WO2006070483A8 - ジフラクトース ジアンヒドリドｉｉｉ結晶の製造方法 - Google Patents

ジフラクトース ジアンヒドリドｉｉｉ結晶の製造方法

Info

Publication number
WO2006070483A8
WO2006070483A8 PCT/JP2004/019832 JP2004019832W WO2006070483A8 WO 2006070483 A8 WO2006070483 A8 WO 2006070483A8 JP 2004019832 W JP2004019832 W JP 2004019832W WO 2006070483 A8 WO2006070483 A8 WO 2006070483A8
Authority
WO
WIPO (PCT)
Prior art keywords
crystallization
producing
iii crystal
dfa iii
iii
Prior art date
Application number
PCT/JP2004/019832
Other languages
English (en)
French (fr)
Other versions
WO2006070483A1 (ja
Inventor
Taizo Nagura
Katsuya Honjyo
Hiroto Kikuchi
Norimitsu Takagi
Tsutomu Aritsuka
Original Assignee
Nippon Beet Sugar Mfg
Taizo Nagura
Katsuya Honjyo
Hiroto Kikuchi
Norimitsu Takagi
Tsutomu Aritsuka
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Beet Sugar Mfg, Taizo Nagura, Katsuya Honjyo, Hiroto Kikuchi, Norimitsu Takagi, Tsutomu Aritsuka filed Critical Nippon Beet Sugar Mfg
Priority to US11/722,936 priority Critical patent/US8039615B2/en
Priority to EP04808182.2A priority patent/EP1834957B1/en
Priority to JP2006550548A priority patent/JP5367948B2/ja
Priority to PCT/JP2004/019832 priority patent/WO2006070483A1/ja
Priority to KR1020077014811A priority patent/KR101102803B1/ko
Priority to CN2004800447289A priority patent/CN101090906B/zh
Publication of WO2006070483A1 publication Critical patent/WO2006070483A1/ja
Publication of WO2006070483A8 publication Critical patent/WO2006070483A8/ja
Priority to US13/210,595 priority patent/US8304534B2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
    • C07H3/10—Anhydrosugars, e.g. epoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
    • C07H3/04—Disaccharides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H9/00—Compounds containing a hetero ring sharing at least two hetero atoms with a saccharide radical
    • C07H9/02—Compounds containing a hetero ring sharing at least two hetero atoms with a saccharide radical the hetero ring containing only oxygen as ring hetero atoms
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12N—MICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N1/00—Microorganisms, e.g. protozoa; Compositions thereof; Processes of propagating, maintaining or preserving microorganisms or compositions thereof; Processes of preparing or isolating a composition containing a microorganism; Culture media therefor
    • C12N1/20—Bacteria; Culture media therefor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Genetics & Genomics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Biomedical Technology (AREA)
  • Microbiology (AREA)
  • Virology (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • General Engineering & Computer Science (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

本発明は、ジフラクトース　ジアンヒドリドIII(difructose　dianhydride　III:DFA　III)、すなわち、フラクトース2分子が1,2';2,3'で結合している難消化性二糖類(di-D-fructofuranose-1,2';2,3'dianhydride)を含有する溶液のpHが5以上、好ましくは5～8、更に好ましくは6～8であることを特徴とするDFA　III結晶の製造方法である。本発明方法によれば、たとえ循環系で結晶化を行っても、結晶化率を低下させることなくDFA　IIIを工業生産でき、その際、更に、(粗)結晶化母液のフラクトースの含量合計が固形分当たり5%以下であり、そしてフラクトース含量が5%以下とすることにより更に効果が高まる。
PCT/JP2004/019832 2004-12-28 2004-12-28 ジフラクトース ジアンヒドリドｉｉｉ結晶の製造方法 WO2006070483A1 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
US11/722,936 US8039615B2 (en) 2004-12-28 2004-12-28 Process for producing difructose dianhydride III crystals
EP04808182.2A EP1834957B1 (en) 2004-12-28 2004-12-28 Process for producing difructose dianhydride iii crystal
JP2006550548A JP5367948B2 (ja) 2004-12-28 2004-12-28 ジフラクトースジアンヒドリドｉｉｉ結晶の製造方法
PCT/JP2004/019832 WO2006070483A1 (ja) 2004-12-28 2004-12-28 ジフラクトース ジアンヒドリドｉｉｉ結晶の製造方法
KR1020077014811A KR101102803B1 (ko) 2004-12-28 2004-12-28 디프룩토스 ２무수물 ⅲ 결정 제조 방법
CN2004800447289A CN101090906B (zh) 2004-12-28 2004-12-28 二果糖二酐ⅲ晶体的制备方法
US13/210,595 US8304534B2 (en) 2004-12-28 2011-08-16 Process for producing difructose dianhydride III crystals

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/JP2004/019832 WO2006070483A1 (ja) 2004-12-28 2004-12-28 ジフラクトース ジアンヒドリドｉｉｉ結晶の製造方法

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US11/722,936 A-371-Of-International US8039615B2 (en) 2004-12-28 2004-12-28 Process for producing difructose dianhydride III crystals
US13/210,595 Continuation US8304534B2 (en) 2004-12-28 2011-08-16 Process for producing difructose dianhydride III crystals

