavender of the present invention is fresh
The DPPH free radical scavenging activity (IC50) of running water is higher than the measured value of common distillation lavender liquid, illustrates that lavender of the present invention is fresh
The antioxidant activity of running water is higher.
2 antioxidant activity of table
Embodiment 4: the fresh and alive water active material analysis of lavender
Pass through lavender liquid is commonly distilled in the fresh and alive water of the lavender prepared in the embodiment of the present invention 1 and comparative example17O-
NMR (nuclear magnetic resonance), Mass Spectrometer Method analysis, micel size are shown in Table 3, and the fresh and alive water aroma substance composition analysis of lavender is shown in Table
4,17O-NMR (nuclear magnetic resonance), Mass Spectrometer Method map are shown in Figure 4 and 5.By above-mentioned table 3,4 and Fig. 4,5 it is found that lavender of the present invention is fresh
The ratio of components of its active constituent of running water commonly distills that lavender liquid active constituent is significantly different, point of the fresh and alive water of lavender of the present invention
Son group is smaller, is easy to be absorbed by organism, and active constituent type is abundant, is rich in various active substance.
3 micel size of table
The fresh and alive water aroma substance composition of 4 lavender of table
Comparative example 1,
The preparation of common distillation lavender liquid:
Using this field most-often used " water-boiling method ", 1 kilogram of the fresh flower flower bud of lavender and water are placed in distillation still often
Pressure is heated to 100~110 DEG C to boiling, and the aromatic substance in lavandulae flos evaporates together with water vapour, is imported and is condensed by conduit
It is cooled down in device to get common distillation lavender liquid.
Claims (8)
1. a kind of preparation method of the fresh and alive water of lavender is following steps: lavandulae flos being placed in reactor, are vacuumized；So
After be evaporated under reduced pressure, collect condensate liquid to get arrive the fresh and alive water of lavender；
The temperature of the vacuum distillation is 65~75 DEG C；
The time of the vacuum distillation is 1.5~2.5h；
The vacuum degree of the vacuum distillation is 60~100Pa；
The reactor is Rotary Evaporators.
2. the fresh and alive water of the lavender of method preparation described in claim 1.
3. application of the fresh and alive water of lavender described in claim 2 in the product that preparation has following at least one functions:
1) whitening；
2) anti-aging；
3) free radical is removed；
4) inhibit tyrosinase.
4. application according to claim 3, it is characterised in that: the product be cosmetics, food and health care product in extremely
Few one kind.
5. application according to claim 4, it is characterised in that: the cosmetics are facial mask, Essence, toner and skin softening
Any one of water.
6. a kind of product with following at least one functions, the active constituent of the product is that lavender described in claim 2 is fresh
Running water:
1) whitening；
2) anti-aging；
3) free radical is removed；
4) inhibit tyrosinase.
7. product according to claim 6, it is characterised in that: the product be cosmetics, food and health care product in extremely
Few one kind；
The cosmetics are any one of facial mask, Essence, toner and smoothing toner.
8. product according to claim 6 or 7, it is characterised in that: the lavender active water adding in said products
The mass percentage added is 1~100%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510755241.1A CN105213272B (en) | 2015-11-09 | 2015-11-09 | A kind of fresh and alive water of lavender and the preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510755241.1A CN105213272B (en) | 2015-11-09 | 2015-11-09 | A kind of fresh and alive water of lavender and the preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105213272A CN105213272A (en) | 2016-01-06 |
| CN105213272B true CN105213272B (en) | 2019-02-01 |
Family
ID=54982798
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510755241.1A Active CN105213272B (en) | 2015-11-09 | 2015-11-09 | A kind of fresh and alive water of lavender and the preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105213272B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107951830A (en) * | 2017-12-07 | 2018-04-24 | 广州赛莱拉干细胞科技股份有限公司 | Rosemary stem cell extract antioxidant composition and the skin care item containing said composition |
| CN108434035A (en) * | 2018-05-21 | 2018-08-24 | 杭州千岛湖蓝色天使实业有限公司 | It is a kind of to moisten smooth active essence cream and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1125461A (en) * | 1993-05-11 | 1996-06-26 | 阿奇麦克斯 | Method and plant for solvent-free microwave extraction of natural products |
