AR109367A2 - Proceso continuo para preparar sílice y productos preparados a partir de esta - Google Patents

Proceso continuo para preparar sílice y productos preparados a partir de esta

Info

Publication number
AR109367A2
AR109367A2 ARP170102302A ARP170102302A AR109367A2 AR 109367 A2 AR109367 A2 AR 109367A2 AR P170102302 A ARP170102302 A AR P170102302A AR P170102302 A ARP170102302 A AR P170102302A AR 109367 A2 AR109367 A2 AR 109367A2
Authority
AR
Argentina
Prior art keywords
loop
reaction zone
liquid medium
continuous process
silica
Prior art date
Application number
ARP170102302A
Other languages
English (en)
Original Assignee
Huber Corp J M
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=44209705&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=AR109367(A2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Huber Corp J M filed Critical Huber Corp J M
Publication of AR109367A2 publication Critical patent/AR109367A2/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/126—Preparation of silica of undetermined type
    • C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K6/00—Preparations for dentistry
    • A61K6/70—Preparations for dentistry comprising inorganic additives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28059—Surface area, e.g. B.E.T specific surface area being less than 100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28061—Surface area, e.g. B.E.T specific surface area being in the range 100-500 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
    • A61K9/1605—Excipients; Inactive ingredients
    • A61K9/1611—Inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/19—Oil-absorption capacity, e.g. DBP values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/21—Attrition-index or crushing strength of granulates
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Silicon Compounds (AREA)
  • Cosmetics (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Silicon Polymers (AREA)

Abstract

Se describe en la presente un proceso continuo para preparar un producto de sílice, que comprende: (a) alimentar de forma continua un agente acidulante y un silicato de metal alcalino en una zona de reacción del bucle que comprende una corriente de medio líquido; en donde al menos una porción del agente acidulante y el silicato de metal alcalino reaccionan para formar un producto de sílice en el medio líquido de la zona de reacción del bucle; (b) hacer recircular de forma continua el medio líquido a través de la zona de reacción del bucle; y (c) descargar de forma continua de la zona de reacción del bucle una porción del medio líquido que comprende el producto de sílice. También se describen productos de sílice y composiciones dentífricas que comprenden los productos de sílice. Además se describe un reactor de bucle continuo.
ARP170102302A 2010-02-24 2017-08-17 Proceso continuo para preparar sílice y productos preparados a partir de esta AR109367A2 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US12/711,321 US8609068B2 (en) 2010-02-24 2010-02-24 Continuous silica production process and silica product prepared from same

Publications (1)

Publication Number Publication Date
AR109367A2 true AR109367A2 (es) 2018-11-21

Family

ID=44209705

Family Applications (3)

Application Number Title Priority Date Filing Date
ARP110100570A AR080655A1 (es) 2010-02-24 2011-02-24 Proceso continuo para preparar silice y productos preparados a partir de esta
ARP140101972A AR096331A2 (es) 2010-02-24 2014-05-16 Proceso continuo para preparar sílice y productos preparados a partir de esta
ARP170102302A AR109367A2 (es) 2010-02-24 2017-08-17 Proceso continuo para preparar sílice y productos preparados a partir de esta

Family Applications Before (2)

Application Number Title Priority Date Filing Date
ARP110100570A AR080655A1 (es) 2010-02-24 2011-02-24 Proceso continuo para preparar silice y productos preparados a partir de esta
ARP140101972A AR096331A2 (es) 2010-02-24 2014-05-16 Proceso continuo para preparar sílice y productos preparados a partir de esta

Country Status (20)

