UA103301C2 - Способ получения бисфенола a - Google Patents

Способ получения бисфенола a

Info

Publication number
UA103301C2
UA103301C2 UAA200908556A UAA200908556A UA103301C2 UA 103301 C2 UA103301 C2 UA 103301C2 UA A200908556 A UAA200908556 A UA A200908556A UA A200908556 A UAA200908556 A UA A200908556A UA 103301 C2 UA103301 C2 UA 103301C2
Authority
UA
Ukraine
Prior art keywords
acetone
crystallization
subjected
phenol
solvent
Prior art date
Application number
UAA200908556A
Other languages
English (en)
Ukrainian (uk)
Inventor
Богуслав ТКАЧ
Тереза РДЕСИНСКА-ЦВИК
Камиль КУЛЕША
Анджей Крюгер
Станислав Матия
Мария Майхжак
Войцех БАЛЬЦЕРОВЯК
Божена Банас
Алина ИВАНЕЙКО
Ежи Ясинкевич
Original Assignee
Институт Ценжкей Синтези Органичней Блаховня
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Институт Ценжкей Синтези Органичней Блаховня filed Critical Институт Ценжкей Синтези Органичней Блаховня
Publication of UA103301C2 publication Critical patent/UA103301C2/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/11—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
    • C07C37/20—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Изобретение касается получения бисфенола А из фенола и ацетона путем каталитического конденсирования в присутствии промотированных сульфонилированных ионообменных смол, используя фракционную кристаллизацию для выделения п,п'-БФА изомера. Реакцию конденсации ацетона и фенола проводят в многостадийной реакционной системе с межстадийным контролем температуры реакции и концентрации ацетона, также как и с контролем концентрации воды перед последней стадией реакционной системы. Часть послекристаллизационных жидкостей с кристаллизаций из растворителя рециклизируют до последнего реактора. Воду и ацетон выпаривают из по�
UAA200908556A 2007-02-14 2008-02-14 Способ получения бисфенола a UA103301C2 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PL381757A PL210812B1 (pl) 2007-02-14 2007-02-14 Sposób otrzymywania bisfenolu A
PCT/PL2008/000016 WO2008100165A1 (en) 2007-02-14 2008-02-14 Process for producing bisphenol a

Publications (1)

Publication Number Publication Date
UA103301C2 true UA103301C2 (ru) 2013-10-10

Family

ID=39233566

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA200908556A UA103301C2 (ru) 2007-02-14 2008-02-14 Способ получения бисфенола a

Country Status (6)

