WO2008114771A1 - ゼオライト成形触媒を用いる炭化水素の変換方法 - Google Patents

ゼオライト成形触媒を用いる炭化水素の変換方法 Download PDF

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WO2008114771A1
WO2008114771A1 PCT/JP2008/054862 JP2008054862W WO2008114771A1 WO 2008114771 A1 WO2008114771 A1 WO 2008114771A1 JP 2008054862 W JP2008054862 W JP 2008054862W WO 2008114771 A1 WO2008114771 A1 WO 2008114771A1
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Prior art keywords
catalyst
zeolite
inorganic binder
hydrocarbons
conversion
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PCT/JP2008/054862
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English (en)
French (fr)
Inventor
Phala Heng
Teruo Muraishi
Michiaki Umeno
Hirokazu Ikenaga
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Mitsui Chemicals, Inc.
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Publication date
Application filed by Mitsui Chemicals, Inc. filed Critical Mitsui Chemicals, Inc.
Priority to EP08722257A priority Critical patent/EP2138554A4/en
Priority to JP2009505214A priority patent/JP5072953B2/ja
Priority to US12/531,535 priority patent/US8138386B2/en
Priority to CN200880008881.4A priority patent/CN101641426B/zh
Publication of WO2008114771A1 publication Critical patent/WO2008114771A1/ja

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/02—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons
    • C07C2/04—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation
    • C07C2/06—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition between unsaturated hydrocarbons by oligomerisation of well-defined unsaturated hydrocarbons without ring formation of alkenes, i.e. acyclic hydrocarbons having only one carbon-to-carbon double bond
    • C07C2/08—Catalytic processes
    • C07C2/12—Catalytic processes with crystalline alumino-silicates or with catalysts comprising molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C4/00—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms
    • C07C4/02—Preparation of hydrocarbons from hydrocarbons containing a larger number of carbon atoms by cracking a single hydrocarbon or a mixture of individually defined hydrocarbons or a normally gaseous hydrocarbon fraction
    • C07C4/06—Catalytic processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/02—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils characterised by the catalyst used
    • C10G11/04—Oxides
    • C10G11/05—Crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/10—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with stationary catalyst bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/633—Pore volume less than 0.5 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/651—50-500 nm
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2521/00—Catalysts comprising the elements, oxides or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium or hafnium
    • C07C2521/14—Silica and magnesia
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups C07C2529/08 - C07C2529/65
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1088—Olefins
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/4018—Spatial velocity, e.g. LHSV, WHSV
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/20—C2-C4 olefins

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

　本発明は、低含有量の無機物バインダーで且つ高細孔容積を有しつつも、炭化水素を原料とする固定床の工業的反応プロセスに使用できる高触媒活性、長触媒寿命及び高破砕強度を有するゼオライト成形触媒を用いる炭化水素の変換方法を提供することを課題とする。 　本発明の方法に用いられるゼオライト成形触媒は、ゼオライト、無機物バインダーの原料、成形助剤、平均直径が０．１～６μｍの有機高分子粒子、及び水を混錬することにより混錬物を製造し、該混錬物を押出し、乾燥、焼成することにより得られた、ゼオライト及び無機物バインダーを含むゼオライト成形触媒であって、ゼオライト成分の含量が全量の60重量%以上であり、該成形触媒の細孔容積が0.4～1.0ml/gであり、且つ体積中央細孔径が80～500nmであり、破砕強度が0.9kg/以上であることを特徴とするゼオライト成形触媒である。
PCT/JP2008/054862 2007-03-20 2008-03-17 ゼオライト成形触媒を用いる炭化水素の変換方法 WO2008114771A1 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP08722257A EP2138554A4 (en) 2007-03-20 2008-03-17 METHOD FOR CONVERTING HYDROCARBONS WITH SHAPED ZEOLITE CATALYST
JP2009505214A JP5072953B2 (ja) 2007-03-20 2008-03-17 ゼオライト成形触媒を用いる炭化水素の変換方法
US12/531,535 US8138386B2 (en) 2007-03-20 2008-03-17 Method for converting hydrocarbons with zeolite shaped catalyst
CN200880008881.4A CN101641426B (zh) 2007-03-20 2008-03-17 使用沸石成形催化剂的烃转换方法

Applications Claiming Priority (2)

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JP2007-072979 2007-03-20
JP2007072979 2007-03-20

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US (1) US8138386B2 (ja)
EP (1) EP2138554A4 (ja)
JP (1) JP5072953B2 (ja)
KR (1) KR101216232B1 (ja)
CN (1) CN101641426B (ja)
SA (1) SA08290146B1 (ja)
TW (1) TWI440706B (ja)
WO (1) WO2008114771A1 (ja)

Cited By (6)