Country Link
US (4) US8609068B2 (es)
EP (3) EP3216442B1 (es)
JP (2) JP5905401B2 (es)
KR (4) KR101652771B1 (es)
CN (3) CN104402008B (es)
AR (3) AR080655A1 (es)
AU (1) AU2011221218B2 (es)
BR (3) BR122014004122B1 (es)
DE (1) DE11718532T1 (es)
ES (3) ES2748576T3 (es)
HU (2) HUE047179T2 (es)
MX (3) MX2012008829A (es)
MY (1) MY158259A (es)
PH (2) PH12017500235A1 (es)
PL (3) PL3210592T3 (es)
PT (2) PT3210592T (es)
RU (3) RU2673449C9 (es)
TR (1) TR201902549T4 (es)
TW (3) TWI443066B (es)
WO (1) WO2011106289A2 (es)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8609068B2 (en) 2010-02-24 2013-12-17 J.M. Huber Corporation Continuous silica production process and silica product prepared from same
US8642529B2 (en) * 2010-11-15 2014-02-04 Conopco, Inc. Liquid low surfactant compositions structured with a fibrous polymer
US9028605B2 (en) 2011-02-25 2015-05-12 J.M. Huber Corporation Coating compositions comprising spheroid silica or silicate
US9724277B2 (en) * 2011-04-04 2017-08-08 Robert L. Karlinsey Microbeads for dental use
DE102012202587A1 (de) * 2012-02-21 2013-08-22 Evonik Degussa Gmbh Verfahren zur Herstellung von hochreinem SiO2
JP5968126B2 (ja) * 2012-07-04 2016-08-10 太平洋セメント株式会社 非晶質シリカの製造方法
US9186307B2 (en) * 2012-11-19 2015-11-17 J.M. Huber Corporation Treated silicas and metal silicates for improved cleaning in dentifrice
BR112016013531A8 (pt) 2013-12-20 2020-05-19 Colgate Palmolive Co composição de cuidado oral
AU2014369061B2 (en) 2013-12-20 2017-03-02 Colgate-Palmolive Company Tooth whitening oral care product with core shell silica particles
DE102014204053A1 (de) * 2014-03-05 2015-09-10 Beiersdorf Ag Abrasive Hautreinigungsmittel II
BR112017023974B1 (pt) 2015-05-08 2022-10-18 Evonik Operations Gmbh Partículas de pigmento colorido e seu uso, processo de produção e composição
JP6797194B2 (ja) 2015-09-28 2020-12-09 エボニック オペレーションズ ゲーエムベーハー シリカベースの抗微生物性口腔用組成物
US10547056B2 (en) 2015-09-30 2020-01-28 Umicore Precursors for lithium transition metal oxide cathode materials for rechargeable batteries
EP3393971B1 (en) * 2015-12-23 2021-10-20 Tata Chemicals Limited A process for preparing precipitated silica
JP7044718B2 (ja) 2016-05-16 2022-03-30 マルチンスヴェルク ゲーエムベーハー アルミナ製品および高熱伝導率のポリマー組成物におけるその使用
WO2018019373A1 (de) * 2016-07-27 2018-02-01 Wacker Chemie Ag Verfahren zur herstellung einer modifizierten fällungskieselsäure und zusammensetzung enthaltend diese
US10486973B2 (en) * 2016-11-18 2019-11-26 Ppg Industries Ohio, Inc. Silica-based spherical particulates and methods of preparing the same
JP7060600B2 (ja) * 2016-12-19 2022-04-26 エボニック オペレーションズ ゲーエムベーハー 第一スズ適合性シリカ
RU2726804C1 (ru) 2016-12-19 2020-07-15 Дзе Проктер Энд Гэмбл Компани Композиции для чистки зубов, содержащие совместимые с оловом частицы оксида кремния
CN111295228A (zh) * 2017-08-28 2020-06-16 赢创运营有限公司 用于小管封闭的球形二氧化硅
KR20200044894A (ko) * 2017-08-29 2020-04-29 에보니크 오퍼레이션즈 게엠베하 Rda 제어를 위한 구형 실리카 입자 크기
CN108046278B (zh) * 2018-01-23 2020-12-08 合肥星巢环保科技有限公司 一种管式连续流法制备高比表面积二氧化硅的方法
KR102567067B1 (ko) * 2018-04-30 2023-08-11 주식회사 엘지화학 우수한 분산성을 갖는 알루미노실리케이트 나노입자의 제조 방법, 상기 알루미노실리케이트 나노입자를 포함한 고무 보강재 및 이를 포함한 타이어용 고무 조성물
HUE063806T2 (hu) 2018-06-12 2024-02-28 Evonik Operations Gmbh Gömb alakú, ónnal kompatibilis szilícium-dioxid részecskék csökkentett RDA-hoz
AU2019287467B2 (en) 2018-06-12 2022-02-03 The Procter & Gamble Company Dentifrice formulations having spherical stannous compatible silica particles for reduced RDA
CN109319794A (zh) * 2018-11-20 2019-02-12 福建省三明同晟化工有限公司 一种连续法制备沉淀二氧化硅的方法
US20210393495A1 (en) * 2018-11-23 2021-12-23 Blbr Gmbh Foamable dental care composition, system consisting of the dental care composition and a dispenser, and use of the dental care composition in a method for simultaneously cleaning several, preferably all, teeth
EP3659968A1 (en) * 2018-11-29 2020-06-03 ImerTech Mineral composition
CN113164337A (zh) 2018-12-04 2021-07-23 宝洁公司 具有改善的锡相容性的口腔护理组合物
CN109850911B (zh) * 2019-04-08 2023-11-28 原初科技（北京）有限公司 一种利用氯化氢气体浸取硅酸盐矿制备超细二氧化硅的系统及方法
US20220275191A1 (en) * 2019-07-30 2022-09-01 Kuraray Co., Ltd. Resin powder and method for producing same
CN110606492B (zh) * 2019-10-29 2022-07-12 朱志宏 一种连续合成白炭黑及氟化钠的方法
WO2021093961A1 (de) 2019-11-14 2021-05-20 Wacker Chemie Ag Modifizierte fällungskieselsäure mit reduziertem feuchteanteil
CN111392739B (zh) * 2020-03-27 2020-12-01 广州市飞雪材料科技有限公司 一种高分散性增稠型二氧化硅的制备方法及应用
CN112174147B (zh) * 2020-09-30 2023-12-22 南京工业大学 一种管式连续流法制备球形纳米二氧化硅的方法
CN116323822A (zh) 2020-10-02 2023-06-23 赢创运营有限公司 在粉末涂料中作为消光剂的低表面积球形沉淀二氧化硅
CA3138558C (en) 2020-11-16 2024-01-30 Church & Dwight Co., Inc. Teeth cleaning composition comprising banana extract
KR20230138530A (ko) 2021-02-11 2023-10-05 에보니크 오퍼레이션즈 게엠베하 무정형 비-다공성 실리카
WO2023117446A1 (en) * 2021-12-20 2023-06-29 Evonik Operations Gmbh Precipitated silica and methods thereof
WO2023227642A1 (en) 2022-05-27 2023-11-30 Evonik Operations Gmbh Spherical calcium silicate
WO2023245069A2 (en) * 2022-06-14 2023-12-21 Aquestive Therapeutics, Inc. Enhanced delivery epinephrine and prodrug compositions

