WO2003045890A1 - Method for purifying (meth)acrylic acid - Google Patents

Method for purifying (meth)acrylic acid Download PDF

Info

Publication number
WO2003045890A1
WO2003045890A1 PCT/JP2002/011308 JP0211308W WO03045890A1 WO 2003045890 A1 WO2003045890 A1 WO 2003045890A1 JP 0211308 W JP0211308 W JP 0211308W WO 03045890 A1 WO03045890 A1 WO 03045890A1
Authority
WO
WIPO (PCT)
Prior art keywords
meth
acrylic acid
distillation
fed
distillation column
Prior art date
Application number
PCT/JP2002/011308
Other languages
English (en)
French (fr)
Inventor
Shuhei Yada
Yasushi Ogawa
Yoshiro Suzuki
Kenji Takasaki
Original Assignee
Mitsubishi Chemical Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP2001332008A external-priority patent/JP2003137834A/ja
Priority claimed from JP2001360437A external-priority patent/JP3918528B2/ja
Priority claimed from JP2001368858A external-priority patent/JP3981550B2/ja
Priority claimed from JP2001373671A external-priority patent/JP2003170001A/ja
Priority claimed from JP2002003590A external-priority patent/JP3997782B2/ja
Priority claimed from JP2002131675A external-priority patent/JP2003321419A/ja
Priority to AU2002344613A priority Critical patent/AU2002344613A1/en
Application filed by Mitsubishi Chemical Corporation filed Critical Mitsubishi Chemical Corporation
Publication of WO2003045890A1 publication Critical patent/WO2003045890A1/ja
Priority to US10/834,075 priority patent/US7414150B2/en
Priority to US11/103,617 priority patent/US7265241B2/en
Priority to US11/103,622 priority patent/US20050176998A1/en
Priority to US11/226,360 priority patent/US20060009657A1/en
Priority to US12/014,186 priority patent/US20080245652A1/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146—Multiple effect distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
    • B01D1/222—In rotating vessels; vessels with movable parts
    • B01D1/223—In rotating vessels; vessels with movable parts containing a rotor
    • B01D1/225—In rotating vessels; vessels with movable parts containing a rotor with blades or scrapers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
PCT/JP2002/011308 2001-10-30 2002-10-30 Method for purifying (meth)acrylic acid WO2003045890A1 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
AU2002344613A AU2002344613A1 (en) 2001-10-30 2002-10-30 Method for purifying (meth)acrylic acid
US10/834,075 US7414150B2 (en) 2001-10-30 2004-04-29 Method for purifying (meth)acrylic acid
US11/103,617 US7265241B2 (en) 2001-10-30 2005-04-12 Method for purifying (meth)acrylic acid
US11/103,622 US20050176998A1 (en) 2001-10-30 2005-04-12 Method for purifying (meth)acrylic acid
US11/226,360 US20060009657A1 (en) 2001-10-30 2005-09-15 Method for purifying (meth)acrylic acid
US12/014,186 US20080245652A1 (en) 2001-10-30 2008-01-15 Method for purifying (meth)acrylic acid

Applications Claiming Priority (12)

Application Number Priority Date Filing Date Title
JP2001332008A JP2003137834A (ja) 2001-10-30 2001-10-30 （メタ）アクリル酸の精製方法
JP2001-332008 2001-10-30
JP2001-360437 2001-11-27
JP2001360437A JP3918528B2 (ja) 2001-11-27 2001-11-27 （メタ）アクリル酸の精製方法
JP2001368858A JP3981550B2 (ja) 2001-12-03 2001-12-03 アクリル酸エステルの製造方法
JP2001-368858 2001-12-03
JP2001-373671 2001-12-07
JP2001373671A JP2003170001A (ja) 2001-12-07 2001-12-07 薄膜蒸発器
JP2002-003590 2002-01-10
JP2002003590A JP3997782B2 (ja) 2002-01-10 2002-01-10 （メタ）アクリル酸の製造方法
JP2002-131675 2002-05-07
JP2002131675A JP2003321419A (ja) 2002-05-07 2002-05-07 高純度（メタ）アクリル酸の製造方法

