WO2013054906A1 - たばこ製品用香喫味有用成分の増強方法、たばこ原料、シガレットおよび葉巻 - Google Patents
たばこ製品用香喫味有用成分の増強方法、たばこ原料、シガレットおよび葉巻 Download PDFInfo
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- WO2013054906A1 WO2013054906A1 PCT/JP2012/076494 JP2012076494W WO2013054906A1 WO 2013054906 A1 WO2013054906 A1 WO 2013054906A1 JP 2012076494 W JP2012076494 W JP 2012076494W WO 2013054906 A1 WO2013054906 A1 WO 2013054906A1
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- fragrance
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
Definitions
- the present invention relates to a method for enhancing a flavorful ingredient for tobacco products, a tobacco material, a cigarette and a cigar.
- Tobacco products are added with flavors to improve the flavor.
- Various attempts have been made to improve fragrances due to demands from smokers for better savory tastes, changes in taste, a tendency to decrease the amount of mainstream smoke tar in the entire cigarette (decrease in flavor), or reduction in manufacturing costs. It is.
- the main raw materials for fragrances for tobacco products are natural product-derived sugars and plant-derived extracts.
- a method is known in which a necessary substance is added to the original extract or processed to be modified.
- a modification method in which a necessary substance is added to or processed in a plant extract may cause an extreme change in the content of the original extract and may impair the characteristics of the original extract.
- the effects of plant extracts may change over time.
- tea leaf steam distilled liquid is heated at a temperature of 100 ° C. or less to extract a first extract, and ascorbic acid is added to the tea leaf steam distillation residue to obtain a second extract.
- Japanese Patent Application Laid-Open No. 2009-219488 discloses a method in which a mixed liquid of coffee extract, saccharide and water is heated at 130 to 180 ° C. for 10 minutes or more to cause an aminocarbonyl reaction to increase aroma components.
- the aroma component is a furan compound other than furfural.
- Japanese Patent Application Laid-Open No. 2002-272408 describes that an extract is produced by the following method. First, an unheated juice of an edible plant is heat-treated at 70 to 135 ° C. for 2 to 15 minutes under no pressure. Subsequently, the juice after the heat treatment is heat-treated at a pressure of 1.2 to 3.2 MPA at 105 to 135 ° C. for 2 to 8 minutes to form an aggregate. Thereafter, by removing the agglomerates, an extract having an increased sweetness and umami and almost no aroma is produced.
- JP-A-2-245169 discloses a method for producing a bouillon having excellent quality such as flavor by mixing an animal extract and a plant extract and heating them at 80 to 100 ° C. for 15 minutes or more.
- the present invention does not cause an extreme change in its components from at least one fragrance raw material selected from the group consisting of saccharides derived from natural products, plant bases, and liquid extracts obtained by extracting or concentrating plant bases, It is an object of the present invention to provide a method for enhancing a flavorful ingredient for tobacco products that can efficiently enhance a flavorful ingredient (or group of ingredients).
- the present invention contains a fragrance raw material containing a flavorful useful component enhanced by the above method, and the fragrance, flavor (flavor) without changing the original fragrance, flavor (flavor) of the fragrance raw material by burning during smoking
- the purpose is to provide a tobacco material with enhanced fortification.
- the present invention comprises a tobacco raw material containing a fragrance raw material containing a flavorful useful ingredient enhanced by the above method, and the fragrance without changing the original fragrance, flavor (flavor) of the fragrance raw material by burning during smoking
- An object of the present invention is to provide a cigarette and cigar with enhanced flavor (flavor).
- a method for enhancing a flavorful useful ingredient for tobacco products is provided.
- a tobacco raw material containing a fragrance raw material containing a flavorful useful component enhanced by the method described in the first aspect.
- a cigarette provided with a tobacco raw material containing a raw material for a fragrance containing a flavorful useful component enhanced by the method described in the first aspect.
- a cigar provided with a tobacco raw material containing a fragrance raw material containing a flavor-enhancing useful component enhanced by the method described in the first aspect.
- FIG. 6 is a graph showing the rate of increase of 2,5-dioxyfructosazine and 2,6-dioxyfructosazine in the carob extract treated in Example 6. It is a figure which shows the quantity of DDMP and 5-HMF in the honey after the enhancement process by Example 11 in GC / MS measurement, and before the enhancement process. It is a figure which shows the quantity of DDMP and 5-HMF in the honey after the enhancement process by Example 14 in GC / MS measurement, and before the enhancement process.
- FIG. 6 is a graph showing the rate of increase of 2,5-dioxyfructosazine and 2,6-dioxyfructosazine in the carob extract treated in Example 6. It is a figure which shows the quantity of DDMP and 5-HMF in the honey after the enhancement process by Example 11 in GC / MS measurement, and before the enhancement process. It is a figure which shows the quantity of DDMP and 5-HMF in the honey after the enhancement process by Example 14 in GC
- Example 14 shows the increase in DDMP and 5-HMF in honey enhanced in Example 11 and Example 14. It is a figure which shows the quantity of DDMP and 5-HMF in the honey after the enhancement process by Example 16 in GC / MS measurement, and before the enhancement process. It is a figure which shows the quantity of 3-hydroxy- ⁇ -damascon and 4-vinyl guaiacol in the mate tea extract after the enhancement treatment according to Example 22 and before the enhancement treatment in the GC / MS measurement.
- FIG. 22 is a graph showing the rate of increase of 3-hydroxy- ⁇ -damascone and 4-vinylguaiacol in the mate tea extract enhanced in Example 22.
- the method for enhancing a flavorful ingredient for tobacco products according to the first embodiment is for at least one fragrance selected from the group consisting of sugars derived from natural products, plant active ingredients, and liquid extracts obtained by extracting or concentrating plant active ingredients.
- a step of preparing the raw material (first step), a step of storing the fragrance raw material in the pot in a volume of 50 to 80% by volume with respect to the volume of the pot (second step), A step of heating the fragrance raw material to 80 ° C. to 100 ° C.
- savory taste useful ingredient means an ingredient (or ingredient group) that contributes to aroma and flavor (flavor) when placed in combustion during smoking.
- the processing from the first step to the fourth step is performed, and in particular, the heating temperature in the third step and the cooling rate during cooling in the fourth step are defined.
- a flavorful ingredient at least one selected from the group consisting of a saccharide derived from a natural product that is a raw material for perfume, a plant raw material, and a liquid extract obtained by extracting or concentrating the plant raw material. It is possible to provide a method for enhancing a flavorful useful ingredient for tobacco products, which is capable of significantly enhancing a component sometimes useful as a flavorful taste.
- the fragrance raw material with enhanced savory ingredients is contained in the tobacco raw material and placed under heating by combustion during smoking, so that the savory useful ingredients in the fragrance raw materials are pyrolyzed into volatile components. Or evaporated and stripped. For this reason, complex roasty fragrance and flavor (flavor) are expressed.
- saccharides derived from natural products in the fragrance raw material used in the first step include polysaccharides such as honey and starch.
- Examples of the plant base in the fragrance raw material used in the first step include mate tea and green tea.
- the liquid extract in the fragrance raw material used in the first step is a seed extract such as carob extract, coffee extract, cocoa extract, fenugreek extract, malt extract; leaf quality such as tea leaf extract, camomil extract, rosemary extract. System extracts; and the like.
- flavor used at the 1st process may be a mixture of two or more selected from the group consisting of sugars derived from natural products, plant active ingredients and liquid extracts.
- the volume ratio of the fragrance raw material to the volume of the kettle is less than 50% by volume, the volume of the fragrance raw material to be treated in the kettle is reduced, and the processing efficiency for enhancing the flavorful ingredients is enhanced. May fall.
- the volume ratio of the fragrance raw material with respect to the volume of the kettle exceeds 80% by volume, it is difficult to efficiently enhance the savory useful components in the fragrance raw material in stirring and heat treatment.
- the rotation speed of the stirring blade is preferably 15 to 100 rpm.
- the third step it is possible to efficiently enhance the flavorful ingredients in the fragrance raw material by heating to 80 ° C to 100 ° C at a temperature increase rate of 1.0 to 2.0 ° C / min. become.
- the heating temperature is less than 80 ° C., it is difficult to sufficiently enhance the savory component in the fragrance material.
- the heating temperature exceeds 100 ° C., there is a possibility that the flavorful useful component in the fragrance raw material may be altered.
- the heating temperature is preferably maintained for 240 minutes or less.
- the lower limit of the holding time is preferably 30 minutes.
- the fourth step it is possible to more efficiently enhance the flavorful useful components in the fragrance raw materials by regulating the cooling rate during cooling to 0.40 to 0.85 ° C./min.
- the cooling rate during cooling is out of the above range, it is difficult to sufficiently enhance the flavorful useful components in the fragrance raw material.
- the ultimate cooling temperature by “cooling to a desired temperature” varies depending on the kind of the fragrance raw material, but is usually preferably 40 to 60 ° C.
- the inside of the kettle in the second to fourth steps may be atmospheric pressure or a pressurized state higher than atmospheric pressure.
- the pressurization is preferably 0.105 to 0.11 MPa.
- the tobacco raw material which concerns on 2nd Embodiment contains the raw material for fragrance
- tobacco materials include tobacco lamina, tobacco tobacco, reconstituted tobacco, puffed tobacco, tobacco bone, tobacco tobacco, cigarette filters, cigarette glue, pipe tobacco, cigar materials (fillers, binders, and wrappers). be able to.
- the content of the fragrance raw material in the tobacco raw material is appropriately selected depending on the type of the tobacco raw material.
- the thermal decomposition of the enhanced flavorful useful component in the fragrance raw material without changing the original fragrance and flavor (flavor) of the fragrance raw material by combustion during smoking, or Tobacco raw materials with enhanced aroma and flavor (flavor) by evaporation and volatilization can be provided.
- the cigarette which concerns on 3rd Embodiment is provided with the tobacco raw material containing the raw material for fragrance
- a specific cigarette for example, a cigarette with a filter
- a specific cigarette for example, a cigarette with a filter
- the cigarette with a filter includes a tobacco rod 1 and a filter 2 having a circumference equal to or thinner than that of the tobacco rod 1.
- the tobacco rod 1 and the filter 2 are abutted with each other at the end, and the tobacco rod 1 and the filter 2 are integrated by encapsulating the entire outer peripheral surface of the filter 2 and the outer peripheral surface portion of the tobacco rod 1 in the vicinity of the butting with the tip paper 3. ing.
- the tobacco rod 1 is formed by encapsulating a tobacco ingot 4 with a wrapping paper 5 in a cylindrical shape.
- the filter 2 is formed of, for example, a filter material (not shown) formed by bundling or folding non-woven fabrics of acetate fiber or pulp, and plug paper (molded paper) 6 in which the filter material is spread in a columnar shape. Has been.
- the tobacco 4 of the tobacco rod 1 contains a flavoring material containing a flavorful component enhanced by the method of the first embodiment, or the filter material of the filter 2 is the method of the first embodiment.
- flavor useful component reinforced by is contained.
- the combustion at the time of smoking is provided by providing the filter material (or tobacco stamp 4) containing the raw material for fragrance
- the filter material (or tobacco engraving 4) the fragrance raw material inherent aroma, without changing the flavor (flavor), thermal decomposition or evaporation of the enhanced flavor useful component in the fragrance raw material, Cigarettes with enhanced aroma and flavor (flavor) can be provided by volatilization.
- the cigar includes, for example, a cylindrical filler 11, a binder 12 that encloses the outer peripheral surface including the suction port (right end in FIG. 2) of the filler 11, a wrapper 13 that encapsulates the entire binder, and the outer periphery of the wrapper 13 near the suction port. And a ring 14 attached to the surface.
- the edge part (left end of FIG. 2) opposite to a suction mouth becomes a fired part. All of the filler 11, binder 12 and wrapper 13 are made from leaf tobacco.
- the filler 11 contains a fragrance raw material containing a savory useful component enhanced by the method of the first embodiment.
- the filler 11 containing the raw material for fragrance
- the fragrance and flavor (flavor) were enhanced by thermal decomposition, evaporation, or volatilization of the enhanced flavorful useful component in the fragrance raw material.
- Cigars can be provided.
- Example 1 Carob extract> A 600 liter kettle (manufactured by Kajiwara Co., Ltd .: Leonida KHM-6FT) equipped with a stirring mechanism having a stirring blade and a heating / cooling mechanism having a jacket was prepared. Moreover, after extracting with hydrous alcohol, the carob extract concentrated to Brix 75 (water content of 25 weight%) under normal pressure was prepared.
- the contents in the kettle were cooled to 50 ° C. at a temperature lowering rate of 0.42 ° C./min after maintaining the temperature while continuing stirring with the stirring blades. Cooling was performed by circulating water through the jacket and adjusting the water temperature.
- Nonvolatile pyrazines (2,5-dioxyfructosazine [hereinafter referred to as 2,5-DFS]) and 2,6-dioxyfract which are useful flavor components in the carob extract treated in Examples 1 to 10
- the amount of sajin [hereinafter referred to as 2,6-DFS] was measured by the following method.
- the temperature rising rate was 1.0 to 2.0 ° C./min
- the heating temperature was 80 ° C. to 100 ° C.
- the temperature falling rate during cooling was 0.40.
