WO2014087592A1 - 原料気化供給装置 - Google Patents

原料気化供給装置 Download PDF

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Publication number
WO2014087592A1
WO2014087592A1 PCT/JP2013/006812 JP2013006812W WO2014087592A1 WO 2014087592 A1 WO2014087592 A1 WO 2014087592A1 JP 2013006812 W JP2013006812 W JP 2013006812W WO 2014087592 A1 WO2014087592 A1 WO 2014087592A1
Authority
WO
WIPO (PCT)
Prior art keywords
raw material
control device
gas
flow rate
receiving tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2013/006812
Other languages
English (en)
French (fr)
Japanese (ja)
Inventor
敦志 日高
正明 永瀬
哲 山下
西野　功二
池田　信一
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujikin Inc
Original Assignee
Fujikin Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fujikin Inc filed Critical Fujikin Inc
Priority to US14/650,496 priority Critical patent/US9994955B2/en
Priority to CN201380057690.8A priority patent/CN104822858B/zh
Priority to KR1020157003850A priority patent/KR101613141B1/ko
Publication of WO2014087592A1 publication Critical patent/WO2014087592A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/448—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
    • C23C16/4481—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials by evaporation using carrier gas in contact with the source material
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/448—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
    • C23C16/4481—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials by evaporation using carrier gas in contact with the source material
    • C23C16/4482—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials by evaporation using carrier gas in contact with the source material by bubbling of carrier gas through liquid source material
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/448—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
    • C23C16/4485—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials by evaporation without using carrier gas in contact with the source material
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/52—Controlling or regulating the coating process
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C9/00—Methods or apparatus for discharging liquefied or solidified gases from vessels not under pressure
    • F17C9/02—Methods or apparatus for discharging liquefied or solidified gases from vessels not under pressure with change of state, e.g. vaporisation
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F22—STEAM GENERATION
    • F22B—METHODS OF STEAM GENERATION; STEAM BOILERS
    • F22B1/00—Methods of steam generation characterised by form of heating method
    • F22B1/28—Methods of steam generation characterised by form of heating method in boilers heated electrically
    • F22B1/284—Methods of steam generation characterised by form of heating method in boilers heated electrically with water in reservoirs
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F22—STEAM GENERATION
    • F22B—METHODS OF STEAM GENERATION; STEAM BOILERS
    • F22B1/00—Methods of steam generation characterised by form of heating method
    • F22B1/28—Methods of steam generation characterised by form of heating method in boilers heated electrically
    • F22B1/284—Methods of steam generation characterised by form of heating method in boilers heated electrically with water in reservoirs
    • F22B1/285—Methods of steam generation characterised by form of heating method in boilers heated electrically with water in reservoirs the water being fed by a pump to the reservoirs

Definitions

  • MFC 1 to MFC 3 are calorific mass flow controllers
  • TC is a tank temperature controller
  • T is a raw material receiving tank
  • PR is a tank internal pressure controller
  • RTU is a reactor tube (test sample)
  • FT-IR Is an infrared spectrophotometer
  • the raw material receiving tank T is filled with dimethyl zinc (DMZn, saturated vapor pressure 15 Torr at 24 ° C.).
  • DMZn dimethyl zinc
  • the temperature in the vicinity of the reactor tube RTU and FT-IR is adjusted to a temperature of 100 to 700 ° C. by a heating device.
  • the vaporizer 1 heats the inside of the vaporization chamber 3, the vaporization chamber 3 having a plurality of compartments (three chambers in the embodiment), a vaporization promoting block body (not shown) provided in each chamber, and the vaporization chamber 3.
  • a heating device (not shown) is provided, and the vaporized source gas G flows into the high-temperature pressure flow control device 2 from the gas outlet 3e.
  • a block body and a heating device are provided in each chamber of the vaporization chamber 3, but each chamber of the vaporization chamber 3 can be a vacant chamber.
  • the high-temperature pressure type flow rate control device 2 is a well-known device, and the device main body 2a is adjustable in temperature by a heating device (not shown).
  • 22 is a downstream stop valve, and 23 is a source gas outlet.
  • the wetted parts and / or the wetted parts made of stainless steel (SUS316L), Hastelloy C22 and Spron 100 are all subjected to Al 2 O 3 passivation treatment and have an average thickness of 20 nm.
  • a film mainly composed of Al 2 O 3 is uniformly formed on the entire wetted part and / or the wetted part.
  • Al 2 O 3 passivation treatment is performed, but Cr 2 O 3 passivation treatment may be performed instead. In some cases, it is also possible to perform Al 2 O 3 passivation treatment on some devices and Cr 2 O 3 passivation treatment on other devices.
  • FIG. 4 is a block configuration diagram of the raw material vaporization supply apparatus according to the second embodiment, and the configuration of the raw material vaporization supply apparatus is the same as the apparatus shown in FIGS.
  • the pressure detector of the high-temperature pressure flow controller 2 is a Hastelloy C22
  • the diaphragm constituting the valve body of the high-temperature pressure flow controller 2 is a spron 100.
  • the gas installation part and the liquid contact part of the equipment are all formed of stainless steel (SUS316L).
  • FIG. 7 is a block diagram of the raw material vaporization supply apparatus according to the third embodiment, and the configuration of the raw material vaporization supply apparatus is the same as that shown in FIG.
  • the pressure detector of the high-temperature pressure-type flow control device 2 is a Hastelloy C22
  • the diaphragm constituting the valve body part of the high-temperature-type pressure-type flow control device 2 is a spron 100.
  • the gas contact part and the liquid contact part of the devices are all formed of stainless steel (SUS316L).

