ZA200701627B - Method for separating lignin from a lignin containing liquid/slurry - Google Patents
Method for separating lignin from a lignin containing liquid/slurry Download PDFInfo
- Publication number
- ZA200701627B ZA200701627B ZA200701627A ZA200701627A ZA200701627B ZA 200701627 B ZA200701627 B ZA 200701627B ZA 200701627 A ZA200701627 A ZA 200701627A ZA 200701627 A ZA200701627 A ZA 200701627A ZA 200701627 B ZA200701627 B ZA 200701627B
- Authority
- ZA
- South Africa
- Prior art keywords
- lignin
- level
- slurry
- liquid
- dewatering
- Prior art date
Links
- 229920005610 lignin Polymers 0.000 title claims description 78
- 238000000034 method Methods 0.000 title claims description 47
- 239000007788 liquid Substances 0.000 title claims description 36
- 239000002002 slurry Substances 0.000 title claims description 28
- 239000000047 product Substances 0.000 claims description 22
- 238000011084 recovery Methods 0.000 claims description 21
- 238000005406 washing Methods 0.000 claims description 19
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 17
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 15
- 150000001875 compounds Chemical class 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 12
- 239000012065 filter cake Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000000126 substance Substances 0.000 claims description 10
- 238000000926 separation method Methods 0.000 claims description 9
- 239000003546 flue gas Substances 0.000 claims description 8
- 239000007789 gas Substances 0.000 claims description 8
- 235000002918 Fraxinus excelsior Nutrition 0.000 claims description 7
- 239000002956 ash Substances 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 6
- 150000002500 ions Chemical class 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000000725 suspension Substances 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical class [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 5
- 230000001376 precipitating effect Effects 0.000 claims description 5
- -1 sulphate ions Chemical class 0.000 claims description 5
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 claims description 4
- 229910001424 calcium ion Inorganic materials 0.000 claims description 4
- 238000006073 displacement reaction Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 229910001420 alkaline earth metal ion Inorganic materials 0.000 claims description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 2
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 2
- 239000004571 lime Substances 0.000 claims description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 8
- 238000001556 precipitation Methods 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- 239000001569 carbon dioxide Substances 0.000 description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- 238000002485 combustion reaction Methods 0.000 description 3
- 239000000446 fuel Substances 0.000 description 3
- 239000001117 sulphuric acid Substances 0.000 description 3
- 235000011149 sulphuric acid Nutrition 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000020477 pH reduction Effects 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000004155 Chlorine dioxide Substances 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
- 241000549548 Fraxinus uhdei Species 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000002535 acidifier Substances 0.000 description 1
- 239000008186 active pharmaceutical agent Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000002551 biofuel Substances 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 239000001175 calcium sulphate Substances 0.000 description 1
- 235000011132 calcium sulphate Nutrition 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 235000019398 chlorine dioxide Nutrition 0.000 description 1
- 230000001112 coagulating effect Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000002535 lyotropic effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 150000004028 organic sulfates Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
Landscapes
- Compounds Of Unknown Constitution (AREA)
- Paper (AREA)