| CN1693438A (en) * | 2005-05-12 | 2005-11-09 | 中国科学院广州化学研究所 | Process for extracting and refining lavender oil |
| CN1994269A (en) * | 2006-12-28 | 2007-07-11 | 上海交通大学 | Method for preparing fragrant lavender liquid |
| CN102379834B (en) * | 2011-10-31 | 2013-05-22 | 上海交通大学 | Scent plant extractive for comprehensively conditioning skin around eyes and eye care product thereof |
| CN103173287A (en) * | 2013-04-23 | 2013-06-26 | 四川紫颐天堂香草科技开发有限公司 | Method for extracting lavender essential oil |
| CN103385832A (en) * | 2013-07-24 | 2013-11-13 | 云南西草资源开发有限公司 | Anti-aging cosmetic taking lavender extract as main active ingredient |
-
2015
- 2015-11-09 CN CN201510755241.1A patent/CN105213272B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1125461A (en) * | 1993-05-11 | 1996-06-26 | 阿奇麦克斯 | Method and plant for solvent-free microwave extraction of natural products |
| CN1693438A (en) * | 2005-05-12 | 2005-11-09 | 中国科学院广州化学研究所 | Process for extracting and refining lavender oil |
| CN1994269A (en) * | 2006-12-28 | 2007-07-11 | 上海交通大学 | Method for preparing fragrant lavender liquid |
| CN102379834B (en) * | 2011-10-31 | 2013-05-22 | 上海交通大学 | Scent plant extractive for comprehensively conditioning skin around eyes and eye care product thereof |
| CN103173287A (en) * | 2013-04-23 | 2013-06-26 | 四川紫颐天堂香草科技开发有限公司 | Method for extracting lavender essential oil |
| CN103385832A (en) * | 2013-07-24 | 2013-11-13 | 云南西草资源开发有限公司 | Anti-aging cosmetic taking lavender extract as main active ingredient |
Non-Patent Citations (1)
| Title |
|---|
| 微波无溶剂提取的应用进展;傅小红;《广东化工》;20140531;第41卷(第9期);第123-124页 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105213272A (en) | 2016-01-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105250180B (en) | A kind of fresh and alive water of rose and the preparation method and application thereof | |
| CN102028646A (en) | Thyme perfume | |
| CN102150704A (en) | Fruit and vegetable fresh-keeping agent and preparation method thereof | |
| CN101536968A (en) | Cellular fluid of fresh flowers of roses and preparation method thereof | |
| CN101693853A (en) | Device for extracting plant essential oil and method for preparing bamboo leaf essential oil by using same | |
| CN103396885A (en) | Method for preparing pepper aromatic oil | |
| JP2017048322A (en) | Method for extracting essential oil and essential oil product including essential oil | |
| CN105662951A (en) | Hydrolat and preparation method and application thereof | |
| CN105213272B (en) | A kind of fresh and alive water of lavender and the preparation method and application thereof | |
| CN109288741A (en) | A kind of Chinese torreya compound essential oil and preparation method thereof | |
| CN105232400B (en) | A kind of fresh and alive water of jasmine and the preparation method and application thereof | |
| CN203582836U (en) | Vacuum plant essential oil extraction device | |
| CN101461558B (en) | Aspergillus bacteriostatic agent and use thereof | |
| CN105087165A (en) | Composite essential oil prepared from taxus cuspidata and coniferous plants and application of composite essential oil | |
| CN111254017A (en) | Extraction process for extracting osmanthus oil by supercritical carbon dioxide fluid and application | |
| CN105232782B (en) | A kind of fresh and alive water of fresh tea and the preparation method and application thereof | |
| Özcan | Antioxidant activity of seafennel (crithmum maritimum l.) essential oil and rose (rosa canina) extract on antioxidant activity of seafennel (crithmum maritimum l.) essential oil and rose (rosa canina) extract on natural olive oilnatural olive oil | |
| CN110180363A (en) | A kind of formaldehyde remover and preparation method thereof with sterilizing function | |
| Samad et al. | Optimization of Plectranthus amboinicus (Lour.) Spreng Extraction Process using Microwave-Assisted Technique. | |
| CN201834902U (en) | Natural essential oil extracting device | |
| CN102653705A (en) | Method for extracting essential oil and natural flavor 2-hendecanone from zanthoxylum bungeanum maxim fruit | |
| CN105213273B (en) | A kind of fresh and alive water of lemon and the preparation method and application thereof | |
| CN109576049A (en) | A kind of tasteless tea oil and the preparation method and application thereof with high active ingredient | |
| CN105287276A (en) | Food-grade mosquito repellent for babies | |
| Nigam et al. | Extraction of essential oil from seasonal fruit rind: a review |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160718 Address after: 100048 Beijing city Haidian District Fuchengmen Road No. 33 Applicant after: Beijing Technology and Business University Applicant after: SHANGHAI DAI COSMETICS INSTRUMENT LTD. Address before: 201608 Shanghai Songjiang District Yexie Road No. 323 Applicant before: SHANGHAI DAI COSMETICS INSTRUMENT LTD. |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant |