WO2010082870A2 - Способ экстрагирования материалов и устройство для его осуществления - Google Patents
Способ экстрагирования материалов и устройство для его осуществления Download PDFInfo
- Publication number
- WO2010082870A2 WO2010082870A2 PCT/RU2010/000090 RU2010000090W WO2010082870A2 WO 2010082870 A2 WO2010082870 A2 WO 2010082870A2 RU 2010000090 W RU2010000090 W RU 2010000090W WO 2010082870 A2 WO2010082870 A2 WO 2010082870A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- extractant
- vacuum
- extraction
- extract
- raw material
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
- B01D11/0284—Multistage extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/12—Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0253—Fluidised bed of solid materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0261—Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
Definitions
- the invention relates to vacuum extraction technology and can be used to extract valuable biologically active components from vegetable, animal, fish, seafood and other types of raw materials used in the food and pharmaceutical industries.
- An extraction method is known (SU 1286232 BOlD 11/02), which involves grinding and evacuating a feed to a residual pressure of 20-30 kPa with pressure soaking, mixing the feed with an extractant, heating the mixture to a temperature of 40-80 0 C, periodically evacuating the mixture, and supplying heat to maintain the temperature of the mixture 5-15 0 C above the boiling point, holding at vacuum pressure, increasing the pressure to atmospheric.
- This extraction method has some operational limitations: the method does not involve the use of extractants with a boiling point at atmospheric pressure below 4O 0 C, in addition, it can be used only for extraction of raw materials with a loose structure.
- a known method of extraction of materials (patent RU 2213606 BOlD 11/02).
- the method includes grinding and heating the raw materials, degassing the raw materials and extractant, heating the extractant to a temperature of 5-15 0 C below the heating temperature of the raw materials, moreover, the degassing of the raw materials and extractant is carried out separately using pulsed evacuation with holding the mixture after each pulsed evacuation for 3 -5 minutes.
- the extraction is carried out in a vacuum-pulse mode at a temperature of 7O 0 C and a residual pressure in the receiver of 1-10 mm Hg, kept under vacuum for 5-10 minutes. with simultaneous heating. After exposure, the pressure in the extractor is increased to atmospheric.
- the above method of extracting materials has several disadvantages.
- the contact of the extractant heated under these conditions with the raw material leads to a decrease in the temperature of the mixture, which, upon subsequent evacuation, adversely affects the rate of boiling of the mixture, which necessitates heating the feedstock to a high temperature, which reduces the quality of the resulting extracts, in addition, preliminary degassing of the extractant leads to a decrease in efficiency in the initial stage of the extraction process.
- a device for extracting plant materials (RU 2225242 BOlD 11/02) is known, comprising a housing located coaxially with the housing of the cylinder, a shaft with an agitator, a cover with a drive and nozzles, a bottom.
- the case is equipped with a hatch with a squeezing device.
- a pulsation chamber is made on the lid, connected with an external generator of pneumatic pressure pulses.
- the closest in technical essence and the achieved effect is the invention (RU 2163827 BOlD 11/02 "Method of extracting materials)), taken as a prototype.
- the method includes the steps of preparing raw materials and extractant, contacting the components, extraction. Crushed and heated to a working temperature that does not reach the temperature of product denaturation, the raw material is subjected to degassing by pulsed evacuation, holding under vacuum for 1-3 minutes, resulting in the removal of gases located between the particles of the raw material in the capillaries and on the surface of the material.
- Extractant raw materials
- a rapid vacuum is released, and the raw materials are impregnated with an extractant.
- the mixture is heated at atmospheric pressure, pulsed vacuum, kept under vacuum.
- the mixture boils, due to overheating of the feedstock and the extractant, diffusion of the target components of the feedstock to the volume of the extractant proceeds. After boiling the extractant, the pressure in the system is increased to atmospheric, the extractant is impregnated with the extractant.
- the method provides the following modes: during preparation and extraction of raw materials - evacuation to a residual pressure of 0.1-13.3 kPa with a time to reach vacuum and discharge - 0.5-1.0 sec, exposure time under vacuum 1.0-10.0 min The extraction cycles are repeated until the maximum completeness of the extraction of valuable components from raw materials.
- the total extraction time is from 30 to 180 minutes.
- a device that is described in the patent (RU 2213606 BOlD 11/02), which implements this method of extraction and is taken as a prototype of the proposed device, containing a container for the extractant and an extractor connected by a pipe through quick-acting valves to each other, with a condensate collector and a receiver, a vacuum pump connected to the receiver, a reflux condenser is installed above the extractor, which provides condensation of the extractant vapor, a heater and a pump, which provide heating and supply of heating fluid to the jacket of the extractant tank extractor.
- the objective of the present invention is to develop an extraction method and a device that implements this method, which allows to increase the operational capabilities of the process by creating conditions for the extraction of various types of biological raw materials using a minimum amount of extractant and at the same time increasing the intensity of the process, the yield of extracted biologically active substances, improving their quality and catch essential oils.
- thermo-vacuum impulse extraction liquid extract is subjected to vacuum-pulse filtration, evaporated to low temperature thermo vacuum-pulsed mode for the purpose of concentration and subsequent drying.
- the installation including an extractor connected through valves to a pipe with a reflux condenser, an extractant tank and an extract collector, connected by pipelines to each other and to a receiver connected to a vacuum pump.
- the installation is equipped at the inlet of the extractor with a serially mounted screw batcher connected through an intermediate tank to the tank
- extractant and continuous heated rollers equipped with a receiving mesh container for collecting pulp impregnated on the rollers soaked in extractant.
- Two vacuum filters are mounted in the installation, connected by pipelines to the extract collector and storage tank.
- the unit has two condensers, cooled by various refrigerants, connected
- an anti-foam agent is additionally mounted above the reflux condenser, which is connected by a pipeline to a common vacuum line.
- extraction unit is equipped with a second extractor mounted parallel to the first, which is connected by piping through valves with a reflux condenser and the capacity of the extractant.
- the difference lies in a different mode of preparation and contacting of raw materials and extractant, in a different embodiment of the device for implementing these
- the fibrillar structure of the raw material undergoes partial destruction due to shear deformations, which improves wetting and impregnation of the raw material and creates conditions for a more efficient and intensive
- thermo-vacuum-pulse extraction of raw materials, filtration and Concentration (evaporation) of the resulting extract gives off valuable volatile essential oils, therefore, to eliminate losses, they are captured, separated from water vapor in condensers and collected in a collector, which increases the overall
- Vacuum-pulse filtration of the extract allows to increase the quality of its purification, that is, to improve the quality of the resulting final product.
- the drawing shows the installation of extraction of materials, which includes a screw dispenser 1, in the hopper of which is fed the feedstock and
- the extractant is dosed from the intermediate tank 2.
- Rollers 3 are installed under the screw batcher for the preliminary extraction process.
- the pulp obtained on the rollers, impregnated with the extractant, is collected in a receiving mesh container 4 of the tank 5.
- the plant has extractors 6 in which
- a reflux condenser 7 is installed above the extractors, which is connected to them through valves 24 of the common pipeline 23.
- a defoamer 8. is mounted above the reflux condenser 8. The extractant is fed into the intermediate container and into the extractors from the extractant container 9. The resulting extract is collected in the extractor 10 after vacuum-pulse filtration
- Raw materials are washed, cleaned of impurities.
- the extractant is heated in a container 9 to an operating temperature of the process that does not reach the temperature of denaturation of the qualitative characteristics of the valuable components of the raw material.
- an extractant distilled water or
- 190 pulp mixed with the extractant is installed in one of the extractors 6, with a heating jacket, which are connected to a vacuum post through a vacuum line by a quick-acting valve 19.
- Two extractors are provided in the installation to ensure the continuity of the process, the mixture is heated in one extractor, and the other is evacuated and vice versa.
- extractant 9 the heated extractant is fed into the extractor, so that the total module (extractant: raw material) is not more than 4.
- a rapid vacuum is released (for 0.5-1.0 s), the mixture is kept under vacuum for 1-3 minutes. Connect the extractor to the atmosphere.
- residual gases and vapors are removed from the surface and from the inner layers of the raw material, its specific gravity increases
- Thermo-vacuum-pulse extraction is carried out at operating temperature. Pre-extraction on rollers allows the process
- the mixture is heated, the mixture is pulsed evacuating with the specified parameters (vacuum depth, mixture temperature, module) with a receiver pos. 17 in which pumps 18 provide a vacuum depth P of up to 1.3 kPa.
- the pulse duration of the vacuum set from the receiver to the extractor is 0.5-1.0 s. Fibrillar is partially destroyed
- the extract obtained from the tank 10 is fed by vacuum to a mesh filter 12 or ceramic 13.
- the extract is filtered through a filter element in a vacuum-pulse mode.
- the extract is cleared of the remains of pulp and after
- the extract is evaporated.