Publications (2)

Publication Number Publication Date
WO2006070483A1 WO2006070483A1 (ja) 2006-07-06
WO2006070483A8 true WO2006070483A8 (ja) 2007-03-29

Family

ID=36614610

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2004/019832 WO2006070483A1 (ja) 2004-12-28 2004-12-28 ジフラクトース ジアンヒドリドｉｉｉ結晶の製造方法

Country Status (6)

Country Link
US (2) US8039615B2 (ja)
EP (1) EP1834957B1 (ja)
JP (1) JP5367948B2 (ja)
KR (1) KR101102803B1 (ja)
CN (1) CN101090906B (ja)
WO (1) WO2006070483A1 (ja)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7893985B1 (en) 2004-03-15 2011-02-22 Grandeye Ltd. Wide angle electronic camera with improved peripheral vision
ES2304223B2 (es) * 2007-03-08 2009-05-01 Universidad De Sevilla Nuevos caramelos con elevado contenido en oligosacaridos prebioticos, procedimiento de preparacion y utilizacion.
JP5920735B2 (ja) * 2011-11-09 2016-05-18 敬一 藤居 コーヒー飲料、そのコーヒー液の抽出方法およびコーヒー液抽出用の抽出溶媒
CA2883897C (en) * 2012-09-11 2021-05-04 Dow Agrosciences Llc Omega-9 canola oil blended with dha
CN105506034B (zh) 2016-01-26 2019-01-11 江南大学 一种合成双果糖酐iii的方法
KR102072695B1 (ko) * 2016-12-08 2020-03-02 주식회사 삼양사 재순환을 이용한 사이코스의 제조방법 및 장치

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5626400B2 (ja) * 1973-03-17 1981-06-18
JPS5626400A (en) 1979-08-09 1981-03-13 Mitsuo Watanabe Device for discharging movable charger
JPS6417688A (en) 1987-07-13 1989-01-20 Mitsubishi Electric Corp Full-automatic washing dryer
JPH066064B2 (ja) 1988-05-13 1994-01-26 農林水産省食品総合研究所長 ジフルクトース・ジアンヒドリドの製造方法
AU4104889A (en) 1988-09-07 1990-03-15 Bioclones (Pty) Ltd Purification of erythropoietin
JPH02115193A (ja) * 1988-10-25 1990-04-27 Mitsubishi Kasei Corp ジフルクトース・ジアンヒドリドの精製方法
JPH03259090A (ja) 1990-03-09 1991-11-19 Mitsubishi Kasei Corp ジフルクトース・ジアンヒドリド３の製造法
JPH04271792A (ja) 1991-02-28 1992-09-28 Mitsubishi Kasei Corp ジフルクトース・ジアンヒドリドｉｉｉの製造方法
JPH05168419A (ja) 1991-06-05 1993-07-02 Mitsubishi Kasei Corp 動物の脂肪低減剤及びこれを用いる動物の飼育方法
JP3514955B2 (ja) 1997-07-29 2004-04-05 日本甜菜製糖株式会社 カルシウム吸収亢進組成物
JPH11103814A (ja) * 1997-09-30 1999-04-20 Showa Sangyo Co Ltd 苦味剤、味質改善剤、苦味付与または味質改善のための使用、および苦味を付与したか味質を改善した飲食品または薬品
JP4271792B2 (ja) 1999-09-29 2009-06-03 トキコテクノ株式会社 給油装置
JP3259090B2 (ja) 1999-12-16 2002-02-18 寛 小長谷 仰臥用書見台
JP2002017391A (ja) * 2000-07-06 2002-01-22 Nippon Beet Sugar Mfg Co Ltd ジフルクトース・ジアンヒドリドｉｖの大量製造法
MXPA03004402A (es) * 2000-11-17 2003-09-05 Johnson & Johnson Composicion mejorada de sucralosa y procedimiento para su preparacion.
JP3776334B2 (ja) * 2001-07-11 2006-05-17 株式会社富士薬品 イヌリン含有製剤
JP4572167B2 (ja) * 2003-03-05 2010-10-27 日本甜菜製糖株式会社 ジフルクトース・ジアンヒドリドｉｉｉの精製方法
JP4391114B2 (ja) * 2003-04-08 2009-12-24 日本甜菜製糖株式会社 酵素の大量生産法

Also Published As

Publication number Publication date
KR20070089212A (ko) 2007-08-30
WO2006070483A1 (ja) 2006-07-06
CN101090906A (zh) 2007-12-19
JP5367948B2 (ja) 2013-12-11
EP1834957A4 (en) 2008-04-16
EP1834957A1 (en) 2007-09-19
CN101090906B (zh) 2012-07-04
US20070287835A1 (en) 2007-12-13
US8304534B2 (en) 2012-11-06
EP1834957B1 (en) 2014-04-09
JPWO2006070483A1 (ja) 2008-06-12
US8039615B2 (en) 2011-10-18
US20110300581A1 (en) 2011-12-08
KR101102803B1 (ko) 2012-01-05

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