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Sustainable Energy (AREA)
  • Sustainable Development (AREA)
  • Thermal Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Vapour Deposition (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
PCT/JP2013/006812 2012-12-06 2013-11-20 原料気化供給装置 Ceased WO2014087592A1 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US14/650,496 US9994955B2 (en) 2012-12-06 2013-11-20 Raw material vaporization and supply apparatus
CN201380057690.8A CN104822858B (zh) 2012-12-06 2013-11-20 原料气化供给装置
KR1020157003850A KR101613141B1 (ko) 2012-12-06 2013-11-20 원료 기화 공급 장치

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2012267021A JP5837869B2 (ja) 2012-12-06 2012-12-06 原料気化供給装置
JP2012-267021 2012-12-06

Publications (1)

Publication Number Publication Date
WO2014087592A1 true WO2014087592A1 (ja) 2014-06-12

Family

ID=50883034

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2013/006812 Ceased WO2014087592A1 (ja) 2012-12-06 2013-11-20 原料気化供給装置

Country Status (6)

Country Link
US (1) US9994955B2 (enExample)
JP (1) JP5837869B2 (enExample)
KR (1) KR101613141B1 (enExample)
CN (1) CN104822858B (enExample)
TW (1) TWI503443B (enExample)
WO (1) WO2014087592A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10646844B2 (en) 2015-04-30 2020-05-12 Fujikin Incorporated Vaporization supply apparatus

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JP6712440B2 (ja) * 2015-03-13 2020-06-24 株式会社堀場エステック 液体材料気化装置、液体材料気化システム
JP6627474B2 (ja) * 2015-09-30 2020-01-08 東京エレクトロン株式会社 原料ガス供給装置、原料ガス供給方法及び記憶媒体
DE102016208166A1 (de) * 2016-05-12 2017-11-16 Robert Bosch Gmbh Kraftstoffversorgungssystem für eine gasbetriebene Brennkraftmaschine und Verfahren zum Betreiben eines Kraftstoffversorgungssystems
US20190257551A1 (en) * 2016-09-28 2019-08-22 Clean Planet Inc. Heat generating system
JP6948803B2 (ja) 2017-03-02 2021-10-13 東京エレクトロン株式会社 ガス供給装置、ガス供給方法及び成膜方法
JP6877188B2 (ja) * 2017-03-02 2021-05-26 東京エレクトロン株式会社 ガス供給装置、ガス供給方法及び成膜方法
WO2019021948A1 (ja) * 2017-07-25 2019-01-31 株式会社フジキン 流体制御装置
JP7097085B2 (ja) 2017-07-25 2022-07-07 株式会社フジキン 流体制御装置
CN108128955A (zh) * 2017-12-27 2018-06-08 江苏南大光电材料股份有限公司 含mo源溶剂的回收装置及其方法
US11788190B2 (en) * 2019-07-05 2023-10-17 Asm Ip Holding B.V. Liquid vaporizer
KR102767031B1 (ko) * 2019-08-29 2025-02-14 가부시키가이샤 후지킨 유체 공급 시스템
JP7577339B2 (ja) 2019-09-19 2024-11-05 株式会社フジキン 気化供給装置
US20230002900A1 (en) 2019-12-16 2023-01-05 Fujikin Incorporated Vaporization supply method and vaporization supply device
JP7412747B2 (ja) * 2020-01-30 2024-01-15 株式会社フジキン 圧電素子駆動式バルブ、圧力式流量制御装置及び気化供給装置
DE102020001894A1 (de) 2020-03-24 2021-09-30 Azur Space Solar Power Gmbh Metallorganische chemische Gasphasenepitaxie- oder Gasphasenabscheidungsvorrichtung
JP7470375B2 (ja) * 2020-03-30 2024-04-18 株式会社フジキン 流体制御装置及びこれを用いた流体制御システム
KR102323922B1 (ko) * 2020-05-18 2021-11-09 주식회사 제이원테크코리아 발광분광분석기의 아르곤 가스 유지관리 시스템 및 그 방법
DE102021117457A1 (de) 2021-07-06 2023-01-12 Aixtron Se Verdampfungsquelle für einen CVD-Reaktor
CN117305099B (zh) * 2023-10-08 2024-05-14 安徽贝宝食品有限公司 一种可旋转全自动发酵设备及方法
WO2025096119A1 (en) * 2023-10-31 2025-05-08 Lam Research Corporation Vapor delivery system with charge volume container

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JPH08288282A (ja) * 1995-04-18 1996-11-01 Asahi Chem Ind Co Ltd 半導体装置用絶縁膜の製造方法
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JP2009252760A (ja) * 2008-04-01 2009-10-29 Fujikin Inc 気化器を備えたガス供給装置
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10646844B2 (en) 2015-04-30 2020-05-12 Fujikin Incorporated Vaporization supply apparatus

Also Published As

Publication number Publication date
CN104822858A (zh) 2015-08-05
JP2014114463A (ja) 2014-06-26
KR20150030770A (ko) 2015-03-20
KR101613141B1 (ko) 2016-04-18
US9994955B2 (en) 2018-06-12
CN104822858B (zh) 2017-08-01
US20150322567A1 (en) 2015-11-12
JP5837869B2 (ja) 2015-12-24
TWI503443B (zh) 2015-10-11
TW201441412A (zh) 2014-11-01

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