- the carob extract treated in Examples 2-6 and 8 set to a range of ⁇ 0.85 ° C./min is significantly enhanced in the amount of non-volatile pyrazines without causing an extreme change in the content of the carob extract. Confirmed.
- Example 4 (heating rate 1.5 ° C./min, heating temperature 100 ° C., holding time 60 minutes during heating, cooling rate 0.42 ° C./cooling during cooling)
- the increase rate of nonvolatile pyrazines (2,5-dioxyfructosazine and 2,6-dioxyfructosazine) in the carob extract treated with (set to minutes) is shown in FIG.
- the carob extracts treated in Examples 2-6 and 8 have enhanced flavor (flavor) compared to the carob extracts treated in Examples 1, 7, 9, and 10.
- Example 11 Honey> A pressure-resistant kettle with an internal volume of 2000 rills equipped with a stirring mechanism with stirring blades and a heating / cooling mechanism with a jacket (manufactured by Daikoh Processing Co., Ltd .: vertical cylindrical jacket type heater FM-14) is available. did.
- the contents in the kettle were cooled to 50 ° C. at a temperature drop rate of 0.42 ° C./min after maintaining the temperature. Cooling was performed by circulating water through the jacket and adjusting the water temperature.
- Example 12 to 21 Honey> The honey was treated in the same manner as in Example 11 except that the conditions in the pot internal pressure, temperature increase rate, heating temperature, holding time during heating, and temperature decrease rate shown in Table 2 below were set.
- the heating rate was 1.0 to 2.0 ° C./min
- the heating temperature was 80 ° C. to 100 ° C.
- the cooling rate during cooling was 0.40.
- Example 11 Example 14, and Example 16 will be specifically described below.
- Example 11 in GC / MS measurement shows the amounts of DDMP and 5-HMF in the honey after the enhancement treatment with and before the enhancement treatment. From the results of FIG. 4, in Example 11, there is no difference between DDMP and 5-HMF, which are fragrance components before and after the enhancement treatment, and no significant increase in the fragrance component due to the enhancement treatment is observed.
- Example 14 in GC / MS measurement (temperature increase rate set to 1.5 ° C./min, heating temperature 100 ° C., heating holding time 30 minutes, cooling temperature decreasing rate 0.42 ° C./min)
- the amounts of DDMP and 5-HMF in the honey after the enhancement treatment with and before the enhancement treatment are shown in FIG. From the results shown in FIG. 5, it is recognized that in Example 14, the aromatic components DDMP and 5-HMF are remarkably increased before and after the enhancement treatment. Moreover, the change of other aroma components is not seen and it is recognized that the content component has not changed.
- Example 11 The increase rate of DDMP and 5-HMF in honey enhanced in Example 11 and Example 14 is shown in FIG.
- FIG. 7 shows the amounts of DDMP and 5-HMF in the honey after the enhancement treatment with and before the enhancement treatment. From the results of FIG. 7, it is recognized that in Example 16, the aroma components DDMP and 5-HMF are significantly increased before and after the enhancement treatment. Moreover, the change of other aroma components is not seen and it is recognized that the content component has not changed.
- DDMP is present in a small amount in honey as a precursor of maltol.
- DDMP itself is odorless, it thermally decomposes to produce a fragrant (smelly odor) fragrance and flavor (flavor) similar to maltol.
- honey-like aroma was enhanced by increasing 5-HMF.
- Example 11 to 21 Further, the honey treated in Examples 11 to 21 was added, and the effect of enhancing the flavor (flavor) when smoked was evaluated by a sensory test. The results are shown in Table 2 below. The evaluation rank is the same as in Example 1-10.
- the honey treated in Examples 12-20 has a stronger flavor (flavor) than the honey treated in Examples 11 and 21.
- Example 22 Mate tea> A 600 liter kettle (manufactured by Kajiwara Co., Ltd .: Leonida KHM-6FT) equipped with a stirring mechanism having a stirring blade and a heating / cooling mechanism having a jacket was prepared.
- the volume ratio of the mate tea extract to the volume of the kettle was 62% by volume.
- the stirring blades are rotated at a rotation speed of 30 rpm, and the mate tea extract in the kettle is stirred, while the liquid is heated at a rate of 1.50 ° C./min. Warm to 95 ° C. Heating was performed by circulating steam through the jacket and adjusting the amount of steam. Subsequently, the mixture was concentrated to Brix.73 at a temperature in the kettle of 95 ° C. ⁇ 5 ° C. while stirring with the stirring blade was continued. This time was 60 minutes.
