ZA848847B - Liquid 2-hydroxy-methylthiobutyric acid and process for the preparation thereof - Google Patents

Liquid 2-hydroxy-methylthiobutyric acid and process for the preparation thereof

Info

Publication number
ZA848847B
ZA848847B ZA848847A ZA848847A ZA848847B ZA 848847 B ZA848847 B ZA 848847B ZA 848847 A ZA848847 A ZA 848847A ZA 848847 A ZA848847 A ZA 848847A ZA 848847 B ZA848847 B ZA 848847B
Authority
ZA
South Africa
Prior art keywords
hydroxy
weight
acid
liquid
methylthiobutyric acid
Prior art date
Application number
ZA848847A
Other languages
English (en)
Inventor
Dennis Arthur Ruest
Masaharu Takano
Lawrence Russell Wolf
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of ZA848847B publication Critical patent/ZA848847B/xx

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/26Separation; Purification; Stabilisation; Use of additives
    • C07C319/28Separation; Purification
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/105Aliphatic or alicyclic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/142Amino acids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K50/00Feeding-stuffs specially adapted for particular animals
    • A23K50/70Feeding-stuffs specially adapted for particular animals for birds
    • A23K50/75Feeding-stuffs specially adapted for particular animals for birds for poultry
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/50Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
    • C07C323/51Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/52Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Food Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Animal Husbandry (AREA)
  • Birds (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fodder In General (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
ZA848847A 1983-11-14 1984-11-13 Liquid 2-hydroxy-methylthiobutyric acid and process for the preparation thereof ZA848847B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/550,857 US4524077A (en) 1983-11-14 1983-11-14 Liquid 2-hydroxy-4-methylthiobutyric acid and process for the preparation thereof

Publications (1)

Publication Number Publication Date
ZA848847B true ZA848847B (en) 1985-09-25

Family

ID=24198852

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA848847A ZA848847B (en) 1983-11-14 1984-11-13 Liquid 2-hydroxy-methylthiobutyric acid and process for the preparation thereof

Country Status (13)

Country Link
US (1) US4524077A (de)
EP (1) EP0142488B1 (de)
JP (2) JPS60156396A (de)
KR (1) KR870000657B1 (de)
AT (1) ATE29131T1 (de)
AU (1) AU562078B2 (de)
CA (1) CA1263668C (de)
DE (1) DE3465592D1 (de)
GB (1) GB2149791B (de)
GE (1) GEP19960463B (de)
MX (1) MX163989B (de)
SU (1) SU1428193A3 (de)
ZA (1) ZA848847B (de)

Families Citing this family (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2005784A6 (es) * 1988-02-22 1989-03-16 Desarrollo Tecnico Ind S A Soc Un procedimiento para preparar soluciones acuosas de acido 2-hidroxi-4-metil-tiobutirico.
MY109603A (en) * 1992-05-21 1997-03-31 Daicel Chem Process for producing 2-hydroxy-4-methylthiobutanoic acid
US5498790A (en) * 1993-06-09 1996-03-12 Novus International, Inc. Regeneration of sulfuric acid from sulfate by-products of 2-hydroxy-4-(methylthio)butyric acid manufacture
RU2130925C1 (ru) * 1994-07-11 1999-05-27 Дегусса Акциенгезельшафт Способ получения 2-гидрокси-4-метилтиомасляной кислоты (гидроксианалогаметионина, гам), гам
DE4428608C1 (de) * 1994-08-12 1996-02-29 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
RU2179550C2 (ru) * 1995-06-07 2002-02-20 Новус Интернэшнл, Инк. Способ получения 2-гидрокси-4-метилтиомасляной кислоты или ее солей
US5856567A (en) * 1995-06-07 1999-01-05 Novus International, Inc. Continuous hydrolysis process for preparing 2-hydroxy-4-methylthiobutanioc acid or salts thereof
DE19548538C2 (de) * 1995-12-23 1997-12-18 Degussa Verfahren zur Gewinnung von 2-Hydroxy-4-methylthiobuttersäure (MHA)
DE19654485A1 (de) * 1996-12-27 1998-07-02 Degussa Verfahren zur Gewinnung von lagerstabiler 2-Hydroxy-4-methylthiobuttersäure (MHA)
JP3804210B2 (ja) * 1997-03-04 2006-08-02 住友化学株式会社 2−ヒドロキシ−4−メチルチオブタン酸の製造方法
US6017563A (en) 1997-07-25 2000-01-25 Novus International, Inc. Process for optimizing milk production
FR2780969B1 (fr) * 1998-07-10 2000-08-18 Rhone Poulenc Nutrition Animal Procede de separation de l'acide hydroxymethylthiobutyrique
FR2780968B1 (fr) * 1998-07-10 2000-08-18 Rhone Poulenc Nutrition Animal Procede de preparation de l'acide hydroxymethylthiobutyrique
FR2791673B1 (fr) * 1999-04-02 2001-06-08 Rhone Poulenc Animal Nutrition Procede de preparation des esters de l'acide hydroxymethylthiobutyrique
US6342651B1 (en) 1999-08-05 2002-01-29 Novus International, Inc. Reductive combustion of ammonium salts of sulfuric acid
US6649794B2 (en) 2000-02-18 2003-11-18 Sumitomo Chemical Company, Limited Method for producing 2-Hydroxy-4-Methylthiobutanoic Acid
TWI296652B (en) * 2000-03-29 2008-05-11 Mitsui Chemicals Inc Production process of amide compound
JP4517474B2 (ja) * 2000-07-25 2010-08-04 住友化学株式会社 2−ヒドロキシ−4−メチルチオブタン酸の製造方法
JP4517486B2 (ja) * 2000-09-25 2010-08-04 住友化学株式会社 2−ヒドロキシ−4−メチルチオブタンニトリルの製造方法
JP4517520B2 (ja) * 2001-02-27 2010-08-04 住友化学株式会社 2−ヒドロキシ−4−メチルチオブタン酸の製造方法
DE10316110A1 (de) * 2003-04-09 2004-10-28 Degussa Ag Verfahren zur Herstellung von 2-Hydroxy-4-methylthio-buttersäure Ammoniumsalz
FR2871028B1 (fr) * 2004-06-08 2006-12-29 Adisseo Ireland Ltd Complement alimentaire pour animaux, comprenant un additif olfactif
JP4696496B2 (ja) 2004-08-18 2011-06-08 住友化学株式会社 2−ヒドロキシ−4−メチルチオ酪酸の製造方法
CN101040051B (zh) * 2004-10-14 2012-02-01 住友化学株式会社 生产2-羟基-4-(甲硫基)丁酸的方法
DE102005050106B4 (de) * 2005-10-18 2008-04-30 Josef Meissner Gmbh & Co. Kg Rückgewinnung von Nitriersäuregemischen aus Nitrienprozessen
ES2279719B1 (es) * 2006-01-26 2008-07-16 Timac Agro España, S.A. Nuevo activador metabolico y nutricional para las plantas.
CN102702046B (zh) 2006-07-21 2014-07-09 住友化学株式会社 生产2-羟基-4-(甲硫基)丁酸或丁酸酯化合物及其中间体的方法
DE102007062199A1 (de) * 2007-12-21 2009-06-25 Evonik Degussa Gmbh 2-Methylthioethyl-substituierte Heterocyclen als Futtermitteladditive
JP2009161499A (ja) * 2008-01-10 2009-07-23 Sumitomo Chemical Co Ltd 2−ヒドロキシ−4−メチルチオブタンアミドの製造方法
FR2938535B1 (fr) 2008-11-20 2012-08-17 Arkema France Procede de fabrication de methylmercaptopropionaldehyde et de methionine a partir de matieres renouvelables
FR2939791B1 (fr) * 2008-12-16 2011-01-14 Adisseo France Sas Procede de preparation d'acroleine a partir de glycerol ou de glycerine brute
MX342139B (es) 2010-12-30 2016-09-14 Metabolic Explorer Sa Produccion fermentativa de analogo de hidroximetionina (mha).
WO2013119955A1 (en) 2012-02-09 2013-08-15 Novus International Inc. Functionalized polymer compositions
KR101419118B1 (ko) * 2012-07-11 2014-07-11 김건희 사료용 향료 조성물
CN107753462B (zh) 2012-07-12 2021-01-08 诺华丝国际股份有限公司 用于保护生物活性剂的基质和层组合物
PE20161125A1 (es) * 2014-02-20 2016-11-08 Smidth As F L Sedimentador de columna para la separacion de fases lquido/liquido de alto rendimiento en procesos hidromelurciales y metodos de los mismos
CN104860855B (zh) * 2014-12-08 2017-06-16 宁夏紫光天化蛋氨酸有限责任公司 一种高纯度的d,l‑2‑羟基‑4‑甲硫基丁酸酯的制备方法
RU2738419C2 (ru) * 2016-06-24 2020-12-14 Новас Интернэшнл Инк. Составы аналогов гидроксиметионина, подходящие для применения в качестве специальных химических агентов
FR3064006B1 (fr) 2017-03-16 2019-03-29 Adisseo France S.A.S. Procede de fabrication de l'acide-2-hydroxy-4-methylthio-butyrique
US10584306B2 (en) 2017-08-11 2020-03-10 Board Of Regents Of The University Of Oklahoma Surfactant microemulsions

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB722024A (en) * 1950-10-31 1955-01-19 Monsanto Chemicals Production of alpha-hydroxy-gamma-mercapto-carboxylic acids and salts thereof and compositions containing the same
US2745745A (en) * 1952-10-30 1956-05-15 Monsanto Chemicals Poultry feed
US2938053A (en) * 1955-12-29 1960-05-24 Monsanto Chemicals Amino acid analogues
CH385823A (de) * 1959-09-01 1964-12-31 Inventa Ag Verfahren zur Herstellung des Calciumsalzes der a-Oxy-y-methylthio-buttersäure
BE611435A (fr) * 1960-12-14 1962-06-12 Stamicarbon Procédé de préparation de sels métalliques d'acide alpha-hydroxy- gamma -méthylmercaptobutyrique
US3773927A (en) * 1971-12-20 1973-11-20 Du Pont Preparation of an aqueous slurry of ammonium chloride and methylmercapto-hydroxybutyric acid
US4310690A (en) * 1980-10-08 1982-01-12 E. I. Du Pont De Nemours And Company Preparation of the calcium salt of α-hydroxy-gamma-methylmercaptobutyric acid

Also Published As

Publication number Publication date
JPH051787B2 (de) 1993-01-11
CA1263668A (en) 1989-12-05
EP0142488A2 (de) 1985-05-22
US4524077A (en) 1985-06-18
AU3535984A (en) 1985-05-23
JPS60156396A (ja) 1985-08-16
MX163989B (es) 1992-07-07
GB2149791A (en) 1985-06-19
EP0142488B1 (de) 1987-08-26
GB8428657D0 (en) 1984-12-19
ATE29131T1 (de) 1987-09-15
JPH05211846A (ja) 1993-08-24
AU562078B2 (en) 1987-05-28
CA1263668C (en) 1989-12-05
KR870000657B1 (ko) 1987-04-04
SU1428193A3 (ru) 1988-09-30
EP0142488A3 (en) 1985-06-26
GB2149791B (en) 1988-04-20
KR850004108A (ko) 1985-07-01
GEP19960463B (en) 1996-07-15
DE3465592D1 (en) 1987-10-01
JPH0797970B2 (ja) 1995-10-25

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