Family Cites Families (89)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2727876A (en) 1952-03-06 1955-12-20 Du Pont Composition and process
US3386810A (en) * 1961-10-03 1968-06-04 Burke Apparatus for the production of silica pigments
US3324093A (en) 1963-10-21 1967-06-06 Phillips Petroleum Co Loop reactor
US4001379A (en) 1968-04-27 1977-01-04 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Process of making superfine amorphous high structural silicic acid
US4122160A (en) * 1974-10-31 1978-10-24 J. M. Huber Corporation Toothpaste compositions containing improved amorphous precipitated silicas
US3987096A (en) 1975-01-20 1976-10-19 E. I. Du Pont De Nemours And Company Process for chlorination of acetaldoxime
GB1561189A (en) 1976-12-24 1980-02-13 Yokohama Rubber Co Ltd Pressure responsive electrically conductive elastomeric composition
US4421527A (en) 1977-12-20 1983-12-20 J. M. Huber Corporation High fluoride compatibility dentifrice abrasives and compositions
US4340583A (en) 1979-05-23 1982-07-20 J. M. Huber Corporation High fluoride compatibility dentifrice abrasives and compositions
US4420312A (en) 1979-05-23 1983-12-13 J. M. Huber Corporation Method for production of high fluoride compatibility dentifrice abrasives and compositions
EP0111748B1 (de) * 1982-11-16 1987-03-25 Hoechst Aktiengesellschaft Aluminiumsilikate mit Zeolithstruktur und Verfahren zu ihrer Herstellung
GB2132996B (en) 1982-12-29 1986-12-10 Lion Corp Oral composition and abrasive therefor
JPS60105609A (ja) 1983-03-04 1985-06-11 Taki Chem Co Ltd 歯磨用シリカ基剤及びその製造方法
FR2567504B1 (fr) 1984-07-11 1989-12-29 Rhone Poulenc Chim Base Colloides de silice et silices spheriques et procedes pour leur obtiention
FR2567505B1 (fr) 1984-07-11 1986-11-21 Rhone Poulenc Chim Base Silice a prise d'huile elevee et a structure primaire controlee et procede pour son obtention
JPS61220182A (ja) 1985-03-26 1986-09-30 Nitto Electric Ind Co Ltd カセツトテ−プ用テ−プガイド
JPS6287507A (ja) * 1985-10-11 1987-04-22 Fuji Debuison Kagaku Kk 歯磨剤
US4874549A (en) 1985-12-13 1989-10-17 Advanced Micro-Matrix, Inc. Pressure sensitive electro-conductive materials
GB8604985D0 (en) * 1986-02-28 1986-04-09 Unilever Plc Precipitated silicas
JPS62252312A (ja) * 1986-04-25 1987-11-04 Nippon Chem Ind Co Ltd:The 含水珪酸の製造方法
US4767433A (en) 1986-05-22 1988-08-30 Asahi Glass Company Ltd. Spherical silica glass powder particles and process for their production
DE3751943T2 (de) 1986-08-04 1997-04-03 Dainippon Ink & Chemicals Herstellungsverfahren von Tonern für die Entwicklung von elektrostatischen Bildern und derartige Toner
US5030286A (en) 1988-09-22 1991-07-09 Ppg Industries, Inc. High solids aqueous silica slurry
JP2742693B2 (ja) 1988-09-22 1998-04-22 コニカ株式会社 磁性トナー
EP0495039B2 (en) * 1990-08-06 2003-10-08 INEOS Silicas Limited Silicas
FR2678259B1 (fr) * 1991-06-26 1993-11-05 Rhone Poulenc Chimie Nouvelles silices precipitees sous forme de granules ou de poudres, procedes de synthese et utilisation au renforcement des elastomeres.
KR960010781B1 (ko) 1991-10-02 1996-08-08 유니레버 엔브이 실리카
US5279807A (en) 1992-05-26 1994-01-18 E. I. Du Pont De Nemours And Company Method for preparing low-concentration polysilicate microgels
IL104722A (en) 1993-02-02 1998-04-05 Rotem Fertilizers Ltd Process for the manufacture of pure silica from rock containing it
JPH06239722A (ja) * 1993-02-15 1994-08-30 Johnson & Johnson Kk 歯みがき組成物
US5691095A (en) 1994-12-09 1997-11-25 Dainippon Ink And Chemicals, Inc. Toner for developing electrostatic latent image and process for producing the same