- Treatment Of Sludge (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE0402437A SE0402437D0 (sv) | 2004-10-07 | 2004-10-07 | Method for separating lignin from a lignin containing liquid/slurry |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ZA200701627B true ZA200701627B (en) | 2008-07-30 |
Family
ID=33434212
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ZA200701627A ZA200701627B (en) | 2004-10-07 | 2005-10-03 | Method for separating lignin from a lignin containing liquid/slurry |
| ZA200802400A ZA200802400B (en) | 2004-10-07 | 2008-03-14 | Method for separating lignin from a lignin containing liquid/slurry |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ZA200802400A ZA200802400B (en) | 2004-10-07 | 2008-03-14 | Method for separating lignin from a lignin containing liquid/slurry |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8815052B2 (fr) |
| EP (1) | EP1797236B1 (fr) |
| JP (1) | JP4887299B2 (fr) |
| AT (1) | ATE513082T1 (fr) |
| BR (1) | BRPI0517543B1 (fr) |
| CA (1) | CA2580834C (fr) |
| ES (1) | ES2368553T3 (fr) |
| PT (1) | PT1797236E (fr) |
| SE (1) | SE0402437D0 (fr) |
| WO (1) | WO2006038863A1 (fr) |
| ZA (2) | ZA200701627B (fr) |
Families Citing this family (72)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE0402201D0 (sv) * | 2004-09-14 | 2004-09-14 | Stfi Packforsk Ab | Method for separating lignin from black liquor |
| US8172981B2 (en) * | 2004-09-14 | 2012-05-08 | Lignoboost Ab | Separating lignin from black liquor by precipitation, suspension and separation |
| JP4316536B2 (ja) * | 2005-06-07 | 2009-08-19 | 独立行政法人科学技術振興機構 | リグニン誘導体の分離及び回収方法 |
| WO2007120091A1 (fr) * | 2006-03-16 | 2007-10-25 | Stfi-Packforsk Ab | Procédé permettant de séparer du pentose polymérique d'un liquide/d'une suspension épaisse |
| SE532840C2 (sv) | 2008-02-14 | 2010-04-20 | Lars Eriksson | Biobränsle |
| BRPI0822336B1 (pt) | 2008-02-21 | 2020-12-01 | Lignoboost Ab | método para separação de lignina de licor negro, produto de lignina, e uso de um produto de lignina para a produção de combustíveis ou materiais |
| EP3037459B1 (fr) * | 2008-07-16 | 2020-11-04 | Renmatix, Inc. | Raffineries bio à plate-forme de technologie nano-catalytico-solvo-thermique |
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| ES2571977T3 (es) | 2009-06-10 | 2016-05-27 | Valmet Oy | Método para precipitar lignina a partir de lejía negra utilizando gases residuales |
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| JP5657657B2 (ja) | 2009-07-13 | 2015-01-21 | ベータ リニューアブルス エス・ピー・エーＢＥＴＡ ＲＥＮＥＷＡＢＬＥＳ Ｓ．ｐ．Ａ． | リグニンの高温分離方法 |
| US9879119B2 (en) | 2009-09-25 | 2018-01-30 | Michael A. Lake | Lignin product and process for making same |
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| US9567360B2 (en) * | 2010-07-07 | 2017-02-14 | Stora Enso Oyj | Process for production of precipitated lignin from black liquor and precipitated lignin produced by the process |
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| CA1172808A (fr) * | 1981-07-23 | 1984-08-21 | Marc F. Beaupre | Methode de recuperation du surplus des liqueurs servant a la fabrication du papier kraft |
| US4470876A (en) * | 1982-07-22 | 1984-09-11 | Beaupre Marc F | Kraft overload recovery process |
| US4674597A (en) | 1986-06-17 | 1987-06-23 | Humphrey Denver L | Tree climbing device |
| US4891070A (en) * | 1987-04-13 | 1990-01-02 | Westvaco Corporation | Lignin amine salt as binder for aqueous printing ink composition |
| US4764597A (en) * | 1987-06-15 | 1988-08-16 | Westvaco Corporation | Method for methylolation of lignin materials |
| FI883934A (fi) * | 1987-08-27 | 1989-02-28 | Holmens Bruk Ab | Saett att genomfoera en sulfatcellulosaprocess och en anlaeggning foer genomfoering av saettet. |
| US5034094A (en) * | 1987-11-06 | 1991-07-23 | Kurple Kenneth R | Method of converting inorganic materials from kraft pulping liquor into pulping chemicals without passing them through a recovery furnace |
| EP0364632A1 (fr) * | 1988-10-17 | 1990-04-25 | Zeneca Limited | Récupération de la lignine |
| US5288857A (en) * | 1988-12-12 | 1994-02-22 | Ligno Tech Sweden Ab | Lignin preparation and method for its manufacture |
| SE468717B (sv) | 1988-12-12 | 1993-03-08 | Holmens Bruk Ab | Ligninpreparat och foerfarande foer dess framstaellning |
