WO2008099850A1 - 官能基を有するかご開裂型シロキサン樹脂とその製造方法 - Google Patents

官能基を有するかご開裂型シロキサン樹脂とその製造方法 Download PDF

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Publication number
WO2008099850A1
WO2008099850A1 PCT/JP2008/052352 JP2008052352W WO2008099850A1 WO 2008099850 A1 WO2008099850 A1 WO 2008099850A1 JP 2008052352 W JP2008052352 W JP 2008052352W WO 2008099850 A1 WO2008099850 A1 WO 2008099850A1
Authority
WO
WIPO (PCT)
Prior art keywords
cage
group
siloxane resin
polar solvent
cleavable siloxane
Prior art date
Application number
PCT/JP2008/052352
Other languages
English (en)
French (fr)
Inventor
Akiko Yamasaki
Takashi Saito
Toshihiro Kawatani
Hideki Andoh
Original Assignee
Nippon Steel Chemical Co., Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Chemical Co., Ltd. filed Critical Nippon Steel Chemical Co., Ltd.
Priority to KR1020097017813A priority Critical patent/KR101494850B1/ko
Priority to CN2008800050696A priority patent/CN101636433B/zh
Priority to JP2008558100A priority patent/JP5346593B2/ja
Publication of WO2008099850A1 publication Critical patent/WO2008099850A1/ja

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C08G77/10—Equilibration processes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Silicon Polymers (AREA)

Abstract

　他の樹脂と相溶性があり、分子量分布及び分子構造の制御されたビニル基、アルキル基、フェニル基、（メタ）アクリロイル基、アリル基又はオキシラン環を有するかご開裂型シロキサン樹脂及びこのかご開裂型シロキサン樹脂を高収率で得る方法を提供する。 　下記一般式(１) 　　　Ｒ1ＳｉＸ3      (１) 〔但し、Ｒ1はビニル基、アルキル基、フェニル基、（メタ）アクリロイル基、アリル基又はオキシラン環を有する基であって、Ｘはアルコキシ基、ハロゲン原子又はヒドロキシル基から選ばれた加水分解性基を示す〕で表されるケイ素化合物の１種又は２種以上を、塩基性触媒存在下、非極性溶媒又は極性溶媒のどちらか一方又は両方を合わせた溶媒中で加水分解反応させると共に一部縮合させ、得られた重縮合物を更に非極性溶媒及び塩基性触媒の存在下で再縮合させ、得られた再縮合物にジシロキサン化合物を平衡化反応させてかご開裂型シロキサン樹脂を得る。
PCT/JP2008/052352 2007-02-16 2008-02-13 官能基を有するかご開裂型シロキサン樹脂とその製造方法 WO2008099850A1 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
KR1020097017813A KR101494850B1 (ko) 2007-02-16 2008-02-13 관능기를 가지는 케이지 개열형 실록산수지와 그 제조방법
CN2008800050696A CN101636433B (zh) 2007-02-16 2008-02-13 具有官能团的笼断裂型硅氧烷树脂及其制造方法
JP2008558100A JP5346593B2 (ja) 2007-02-16 2008-02-13 官能基を有するかご開裂型シロキサン樹脂とその製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007036006 2007-02-16
JP2007-036006 2007-02-16

Publications (1)

Publication Number Publication Date
WO2008099850A1 true WO2008099850A1 (ja) 2008-08-21

Family

ID=39690078

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/052352 WO2008099850A1 (ja) 2007-02-16 2008-02-13 官能基を有するかご開裂型シロキサン樹脂とその製造方法

Country Status (5)

Country Link
JP (1) JP5346593B2 (ja)
KR (1) KR101494850B1 (ja)
CN (1) CN101636433B (ja)
TW (1) TWI431041B (ja)
WO (1) WO2008099850A1 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011195750A (ja) * 2010-03-23 2011-10-06 Nippon Steel Chem Co Ltd 硬化型樹脂組成物及びこれから得られる成形体
WO2012133080A1 (ja) * 2011-03-31 2012-10-04 新日鐵化学株式会社 硬化性シリコーン樹脂組成物及びシリコーン樹脂硬化物
CN113087907A (zh) * 2019-12-23 2021-07-09 万华化学集团股份有限公司 一种硅醇锂及其制备方法和应用

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6021605B2 (ja) * 2012-11-19 2016-11-09 新日鉄住金化学株式会社 かご型シルセスキオキサン化合物、それを用いた硬化性樹脂組成物及び樹脂硬化物
KR102280925B1 (ko) * 2014-07-25 2021-07-26 에스케이이노베이션 주식회사 하드코팅층 형성용 조성물

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003510337A (ja) * 1999-08-04 2003-03-18 ハイブリッド・プラスチックス 多面体オリゴマーシルセスキオキサンの形成方法
JP2003137944A (ja) * 2001-11-05 2003-05-14 Nippon Steel Chem Co Ltd シリコーン樹脂組成物及びシリコーン樹脂成形体
JP2004123936A (ja) * 2002-10-03 2004-04-22 Nippon Steel Chem Co Ltd シリコーン樹脂組成物及びシリコーン樹脂成形体

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4118973B2 (ja) * 1997-03-14 2008-07-16 新日鐵化学株式会社 シリコーン化合物及びその製造方法
JP4793547B2 (ja) 2005-07-25 2011-10-12 信越化学工業株式会社 オルガノシロキサンが結合したイミドの製造方法、及びオルガノシロキサンが結合したアミド酸トリオルガノシリルエステルとその製造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003510337A (ja) * 1999-08-04 2003-03-18 ハイブリッド・プラスチックス 多面体オリゴマーシルセスキオキサンの形成方法
JP2003137944A (ja) * 2001-11-05 2003-05-14 Nippon Steel Chem Co Ltd シリコーン樹脂組成物及びシリコーン樹脂成形体
JP2004123936A (ja) * 2002-10-03 2004-04-22 Nippon Steel Chem Co Ltd シリコーン樹脂組成物及びシリコーン樹脂成形体

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011195750A (ja) * 2010-03-23 2011-10-06 Nippon Steel Chem Co Ltd 硬化型樹脂組成物及びこれから得られる成形体
WO2012133080A1 (ja) * 2011-03-31 2012-10-04 新日鐵化学株式会社 硬化性シリコーン樹脂組成物及びシリコーン樹脂硬化物
JPWO2012133080A1 (ja) * 2011-03-31 2014-07-28 新日鉄住金化学株式会社 硬化性シリコーン樹脂組成物及びシリコーン樹脂硬化物
JP5844796B2 (ja) * 2011-03-31 2016-01-20 新日鉄住金化学株式会社 硬化性シリコーン樹脂組成物及びシリコーン樹脂硬化物
CN113087907A (zh) * 2019-12-23 2021-07-09 万华化学集团股份有限公司 一种硅醇锂及其制备方法和应用
CN113087907B (zh) * 2019-12-23 2023-01-13 万华化学集团股份有限公司 一种硅醇锂及其制备方法和应用

Also Published As

Publication number Publication date
CN101636433A (zh) 2010-01-27
TWI431041B (zh) 2014-03-21
KR20090111341A (ko) 2009-10-26
CN101636433B (zh) 2012-08-15
KR101494850B1 (ko) 2015-02-23
TW200904857A (en) 2009-02-01
JP5346593B2 (ja) 2013-11-20
JPWO2008099850A1 (ja) 2010-05-27

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