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JP2011020045A (ja) * 2009-07-15 2011-02-03 Mitsui Chemicals Inc 変性ゼオライト触媒および該変性ゼオライト触媒を用いた不飽和炭化水素類の製造方法
WO2013114719A1 (ja) * 2012-01-31 2013-08-08 太平洋セメント株式会社 セメント組成物の製造方法
JP2016535718A (ja) * 2013-10-23 2016-11-17 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 疎水性のゼオライト系材料についての成形物及びその製造方法
JP2018176521A (ja) * 2017-04-11 2018-11-15 日揮触媒化成株式会社 ゼオライト押出成型体の製造方法
JP2020500710A (ja) * 2016-12-13 2020-01-16 エスエムエイチ カンパニー，リミテッド 触媒系および前記触媒系を利用する炭化水素フィードの変換方法
WO2020100830A1 (ja) * 2018-11-12 2020-05-22 ユミコア日本触媒株式会社 ディーゼルエンジンの排気ガス浄化用触媒、その製造方法およびそれを用いた排気ガス浄化方法

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JP2013138974A (ja) * 2011-12-28 2013-07-18 Tokyo Institute Of Technology 不飽和炭化水素製造用触媒の製造方法および不飽和炭化水素の製造方法
US9242233B2 (en) 2012-05-02 2016-01-26 Saudi Basic Industries Corporation Catalyst for light naphtha aromatization
US9180441B2 (en) 2012-09-20 2015-11-10 Saudi Basic Industries Corporation Method of forming zeolite shaped body with silica binder
KR101731165B1 (ko) * 2015-05-07 2017-04-27 롯데케미칼 주식회사 에탄올 탈수 촉매 및 이를 이용한 에틸렌 제조방법
CN108996515A (zh) * 2018-07-28 2018-12-14 瑞声科技（南京）有限公司 一种吸音材料及应用该吸音材料的扬声器箱
WO2020091969A1 (en) * 2018-10-30 2020-05-07 Exxonmobil Chemical Patents Inc. Group 1 metal ion content of microporous molecular sieve catalysts
MX2021013340A (es) * 2019-04-29 2021-11-17 Basf Se Pieza moldeada que comprende un titanosilicato zeolitico tipo mfi y un aglutinante de silice, su proceso de preparacion y uso como catalizador.
KR20220095593A (ko) * 2020-12-30 2022-07-07 한국화학연구원 에틸렌-프로필렌 전환용 제올라이트 촉매, 이의 제조방법 및 이를 이용한 프로필렌의 제조방법

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JPS5959741A (ja) 1982-09-30 1984-04-05 Daicel Chem Ind Ltd 有機顔料
JPS6126509A (ja) 1984-07-06 1986-02-05 モービル　オイル　コーポレーシヨン シリカに富む固体の押出成形法
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JP2011020045A (ja) * 2009-07-15 2011-02-03 Mitsui Chemicals Inc 変性ゼオライト触媒および該変性ゼオライト触媒を用いた不飽和炭化水素類の製造方法
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JPWO2013114719A1 (ja) * 2012-01-31 2015-05-11 太平洋セメント株式会社 セメント組成物の製造方法
JP2016535718A (ja) * 2013-10-23 2016-11-17 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 疎水性のゼオライト系材料についての成形物及びその製造方法
JP2020500710A (ja) * 2016-12-13 2020-01-16 エスエムエイチ カンパニー，リミテッド 触媒系および前記触媒系を利用する炭化水素フィードの変換方法
JP2018176521A (ja) * 2017-04-11 2018-11-15 日揮触媒化成株式会社 ゼオライト押出成型体の製造方法
WO2020100830A1 (ja) * 2018-11-12 2020-05-22 ユミコア日本触媒株式会社 ディーゼルエンジンの排気ガス浄化用触媒、その製造方法およびそれを用いた排気ガス浄化方法
JPWO2020100830A1 (ja) * 2018-11-12 2021-10-14 ユミコア日本触媒株式会社 ディーゼルエンジンの排気ガス浄化用触媒、その製造方法およびそれを用いた排気ガス浄化方法
US11344864B2 (en) 2018-11-12 2022-05-31 Umicore Shokubai Japan Co., Ltd. Diesel engine exhaust gas purification catalyst, production method therefor, and exhaust gas purification method using the same
JP7241091B2 (ja) 2018-11-12 2023-03-16 ユミコア日本触媒株式会社 ディーゼルエンジンの排気ガス浄化用触媒、その製造方法およびそれを用いた排気ガス浄化方法

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US8138386B2 (en) 2012-03-20
SA08290146B1 (ar) 2011-06-22
JP5072953B2 (ja) 2012-11-14
EP2138554A4 (en) 2012-08-08
CN101641426A (zh) 2010-02-03
US20100063341A1 (en) 2010-03-11
CN101641426B (zh) 2014-04-16
KR20090130374A (ko) 2009-12-23
TW200904960A (en) 2009-02-01
KR101216232B1 (ko) 2012-12-28

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