- the tank 11 is connected to the evacuation line by opening the high-speed valve 19. Water entering the vacuum line,
- the water vapor of the extract condenses into a condenser 14 cooled by cold water, and essential oils are captured by a condenser 14 cooled by a refrigerant.
- the condensate from the condensers is collected respectively in the collectors 15.
- the wet concentrated extract is sent for drying to the required residual moisture.
- the transportation of the extract, 235 extractant in pipelines and apparatuses occurs under the influence of vacuum in the absence of special mechanical means of pumping.
- the total extraction time was 15 minutes.
- the extract obtained after filtration fully met the requirements of GOST 22840-77 “Licorice root extract”, the extraction time was reduced by 4 times, and the amount of extractant used was 1.5 times compared to the prototype.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mycology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Botany (AREA)
- Physics & Mathematics (AREA)
- Acoustics & Sound (AREA)
- Mechanical Engineering (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
Description
Claims
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020117017649A KR101604158B1 (ko) | 2008-12-29 | 2010-02-26 | 물질의 추출 방법 및 그를 실행하기 위한 장치 |
JP2011543465A JP5751710B2 (ja) | 2008-12-29 | 2010-02-26 | 材料を抽出する方法及び同方法を実施するための装置 |
CN201080005393.5A CN102395413B (zh) | 2008-12-29 | 2010-02-26 | 用于提取材料的方法及实施其的装置 |
EP10731436.1A EP2374516B1 (en) | 2008-12-29 | 2010-02-26 | Method for extracting materials and device for implementing same |
US13/138,038 US8674123B2 (en) | 2008-12-29 | 2010-02-26 | Method for extracting materials and device for implementing same |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
RU2008152177 | 2008-12-29 | ||
RU2008152177/15A RU2382669C1 (ru) | 2008-12-29 | 2008-12-29 | Способ экстрагирования материалов и устройство для его осуществления |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2010082870A2 true WO2010082870A2 (ru) | 2010-07-22 |
WO2010082870A3 WO2010082870A3 (ru) | 2010-10-21 |
Family
ID=42127762
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/RU2010/000090 WO2010082870A2 (ru) | 2008-12-29 | 2010-02-26 | Способ экстрагирования материалов и устройство для его осуществления |
Country Status (7)
Country | Link |
---|---|
US (1) | US8674123B2 (ru) |
EP (1) | EP2374516B1 (ru) |
JP (1) | JP5751710B2 (ru) |
KR (1) | KR101604158B1 (ru) |
CN (1) | CN102395413B (ru) |
RU (1) | RU2382669C1 (ru) |
WO (1) | WO2010082870A2 (ru) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2296470A1 (en) | 1997-07-18 | 1999-01-28 | Ardis L. Holte | Reverse circulation drilling system with bit locked underreamer arms |
RU2402368C1 (ru) * | 2010-02-03 | 2010-10-27 | Закрытое Акционерное Общество "Твин Трейдинг Компани" | Способ экстрагирования материалов и устройство для его осуществления |
CN103657139B (zh) * | 2013-11-25 | 2015-07-22 | 吉首大学 | 真空脉动式杜仲胶提取装置 |
CN104138670B (zh) * | 2014-07-08 | 2016-02-03 | 四川理工学院 | 一种山楂总黄酮的提取浓缩工艺 |
CN104096382B (zh) * | 2014-07-23 | 2016-03-16 | 安徽红星药业股份有限公司 | 茶水的提取系统 |
JP7197583B2 (ja) | 2017-08-08 | 2022-12-27 | カルテヴァット,インク. | ゴム及び副産物抽出システム及び方法 |
US11033833B2 (en) | 2017-08-08 | 2021-06-15 | Kultevat, Inc. | System and method for continuous stirred tank solvent extraction using feedstock |
CN108939606A (zh) * | 2018-09-18 | 2018-12-07 | 迪茗(上海)智能科技有限公司 | 一种提取浓缩系统及方法 |
CN110559683A (zh) * | 2019-08-12 | 2019-12-13 | 佛山市欧若拉生物科技有限公司 | 一种植物提取物专用萃取设备 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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SU1286232A1 (ru) | 1985-08-08 | 1987-01-30 | Институт технической теплофизики АН УССР | Способ экстрагировани из твердого тела |