- the contents in the kettle were cooled to 50 ° C. at a temperature lowering rate of 0.84 ° C./min after the temperature was maintained while continuing stirring with the stirring blades. Cooling was performed by circulating water through the jacket and adjusting the water temperature.
- Examples 23 and 24 Mate tea> The mate tea extract was treated in the same manner as in Example 22 except that the conditions in the kettle internal pressure, temperature increase rate, heating temperature, holding time during heating, and temperature decreasing rate shown in Table 3 below were set.
- the heating rate was 1.0 to 2.0 ° C./min
- the heating temperature was 80 ° C. to 100 ° C.
- the mate tea extract treated in Example 22-24 in which the cooling rate during cooling was set in the range of 0.40 to 0.85 ° C./min did not cause an extreme change in its content component, and 3-hydroxy- ⁇ - It was confirmed that the amount of damascon and 4-vinyl guaiacol was significantly increased.
- FIG. 8 shows the amounts of 3-hydroxy- ⁇ -damascone and 4-vinylguaiacol in the mate tea extract after the enhancement treatment and before the enhancement treatment. Moreover, the increase rate of 3-hydroxy- ⁇ -damascone and 4-vinylguaiacol in the mate tea extract enhanced in Example 22 is shown in FIG.
- 3-Hydroxy- ⁇ -damascon is represented by the following structural formula and is known to exist as a component of tobacco leaves. Stimulation and bitterness can be suppressed by increasing this component.
- 4-Vinylguaiacol is represented by the following structural formula, and has a sweet spicy fragrance and gives a rich flavor (flavor and sweetness).
- 4-vinyl guaiacol produces vanillin represented by the following structural formula by oxidation.
- Example 25 Sensory evaluation of carob extract> Tobacco leaves were produced by cutting tobacco leaves (yellow seeds) with a predetermined width. 0.5% by weight of the carob extract prepared in Example 1 (without enhancement treatment) was added to this cigarette. The cigarette with the carob extract was wound into a cigarette having a winding length of 63 mm and a winding circumference of 24.9 mm.
- Example 26 Sensory evaluation of carob extract> To the same tobacco as in Example 25, 0.5% by weight of the carob extract enhanced in Example 2 was added. The tobacco cut carob extract was wound into a cigarette shape as in Example 25.
- the cigarettes obtained in Examples 25 and 26 were stored in a thermostatic oven at 70 ° C. in a sealed state for 7 hours. In addition, cigarettes before and after storage were smoked and subjected to a sensory test.
- ⁇ Score 8.0 or more A evaluation (there is an additive effect and can be used favorably), ⁇ Score from 7.0 to less than 8.0: B rating (although there are some drawbacks, it can be used), -Score less than 7.0: C rating (use is not preferred).
- Example 25 As is apparent from Table 4, it can be seen that the cigarette of Example 25 to which the carob extract without the enhancement treatment (Example 1) was added had a lower score after storage than before storage (A evaluation ⁇ B evaluation).
- Example 26 the cigarette of Example 26 to which the carob extract with enhanced treatment (Example 2) was added had a high score even before storage, and there was little difference between before and after storage (A evaluation ⁇ A evaluation). This is because the carob extract is enhanced to enhance the characteristics of “caramelic” due to the increase in non-volatile pyrazine compared to Example 25 (before storage: rating 8.3 ⁇ 9.1). Since the score is higher than that of Example 25 (average score: 7.5 ⁇ 8.0), it means that the storage resistance is excellent.
- Example 27 Sensory evaluation of honey> To the same tobacco as in Example 25, 0.5% by weight of the honey (no enhancement treatment) used in Example 11 was added. The tobacco with honey was wound into a cigarette having a winding length of 63 mm and a winding circumference of 24.9 mm.
- Example 28 Sensory evaluation of honey> To the same tobacco as in Example 25, 0.5% by weight of the honey enhanced in Example 14 was added. The tobacco with honey was wound into a cigarette shape as in Example 25.
- the cigarettes obtained in Examples 27 and 28 were stored in a thermostatic oven at 70 ° C. in a sealed state for 7 hours. In addition, cigarettes before and after storage were smoked and subjected to a sensory test.
- ⁇ Score 8.0 or more A evaluation (there is an additive effect and can be used favorably), ⁇ Score from 7.0 to less than 8.0: B rating (although there are some drawbacks, it can be used), -Score less than 7.0: C rating (use is not preferred).
- Example 11 As is apparent from Table 5, it can be seen that the cigarette of Example 27 to which the honey without enhancement treatment (Example 11) was added had a lower score after storage than before storage (A evaluation ⁇ B evaluation).