US5676932A (en) * 1995-05-02 1997-10-14 J.M. Huber Corporation Silica abrasive compositions
US5658553A (en) 1995-05-02 1997-08-19 The Procter & Gamble Company Dentifrice compositions
US5651958A (en) 1995-05-02 1997-07-29 The Procter & Gamble Company Dentifrice compositions
DE19524182A1 (de) 1995-07-03 1997-01-09 Basf Ag Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren
US5891421A (en) * 1996-03-22 1999-04-06 J.M. Huber Corporation Precipitated silicas having improved dentifrice performance characteristics and methods of preparation
FR2747669B1 (fr) 1996-04-22 1998-05-22 Rhone Poulenc Chimie Procede de preparation de particules creuses de silice
US5929156A (en) * 1997-05-02 1999-07-27 J.M. Huber Corporation Silica product for use in elastomers
CN1152822C (zh) * 1997-06-04 2004-06-09 纳幕尔杜邦公司 改进的制备低浓度聚硅铝酸盐微凝胶的方法
KR100573343B1 (ko) 1997-06-13 2006-04-24 이 아이 듀폰 디 네모아 앤드 캄파니 저-농도 폴리알루미노실리케이트 마이크로겔의 개선된제조 방법
US6239235B1 (en) * 1997-07-15 2001-05-29 Phillips Petroleum Company High solids slurry polymerization
DE69910905T2 (de) 1998-06-22 2004-07-15 Mitsubishi Polyester Film Corp. Biaxial-orientierte Polyesterfolie
US6406789B1 (en) 1998-07-22 2002-06-18 Borden Chemical, Inc. Composite proppant, composite filtration media and methods for making and using same
DE60027837T2 (de) 1999-04-02 2006-09-28 Sanyo Chemical Industries, Ltd. Trockenentwickler
JP4412759B2 (ja) * 1999-04-30 2010-02-10 水澤化学工業株式会社 球状シリカゲル粒子及びその製法
US6114430A (en) 1999-08-25 2000-09-05 H.B. Fuller Licensing & Financing, Inc. Aqueous paint compositions comprising polyether amides
US6274112B1 (en) 1999-12-08 2001-08-14 E. I. Du Pont De Nemours And Company Continuous production of silica-based microgels
CA2292819A1 (en) 1999-12-22 2001-06-22 Bayer Inc. Process for the production of a precipitated silica slurry with a controlled aggregate particle size distribution
US6290933B1 (en) * 2000-05-09 2001-09-18 Colgate-Palmolive Company High cleaning dentifrice
US6652611B1 (en) 2000-08-18 2003-11-25 J. M. Huber Corporation Method for making abrasive compositions and products thereof
US6419174B1 (en) 2000-08-18 2002-07-16 J. M. Huber Corporation Abrasive compositions and methods for making same
US6403059B1 (en) 2000-08-18 2002-06-11 J. M. Huber Corporation Methods of making dentifrice compositions and products thereof
JP2002275274A (ja) 2001-03-19 2002-09-25 Dokai Chemical Industries Co Ltd 鱗片状シリカ粒子を含有する高い保存安定性を有する硬化性組成物及びその製造方法
US20050109238A1 (en) 2001-10-25 2005-05-26 Takeyuki Yamaki Coating material composition and article having coating film formed therewith
TWI228553B (en) 2001-11-16 2005-03-01 Du Pont Method of producing coating compositions and coating compositions made therefrom
US20030110338A1 (en) 2001-12-06 2003-06-12 Yuanlong Wang Method and apparatus for emulating computer buses using point-to-point techniues
US6616916B1 (en) 2001-12-10 2003-09-09 J. M. Huber Corporation Transparent dentifrices
GB0130907D0 (en) * 2001-12-22 2002-02-13 Ineos Silicas Ltd Amorphous silica
FR2833937B1 (fr) 2001-12-26 2004-11-12 Rhodia Chimie Sa Silices a faible reprise en eau
US20030228369A1 (en) 2002-05-06 2003-12-11 Kuhrts Eric Hauser Process for conversion of high viscosity fluids and compositions thereof
EP1525158B1 (de) * 2002-08-03 2007-09-12 Degussa GmbH Hochdispersible fällungskieselsäure mit hoher oberfläche
DE10248799B4 (de) 2002-10-19 2007-03-15 Georg Gros Partikel enthaltende Beschichtungszusammensetzung und Verfahren zur Beschichtung von Oberflächen