| CA1335976C (fr) * | 1989-05-31 | 1995-06-20 | Mahmoud Kamran Azarniouch | Recuperation de naoh et d'autres produits a partir de liqueurs usees et d'effluents d'usines de blanchiment |
| US5096540A (en) * | 1990-04-06 | 1992-03-17 | Sell Nancy J | Method for recycling sulfur dioxide from sulfite pulping liquors |
| FI102395B1 (fi) * | 1991-11-26 | 1998-11-30 | Ahlstrom Machinery Oy | Menetelmä energian talteenottamiseksi selluprosessien jäteliemistä |
| US5635024A (en) * | 1993-08-20 | 1997-06-03 | Bountiful Applied Research Corporation | Process for separating lignins and dissolved organic compounds from kraft spent liquor |
| JP3024526B2 (ja) | 1995-10-11 | 2000-03-21 | 日本製紙株式会社 | リグニン組成物、その製造方法及びそれを用いたセメント分散剤 |
| FI961930A (fi) * | 1996-05-07 | 1997-11-08 | Ahlstrom Machinery Oy | Menetelmä ja laitteisto alkalisen sellunvalmistusprosessin tehostamiseksi |
| TR199902246T2 (xx) * | 1997-03-20 | 1999-12-21 | Granit S.A. | Aromatik polimerler i�eren alkali sol�syonlar�n�n haz�rlanmas� i�in y�ntem. |
| US5777086A (en) * | 1997-05-12 | 1998-07-07 | Thermo Fibergen, Inc. | Method of recovering lignin from pulp and paper sludge |
| CA2345394A1 (fr) | 1998-09-24 | 2000-03-30 | Kenneth R. Kurple (Deceased) | Procede de preparation de pate sans four de recuperation |
| US6589427B2 (en) * | 2001-02-28 | 2003-07-08 | Council Of Scientific & Industrial Research | Process for treatment of mixture of spent wash from distillery and black liquor from pulp and paper industry |
| US20020129910A1 (en) * | 2001-03-14 | 2002-09-19 | Lightner Gene E. | Separation of black liquor to produce lignins substantially free of sodium |
| EP1302529A1 (fr) * | 2001-10-09 | 2003-04-16 | Linde AG | Séparation d'eau salée pendant la préparation de savon de tallol |
| US7189306B2 (en) * | 2002-02-22 | 2007-03-13 | Gervais Gibson W | Process of treating lignocellulosic material to produce bio-ethanol |
| US20030221804A1 (en) * | 2002-06-03 | 2003-12-04 | Lightner Gene E. | Lignins derived from black liquor |
| CA2452145A1 (fr) * | 2003-06-03 | 2004-12-03 | David Tarasenko | Methode de production de pate et de lignine |
| FI117507B (fi) * | 2004-07-09 | 2006-11-15 | Kemira Oyj | Menetelmä ligniinin poistamiseksi vedestä |
| SE0402201D0 (sv) * | 2004-09-14 | 2004-09-14 | Stfi Packforsk Ab | Method for separating lignin from black liquor |
| US8172981B2 (en) * | 2004-09-14 | 2012-05-08 | Lignoboost Ab | Separating lignin from black liquor by precipitation, suspension and separation |
| WO2007120091A1 (fr) * | 2006-03-16 | 2007-10-25 | Stfi-Packforsk Ab | Procédé permettant de séparer du pentose polymérique d'un liquide/d'une suspension épaisse |
-
2004
- 2004-10-07 SE SE0402437A patent/SE0402437D0/xx unknown
-
2005
- 2005-10-03 WO PCT/SE2005/001453 patent/WO2006038863A1/fr active Application Filing
- 2005-10-03 BR BRPI0517543A patent/BRPI0517543B1/pt not_active IP Right Cessation
- 2005-10-03 US US11/661,412 patent/US8815052B2/en not_active Expired - Fee Related
- 2005-10-03 CA CA2580834A patent/CA2580834C/fr not_active Expired - Fee Related
- 2005-10-03 ES ES05788548T patent/ES2368553T3/es active Active
- 2005-10-03 AT AT05788548T patent/ATE513082T1/de active
- 2005-10-03 ZA ZA200701627A patent/ZA200701627B/en unknown
- 2005-10-03 EP EP05788548A patent/EP1797236B1/fr not_active Not-in-force
- 2005-10-03 JP JP2007535638A patent/JP4887299B2/ja not_active Expired - Fee Related
- 2005-10-03 PT PT05788548T patent/PT1797236E/pt unknown
-
2008
- 2008-03-14 ZA ZA200802400A patent/ZA200802400B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US8815052B2 (en) | 2014-08-26 |
| ES2368553T3 (es) | 2011-11-18 |
| EP1797236A1 (fr) | 2007-06-20 |
| EP1797236A4 (fr) | 2010-04-28 |
| EP1797236B1 (fr) | 2011-06-15 |
| WO2006038863A1 (fr) | 2006-04-13 |
| BRPI0517543A (pt) | 2008-10-14 |
| CA2580834A1 (fr) | 2006-04-13 |
| ATE513082T1 (de) | 2011-07-15 |
| PT1797236E (pt) | 2011-08-31 |
| JP2008516100A (ja) | 2008-05-15 |
| ZA200802400B (en) | 2009-04-29 |
| BRPI0517543B1 (pt) | 2017-02-07 |
| SE0402437D0 (sv) | 2004-10-07 |
| JP4887299B2 (ja) | 2012-02-29 |
| US20080051566A1 (en) | 2008-02-28 |
| CA2580834C (fr) | 2013-10-01 |
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