- Example 28 to which honey with enhanced treatment (Example 14) was added had a high score even before storage, and there was little difference between before and after storage (A evaluation ⁇ A evaluation).
- the cigarette of Example 28 has an enhanced “sweet taste” compared to Example 27 (score 8.6 ⁇ 9.3).
- Example 28 had little change in “sweet taste” and “flower, honey-like” even after storage (score 9.3 ⁇ 9.1, score 8.8 ⁇ 8, respectively) .7).
- Example 29 Sensory evaluation of mate tea extract> To the same tobacco as in Example 25, 0.5% by weight of the mate tea extract (without enhancement treatment) prepared in Example 22 was added. Tobacco chopped mate tea extract was wound into a cigarette with a winding length of 63 mm and a winding circumference of 24.9 mm.
- Example 30 Sensory evaluation of mate tea extract> To the same tobacco as in Example 25, 0.5% by weight of the mate tea extract enhanced in Example 24 was added. Tobacco chopped mate tea extract was wound in a cigarette shape as in Example 25.
- the cigarettes obtained in Examples 29 and 30 were stored in a thermostatic oven at 70 ° C. in a sealed state for 7 hours. In addition, cigarettes before and after storage were smoked and subjected to a sensory test.
- -Score 8.0 or more A rating (there is an additive effect and can be used favorably), ⁇ Score from 7.0 to less than 8.0: B rating (although there are some drawbacks, it can be used), -Score less than 7.0: C rating (use is not preferred).
- Example 30 to which the mate tea extract with enhanced treatment (Example 24) was added had a high score even before storage, and the difference between before and after storage was small (A evaluation ⁇ A evaluation).
- Example 30 the cigarette of Example 30 to which the mate tea extract with enhanced treatment was added had little change in “stimulation” and “tobacco flavor (flavor)” even after storage (score 8.0 to 8.0, score 8.6, respectively) ⁇ 8.4).
- an extreme change of the component is not caused from at least one fragrance raw material selected from the group consisting of saccharides derived from natural products, plant bases, and liquid extracts obtained by extracting or concentrating plant bases.
- strengthening method of the flavorful useful component for tobacco products which can efficiently enhance a flavorful useful component can be provided.
- the fragrance raw material containing a flavorful component enhanced by the above method is contained, and the fragrance, flavor (flavor) without changing the original fragrance, flavor (flavor) of the fragrance raw material by burning during smoking Tobacco raw materials with enhanced flavor can be provided.