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US10/834,075 Continuation US7414150B2 (en) 2001-10-30 2004-04-29 Method for purifying (meth)acrylic acid

Publications (1)

Publication Number Publication Date
WO2003045890A1 true WO2003045890A1 (en) 2003-06-05

Family

ID=27555009

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2002/011308 WO2003045890A1 (en) 2001-10-30 2002-10-30 Method for purifying (meth)acrylic acid

Country Status (4)

Country Link
US (5) US7414150B2 (ja)
CN (6) CN1263725C (ja)
AU (1) AU2002344613A1 (ja)
WO (1) WO2003045890A1 (ja)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005044772A1 (ja) * 2003-11-11 2005-05-19 Mitsubishi Chemical Corporation 精製（メタ）アクリル酸の製造方法

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CN1263725C (zh) 2001-10-30 2006-07-12 三菱化学株式会社 （甲基）丙烯酸的精制方法
WO2005051883A1 (ja) * 2003-11-28 2005-06-09 Mitsubishi Chemical Corporation （メタ）アクリル酸の精製方法
JP2005289919A (ja) * 2004-04-01 2005-10-20 Mitsubishi Chemicals Corp （メタ）アクリル酸または（メタ）アクロレインの製造方法
JP2005298376A (ja) * 2004-04-08 2005-10-27 Mitsubishi Chemicals Corp アクロレイン及びアクリル酸の製造方法
US8283295B1 (en) * 2007-02-21 2012-10-09 Tajwar Shadikhan Oil solids precipitation
CN101835736B (zh) * 2007-10-23 2013-06-12 Lg化学株式会社 收集(甲基)丙烯酸的方法和收集(甲基)丙烯酸的装置
KR101049561B1 (ko) * 2009-09-08 2011-07-14 주식회사 엘지화학 (메트)아크릴레이트의 제조방법
DE102010028781A1 (de) 2010-05-10 2011-11-10 Evonik Stockhausen Gmbh Abtrennung von Acrylsäure mittels einer einen Seitenabzug aufweisenden Destillationskolonne
US9505901B2 (en) * 2010-12-08 2016-11-29 Pravansu S. Mohanty Depolymerization processes, apparatuses and catalysts for use in connection therewith
CA2781246A1 (en) * 2011-07-14 2013-01-14 Rohm And Haas Company Method for removal of organic compounds from waste water streams in a process for production of (meth)acrylic acid
CN102580332A (zh) * 2012-02-12 2012-07-18 中石油东北炼化工程有限公司吉林设计院 丙烯酸及酯装置薄膜蒸发器夹套加热介质控制系统
CN104168972B (zh) 2012-03-16 2016-01-06 三菱丽阳株式会社 立式离心薄膜蒸发器和单体的精制方法
RU2676308C1 (ru) * 2015-08-07 2018-12-27 Дайкин Индастриз, Лтд. Способ очистки производного акриловой кислоты
DE202015106097U1 (de) * 2015-11-11 2016-02-01 Holger Blum Fördereinrichtung für eine Vakuumdestillationsanlage
CN109632572B (zh) * 2018-12-25 2021-03-30 山西霍家长化合成橡胶有限公司 Pdva油漆聚合终点判定方法
CN113617043B (zh) * 2021-09-08 2022-07-19 浙江金棕榈科技股份有限公司 一种半短程式蒸发器
CN116041162B (zh) * 2022-10-28 2024-04-12 江苏扬农化工集团有限公司 从丙烯醛水合制3-羟基丙醛的产物体系中分离回收丙烯醛的方法

Citations (4)

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GB2285046A (en) * 1993-12-24 1995-06-28 Sumitomo Chemical Co Purifying acrylic acid
JPH10218832A (ja) * 1997-02-13 1998-08-18 Mitsubishi Chem Corp アクリル酸の精製法
EP1046416A2 (en) * 1999-04-23 2000-10-25 Nippon Shokubai Co., Ltd. Method for preventing polymerization in thin-film type evaporating device
JP2001058970A (ja) * 1999-08-20 2001-03-06 Nippon Shokubai Co Ltd アクリル酸の精製方法