RU2163827C2 (ru) | 1998-07-06 | 2001-03-10 | Абрамов Яков Кузьмич | Способ экстрагирования материалов |
RU2213606C1 (ru) | 2002-01-21 | 2003-10-10 | Голицын Владимир Петрович | Способ экстрагирования материалов |
RU2225242C2 (ru) | 1997-01-06 | 2004-03-10 | ОАО "Казанский завод продовольственных товаров "Алекс" | Аппарат для получения экстрактов из растительного сырья |
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GB462494A (en) * | 1935-03-02 | 1937-03-10 | Jaques Aumarechal | Improvements in and relating to the production of substances in the colloidal state |
GB912326A (en) * | 1959-12-28 | 1962-12-05 | Gunnar Koelle | Improvements in or relating to extracting a constituent extractable by a liquid in the cold from a material containing same |
US3535354A (en) | 1968-01-10 | 1970-10-20 | Blaw Knox Co | Continuous solvent extraction and dehydration system for fat and water containing tissues |
NL144490B (nl) * | 1970-08-04 | 1975-01-15 | Danske Sukkerfab | Inrichting voor continue extractie in tegenstroom. |
SU856487A1 (ru) * | 1976-06-14 | 1981-08-23 | Ленинградская Ордена Ленина Лесотехническая Академия Им.С.М.Кирова | Установка дл производства хлорофиллокаротиновой пасты |
SU856467A1 (ru) | 1979-11-20 | 1981-08-23 | Всесоюзный научно-исследовательский институт противопожарной обороны | Устройство дл получени огнетушащей пены |
DE3228927C2 (de) * | 1982-08-03 | 1991-08-14 | Extraktionstechnik Gesellschaft für Anlagenbau mbH, 2000 Hamburg | Verfahren zur kontinuierlichen Extraktion von schüttfähigen Feststoffen |
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RU2173557C2 (ru) | 1999-08-11 | 2001-09-20 | Трубников Алексей Александрович | Способ получения сухого экстракта цикория |
RU2178708C2 (ru) * | 1999-12-03 | 2002-01-27 | Трубников Алексей Александрович | Способ получения инулина |
KR100363112B1 (ko) * | 2000-04-27 | 2002-12-05 | 벤트리 주식회사 | 감태로부터 분리된 신규 물질, 이의 추출 및 정제방법, 및항산화제로 사용하는 용도 |
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-
2008
- 2008-12-29 RU RU2008152177/15A patent/RU2382669C1/ru active
-
2010
- 2010-02-26 EP EP10731436.1A patent/EP2374516B1/en not_active Not-in-force
- 2010-02-26 WO PCT/RU2010/000090 patent/WO2010082870A2/ru active Application Filing
- 2010-02-26 US US13/138,038 patent/US8674123B2/en not_active Expired - Fee Related
- 2010-02-26 JP JP2011543465A patent/JP5751710B2/ja not_active Expired - Fee Related
- 2010-02-26 KR KR1020117017649A patent/KR101604158B1/ko not_active IP Right Cessation
- 2010-02-26 CN CN201080005393.5A patent/CN102395413B/zh not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU1286232A1 (ru) | 1985-08-08 | 1987-01-30 | Институт технической теплофизики АН УССР | Способ экстрагировани из твердого тела |
RU2225242C2 (ru) | 1997-01-06 | 2004-03-10 | ОАО "Казанский завод продовольственных товаров "Алекс" | Аппарат для получения экстрактов из растительного сырья |
RU2163827C2 (ru) | 1998-07-06 | 2001-03-10 | Абрамов Яков Кузьмич | Способ экстрагирования материалов |
RU2213606C1 (ru) | 2002-01-21 | 2003-10-10 | Голицын Владимир Петрович | Способ экстрагирования материалов |
Non-Patent Citations (1)
Title |
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See also references of EP2374516A4 |
Also Published As
Publication number | Publication date |
---|---|
CN102395413A (zh) | 2012-03-28 |
US20120071675A1 (en) | 2012-03-22 |
KR20120111915A (ko) | 2012-10-11 |
RU2382669C1 (ru) | 2010-02-27 |
EP2374516A9 (en) | 2012-10-31 |
CN102395413B (zh) | 2014-12-17 |
EP2374516A4 (en) | 2013-01-16 |
WO2010082870A3 (ru) | 2010-10-21 |
JP2013520294A (ja) | 2013-06-06 |
EP2374516B1 (en) | 2014-05-14 |
JP5751710B2 (ja) | 2015-07-22 |
KR101604158B1 (ko) | 2016-03-16 |
US8674123B2 (en) | 2014-03-18 |
EP2374516A2 (en) | 2011-10-12 |
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