- a tobacco raw material containing a fragrance raw material containing a flavorful component enhanced by the above method is provided, and the original fragrance and flavor (flavor) of the fragrance raw material are not changed by burning during smoking.
- Cigarettes and cigars with enhanced aroma and flavor (flavor) can be provided.
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Abstract
Description
第1実施形態に係るたばこ製品用香喫味有用成分の増強方法は、天然物由来の糖類、植物原体、および植物原体を抽出もしくは濃縮した液体エキスからなる群から選ばれる少なくとも1つの香料用原料を準備する工程(第1工程)と、釜内に前記香料用原料を釜容積量に対して50~80体積%の容率で収容する工程(第2工程)と、前記釜内にて前記香料用原料を攪拌しながら、1.0~2.0℃/分の昇温速度で80℃~100℃に加温する工程(第3工程)と、前記釜内で処理した後の内容物を0.40~0.85℃/分の降温速度で所望の温度まで冷却する工程(第4工程)と、を含む。
第2実施形態に係るたばこ原料は、第1実施形態に係る方法で増強された香喫味有用成分を含む香料用原料を含有する。
第3実施形態に係るシガレットは、第1実施形態の方法で増強された香喫味有用成分を含む香料用原料を含有するたばこ原料を備える。
第4実施形態に係る葉巻は、第1実施形態の方法で増強された香喫味有用成分を含む香料用原料を含有するたばこ原料を備える。
攪拌羽根を有する攪拌機構およびジャケットを有する加温・冷却機構を備えた内容積
600リットルの釜(カジワラ株式会社製:レオニーダーKHM-6FT)を用意した。また、含水アルコールで抽出後、常圧下でBrix 75(25重量%の水分量)まで濃縮されたキャロブエキスを用意した。
下記表1に示す釜内圧、昇温速度、加温温度、加温時の保持時間、降温速度の条件に設定した以外、例1と同様な処理をキャロブエキスに施した。
・使用機器:高速液体クロマトグラフィー Ultimate 3000 (DIONEX)、
・使用カラム:Inertsil ODS-3(150mm×3.0mm×5μm)、
・分析条件:
1) カラムオーブン;6.0℃、
2) UV;275nm、
3) 流量;0.3mL/分、
4) 注入容積;20μL。
攪拌羽根を有する攪拌機構およびジャケットを有する加温・冷却機構を備えた内容積2000リッルの耐圧釜(大興加工機製造(株)製:たて型円筒型ジャケット式加熱器FM-14)を用意した。
下記表2に示す釜内圧、昇温速度、加温温度、加温時の保持時間、降温速度の条件に設定した以外、例11と同様な処理を蜂蜜に施した。
・使用機器:Agilent 5975C、
・使用カラム:DB-WAX(60m×0.25mm×0.3μm)、
・分析条件:
1) 入口温度;250℃、
2) InletMode;Splitless、
3) カラム温度;70℃~220℃、
4) 昇温速度;2℃/分、
5) 流量ガス;He(1.0mL/分)、
6) 注入容積;2μL、
・試料調製:試料90.0gに対し、蒸留水60.0gを加え、攪拌、溶解させた溶液をジエチルエーテル150mL、50℃で6時間抽出濃縮した。
・使用機器:Agilent 6890N、
・使用カラム:TC-WAX(60m×0.25mm×0.3μm)、
・分析条件:
1) 入口温度;250℃、
2) InletMode;Splitless、
3) カラム温度;70℃~220℃、
4) 昇温速度;3℃/分、
5) 流量ガス;He(1.3mL/分)、
6) 注入容積;2μL、
・試料調製:試料90.0gに対し、蒸留水60.0gを加え、攪拌、溶解させた溶液をジエチルエーテル150mL、50℃で6時間抽出濃縮した。
攪拌羽根を有する攪拌機構およびジャケットを有する加温・冷却機構を備えた内容積
600リットルの釜(カジワラ株式会社製:レオニーダーKHM-6FT)を用意した。
下記表3に示す釜内圧、昇温速度、加温温度、加温時の保持時間、降温速度の条件に設定した以外、例22と同様な処理をマテ茶エキスに施した。
・使用機器:Agilent 5975N、
・使用カラム:DB-WAX(60m×0.25mm×0.3μm)、
・分析条件:
1) 入口温度;250℃、
2) InletMode;Splitless、
3) カラム温度;40℃~220℃、
4) 昇温速度;2℃/分、
5) 流量ガス;He(1.0mL/分)、
6) 注入容積;2μL、
・試料調製:試料90.0gに対し、蒸留水60.0gを加え、攪拌、溶解させた溶液をジエチルエーテル150mL、50℃で6時間抽出濃縮した。
たばこ葉(黄色種)を所定の刻幅で裁刻してたばこ刻を作製した。このたばこ刻に前記例1で調製したキャロブエキス(増強処理なし)を0.5重量%添加した。キャロブエキス添加たばこ刻を63mmの巻長、24.9mmの巻円周のシガレット状に巻いた。
例25と同様なたばこ刻に前記例2で増強処理したキャロブエキスを0.5重量%添加した。キャロブエキス添加たばこ刻を例25と同様にシガレット状に巻いた。
訓練された8名のパネラーにより喫煙時のシガレット(蔵置前、蔵置後:各7サンプル)について香気、香味(風味)の官能試験を行って、それらの平均を以下のように評価した。
・評点7.0以上8.0未満:B評価(やや欠点はあるが、使用は可能)、
・評点7.0未満:C評価(使用は好ましくない)。
例25と同様なたばこ刻に前記例11で用いた蜂蜜(増強処理なし)を0.5重量%添加した。蜂蜜添加たばこ刻を63mmの巻長、24.9mmの巻円周のシガレット状に巻いた。
例25と同様なたばこ刻に前記例14で増強処理した蜂蜜を0.5重量%添加した。蜂蜜添加たばこ刻を例25と同様にシガレット状に巻いた。
訓練された8名のパネラーにより喫煙時のシガレット(蔵置前、蔵置後:各7サンプル)について香気、香味(風味)の官能試験を行って、それらの平均を以下のように評価した。
・評点7.0以上8.0未満:B評価(やや欠点はあるが、使用は可能)、
・評点7.0未満:C評価(使用は好ましくない)。
例25と同様なたばこ刻に前記例22で調製したマテ茶エキス(増強処理なし)を0.5重量%添加した。マテ茶エキス添加たばこ刻を63mmの巻長、24.9mmの巻円周のシガレット状に巻いた。