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US4317926A (en) * 1978-01-19 1982-03-02 Nippon Shokubai Kagaku Kogyo Co., Ltd. Process for preparing and recovering acrylic acid
DE3641996A1 (de) * 1986-12-09 1988-06-16 Basf Ag Verfahren zum abtrennen von aldehyden aus (alpha),(beta)-olefinisch ungesaettigten carbonsaeuren
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FR2736912B1 (fr) 1995-07-18 1997-08-22 Atochem Elf Sa Procede de purification de l'acide acrylique obtenu par oxydation catalytique du propylene
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JP4361995B2 (ja) * 1999-12-22 2009-11-11 株式会社日本触媒 アクリル酸の精製方法
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JP4299432B2 (ja) * 2000-03-10 2009-07-22 株式会社日本触媒 （メタ）アクリル酸の精製方法
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BR0109929B1 (pt) 2000-04-11 2012-08-07 processo para a purificaÇço de uma massa fundida de Ácido acrÍlico bruto.
JP3805178B2 (ja) 2000-07-31 2006-08-02 株式会社日本触媒 メタクリル酸の回収方法
CN1263725C (zh) 2001-10-30 2006-07-12 三菱化学株式会社 （甲基）丙烯酸的精制方法
WO2003043968A1 (en) * 2001-11-20 2003-05-30 Mitsubishi Chemical Corporation Process for producing (meth)acrylic acid compounds
WO2003045892A1 (en) * 2001-11-28 2003-06-05 Mitsubishi Chemical Corporation Process for producing (meth)acrylic acid compound
JP2003160532A (ja) * 2001-11-28 2003-06-03 Mitsubishi Chemicals Corp （メタ）アクリル酸の製造方法
JP4016650B2 (ja) * 2001-12-14 2007-12-05 三菱化学株式会社 （メタ）アクリル酸の製造方法
CN1262528C (zh) * 2002-01-29 2006-07-05 三菱化学株式会社 (甲基)丙烯酸的制造方法
JP3971974B2 (ja) * 2002-09-03 2007-09-05 三菱化学株式会社 （メタ）アクリル酸類の製造方法
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Patent Citations (4)

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Publication number Priority date Publication date Assignee Title
GB2285046A (en) * 1993-12-24 1995-06-28 Sumitomo Chemical Co Purifying acrylic acid
JPH10218832A (ja) * 1997-02-13 1998-08-18 Mitsubishi Chem Corp アクリル酸の精製法
EP1046416A2 (en) * 1999-04-23 2000-10-25 Nippon Shokubai Co., Ltd. Method for preventing polymerization in thin-film type evaporating device
JP2001058970A (ja) * 1999-08-20 2001-03-06 Nippon Shokubai Co Ltd アクリル酸の精製方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005044772A1 (ja) * 2003-11-11 2005-05-19 Mitsubishi Chemical Corporation 精製（メタ）アクリル酸の製造方法
CN100450992C (zh) * 2003-11-11 2009-01-14 三菱化学株式会社 生产纯化(甲基)丙烯酸的方法

Also Published As

Publication number Publication date
US20080245652A1 (en) 2008-10-09
AU2002344613A1 (en) 2003-06-10
US7265241B2 (en) 2007-09-04
US20050176998A1 (en) 2005-08-11
US20060009657A1 (en) 2006-01-12
CN1267397C (zh) 2006-08-02
US7414150B2 (en) 2008-08-19
US20040204608A1 (en) 2004-10-14
CN1572781A (zh) 2005-02-02
CN1572777A (zh) 2005-02-02
CN1582268A (zh) 2005-02-16
US20050176997A1 (en) 2005-08-11
CN100389848C (zh) 2008-05-28
CN1572778A (zh) 2005-02-02
CN1263725C (zh) 2006-07-12
CN1572779A (zh) 2005-02-02
CN1288126C (zh) 2006-12-06
CN1562949A (zh) 2005-01-12

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