US6946119B2 (en) 2003-02-14 2005-09-20 J.M. Huber Corporation Precipitated silica product with low surface area, dentifrices containing same, and processes
JP4239835B2 (ja) 2004-01-28 2009-03-18 富士ゼロックス株式会社 静電荷像現像用トナー、静電荷像現像用現像剤及び画像形成方法
US7429789B2 (en) 2004-03-31 2008-09-30 Endicott Interconnect Technologies, Inc. Fluoropolymer dielectric composition for use in circuitized substrates and circuitized substrate including same
GB0416256D0 (en) 2004-07-20 2004-08-25 Avecia Ltd Manufacturing process
US20070258922A1 (en) 2004-11-01 2007-11-08 Wozniak Mark E Novel silica- or silicate-based pigments for wrinkle-hiding cosmetic applications
US20070253987A1 (en) 2004-11-01 2007-11-01 Wozniak Mark E Novel pigments for wrinkle-hiding cosmetic applications
US7267814B2 (en) 2004-11-24 2007-09-11 J.M. Huber Corporation High-cleaning/low abrasive silica and materials and dentifrice containing such materials
US7670593B2 (en) 2004-11-24 2010-03-02 J.M. Huber Corporation High-cleaning silica materials and dentifrice containing such
US20060110307A1 (en) 2004-11-24 2006-05-25 Mcgill Patrick D High-cleaning silica materials made via product morphology control and dentifrice containing such
US7303742B2 (en) 2004-11-24 2007-12-04 J.M. Huber Corporation Viscosity-modifying silica materials that exhibit low cleaning and abrasive levels and dentifrices thereof
US7306788B2 (en) 2004-11-24 2007-12-11 J.M. Huber Corporation High-cleaning/moderate abrasive silica materials and dentifrice containing such materials
MX2007009242A (es) * 2005-02-04 2007-09-19 Unilever Nv Composicion de pasta de dientes de multiples fases.
US7159803B1 (en) * 2005-06-29 2007-01-09 J.M. Huber Corporation Method for making particulate compositions and products thereof
US7731110B2 (en) * 2005-06-29 2010-06-08 J.M. Huber Corporation Method for making precipitated silica compositions and products thereof
DE102005043201A1 (de) * 2005-09-09 2007-03-15 Degussa Ag Fällungskieselsäuren mit einer besonderen Porengrößenverteilung
KR100740346B1 (ko) 2005-12-01 2007-07-19 이엔비나노텍(주) 나노기공 실리카의 제조장치 및 그 제조방법
GB0525369D0 (en) * 2005-12-14 2006-01-18 Ineos Silicas Ltd Silicas
US7906598B2 (en) 2006-08-30 2011-03-15 Intertape Polymer Corp. Recirculation loop reactor bulk polymerization process
US7270803B1 (en) 2006-03-23 2007-09-18 J.M. Huber Corporation High-cleaning, low abrasion, high brightness silica materials for dentrifices
US20070224133A1 (en) 2006-03-23 2007-09-27 Mcgill Patrick D High-cleaning silica materials made via product morphology control under high shear conditions
JPWO2007122930A1 (ja) 2006-04-20 2009-09-03 旭硝子株式会社 コアシェル型シリカおよびその製造方法
JP5631530B2 (ja) * 2007-12-07 2014-11-26 日揮触媒化成株式会社 表面平滑性を備えた多孔質シリカ系粒子、その製造方法および該多孔質シリカ系粒子を配合してなる化粧料
US10213627B2 (en) 2008-05-16 2019-02-26 Colgate-Palmolive Company Oral compositions and uses therof
US20100047742A1 (en) 2008-08-25 2010-02-25 Pitcock Jr William Henry Tubule-blocking silica materials for dentifrices
EP2349489B1 (en) * 2008-11-25 2015-11-11 The Procter and Gamble Company Low ph oral care compositions with fused silica and a fluoride source
US8609068B2 (en) 2010-02-24 2013-12-17 J.M. Huber Corporation Continuous silica production process and silica product prepared from same
US9028605B2 (en) 2011-02-25 2015-05-12 J.M. Huber Corporation Coating compositions comprising spheroid silica or silicate

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