例25と同様なたばこ刻に前記例24で増強処理したマテ茶エキスを0.5重量%添加した。マテ茶エキス添加たばこ刻を例25と同様にシガレット状に巻いた。
訓練された8名のパネラーにより喫煙時のシガレット(蔵置前、蔵置後:各7サンプル)について香気、香味(風味)の官能試験を行って、それらの平均を以下のように評価した。
・評点7.0以上8.0未満:B評価(やや欠点はあるが、使用は可能)、
・評点7.0未満:C評価(使用は好ましくない)。
Claims (7)
- 天然物由来の糖類、植物原体、および植物原体を抽出もしくは濃縮した液体エキスからなる群から選ばれる少なくとも1つの香料用原料を準備する工程と、
釜内に前記香料用原料を釜容積量に対して50~80体積%の容積率で収容する工程と、
前記釜内にて前記香料用原料を攪拌しながら、1.0~2.0℃/分の昇温速度で80~100℃に加温する工程と、
前記釜内で処理した後の内容物を0.40~0.85℃/分の降温速度で所望の温度まで冷却する工程と
を含むたばこ製品用香喫味有用成分の増強方法。 - 前記天然物由来の糖類は、蜂蜜、澱粉のような多糖類であり、前記植物原体はマテ茶または緑茶であり、前記液体エキスはキャロブエキス、コーヒーエキス、ココアエキス、フェヌグリークエキス、モルトエキスのような種子系エキスまたは茶葉エキス、カモミルエキス、ローズマリーエキスのような葉質系エキスである請求項1記載の方法。
- 前記加温温度80~100℃において、240分間以下保持する請求項1記載の方法。
- 前記釜内を密閉し、釜内圧力を0.105~0.11MPAに設定する請求項1記載の方法。
- 請求項1~4いずれか1項記載の方法で増強された香喫味有用成分を含む香料用原料を含有するたばこ原料。
- 請求項1~4いずれか1項記載の方法で増強された香喫味有用成分を含む香料用原料を含有するたばこ原料を備えたシガレット。
- 請求項1~4いずれか1項記載の方法で増強された香喫味有用成分を含む香料用原料を含有するたばこ原料を備えた葉巻。
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CN201280045893.0A CN103813725B (zh) | 2011-10-12 | 2012-10-12 | 用于增强烟草制品的香吸味有用成分的方法、烟草原料、香烟及雪茄烟 |
EP12839421.0A EP2767176B1 (en) | 2011-10-12 | 2012-10-12 | Method for augmenting component providing smoking flavor for tobacco product, tobacco raw material, cigarette, and cigar |
SG11201401271QA SG11201401271QA (en) | 2011-10-12 | 2012-10-12 | Method for augmenting component providing smoking flavor for tobacco product, tobacco raw material, cigarette, and cigar |
RU2014118770/12A RU2585563C2 (ru) | 2011-10-12 | 2012-10-12 | Способ усиления компонента, обеспечивающего курительный аромат табачного продукта, исходный табачный материал, сигареты и сигары |
MYPI2014700701A MY167696A (en) | 2011-10-12 | 2012-10-12 | Method for augmenting component providing smoking flavor for tobacco product, tobacco raw material, cigarette, and cigar |
PL12839421T PL2767176T3 (pl) | 2011-10-12 | 2012-10-12 | Sposób wzmacniania składnika zapewniającego aromat przy paleniu dla produktu tytoniowego, surowiec tytoniowy, papieros i cygaro |
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CN114634841A (zh) * | 2022-03-11 | 2022-06-17 | 吉林烟草工业有限责任公司 | 一种维他奶茶香精、其制备方法和一种卷烟 |
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CN106675784A (zh) * | 2017-03-13 | 2017-05-17 | 河北中烟工业有限责任公司 | 一种用于润雅香风格卷烟的加料香精 |
CN108523206B (zh) * | 2018-05-14 | 2021-06-01 | 四川三联新材料有限公司 | 雪茄风味降温调香段的制备方法以及加热不燃烧卷烟基础棒 |
CN112377813B (zh) * | 2020-10-26 | 2022-05-24 | 河南中烟工业有限责任公司 | 一种料液输送方法及系统 |
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EP2767176A1 (en) | 2014-08-20 |
PL2767176T3 (pl) | 2019-02-28 |
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JP5771697B2 (ja) | 2015-09-02 |
EP2767176B1 (en) | 2018-08-15 |
CN103813725B (zh) | 2016-08-17 |
SG11201401271QA (en) | 2014-08-28 |
JPWO2013054906A1 (ja) | 2015-03-30 |
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