Country Link
CN (1) CN101636371B (ru)
DE (1) DE112008000300T5 (ru)
PL (1) PL210812B1 (ru)
RU (1) RU2451663C2 (ru)
UA (1) UA103301C2 (ru)
WO (1) WO2008100165A1 (ru)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20120283485A1 (en) * 2011-05-02 2012-11-08 Umesh Krishna Hasyagar Robust promoter catalyst system
WO2012150560A1 (en) * 2011-05-02 2012-11-08 Sabic Innovative Plastics Ip B.V. High purity bisphenol a and polycarbonate materials prepared therefrom
CN103502192A (zh) * 2011-05-02 2014-01-08 沙特基础创新塑料Ip私人有限责任公司 高纯度双酚a和由其制备的聚碳酸酯材料
US8735634B2 (en) * 2011-05-02 2014-05-27 Sabic Innovative Plastics Ip B.V. Promoter catalyst system with solvent purification
US9290618B2 (en) 2011-08-05 2016-03-22 Sabic Global Technologies B.V. Polycarbonate compositions having enhanced optical properties, methods of making and articles comprising the polycarbonate compositions
CN103172658B (zh) * 2011-12-26 2016-01-20 宜昌人福药业有限责任公司 一种适合药用的前体药物晶型、制备方法及药用组合物
WO2013116697A1 (en) 2012-02-03 2013-08-08 Sabic Innovative Plastics Ip B.V. Light emitting diode device and method for production thereof containing conversion material chemistry
EP2819981B1 (en) 2012-02-29 2016-12-21 SABIC Global Technologies B.V. Process for producing low sulfur bisphenol a, processes for producing polycarbonate, articles made from polycarbonate
US9287471B2 (en) 2012-02-29 2016-03-15 Sabic Global Technologies B.V. Polycarbonate compositions containing conversion material chemistry and having enhanced optical properties, methods of making and articles comprising the same
US9346949B2 (en) 2013-02-12 2016-05-24 Sabic Global Technologies B.V. High reflectance polycarbonate
PL219656B1 (pl) * 2012-08-23 2015-06-30 Inst Ciężkiej Syntezy Organicznej Blachownia Sposób transformacji produktów ubocznych w procesie syntezy bisfenolu A
WO2014066784A1 (en) 2012-10-25 2014-05-01 Sabic Innovative Plastics Ip B.V. Light emitting diode devices, method of manufacture, uses thereof
WO2014186548A1 (en) 2013-05-16 2014-11-20 Sabic Innovative Plastics Ip B.V. Branched polycarbonate compositions having conversion material chemistry and articles thereof
CN105492519B (zh) 2013-05-29 2018-03-09 沙特基础全球技术有限公司 具有颜色稳定的热塑性光传输制品的照明设备
PL221981B1 (pl) 2013-07-22 2016-06-30 Hreczuch Wiesław MEXEO Sposób otrzymywania bisfenolu A
RU2560183C1 (ru) * 2014-08-08 2015-08-20 Общество с ограниченной ответственностью "Научно-производственное объединение ЕВРОХИМ" Способ получения катализатора для разложения алкилароматических гидропероксидов
CN105130758B (zh) * 2015-08-12 2017-12-08 南通星辰合成材料有限公司 采用悬浮结晶与降膜结晶的组合工艺制备双酚a的方法
EP3558916B1 (en) * 2016-12-20 2021-06-09 SABIC Global Technologies B.V. Method for manufacturing of bisphenol a
CN112409573B (zh) * 2019-08-23 2023-06-20 南通星辰合成材料有限公司 一种副产多元酚环氧树脂及其制造方法与应用
CN116535648B (zh) * 2023-07-04 2024-05-03 山东浩然特塑股份有限公司 一种聚砜树脂的制备方法
CN117717980A (zh) * 2023-12-14 2024-03-19 天津大学 双酚a生产工艺及装置

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3049569A (en) * 1958-10-20 1962-08-14 Union Carbide Corp Production of 2, 2-bis(4-hydroxyphenyl) propane
GB1578952A (en) * 1977-07-11 1980-11-12 Shell Int Research Preparation of bisphenols
GB1578225A (en) * 1977-07-11 1980-11-05 Shell Int Research Preparation of bisphenols
SU798085A1 (ru) * 1978-12-27 1981-01-23 Предприятие П/Я Р-6830 Способ выделени дифенилпро-пАНА"
US4590303A (en) * 1985-06-03 1986-05-20 General Electric Company Method for making bisphenol
US4954661A (en) * 1988-03-11 1990-09-04 Mitsui Toatsu Chemicals, Inc. Process for preparing high-purity bisphenol A
PL164289B1 (pl) * 1990-11-24 1994-07-29 Inst Ciezkiej Syntezy Orga Sposób otrzymywani blsfenolu A PL PL
JPH08333290A (ja) 1995-06-12 1996-12-17 Mitsubishi Chem Corp ビスフェノールａの製造方法
US5783733A (en) * 1996-06-13 1998-07-21 General Electric Company Process for manufacture of bisphenol
USH1943H1 (en) * 1998-12-15 2001-02-06 General Electric Co. Process for the manufacture of bisphenol-A
US6133486A (en) 1998-12-30 2000-10-17 General Electric Company Phenol recovery from BPA process waste streams
TW530045B (en) 1999-04-13 2003-05-01 Idemitsu Petrochemical Co Method of producing bisphenol A
US6858759B2 (en) * 2002-12-20 2005-02-22 General Electric Company Process for manufacture of bisphenols
US7989666B2 (en) * 2003-09-28 2011-08-02 China Petroleum & Chemical Corporation Method for preparing bisphenol A
US8039679B2 (en) * 2005-10-07 2011-10-18 Badger Licensing Llc Bisphenol-A plant yield enhancement
KR100767448B1 (ko) 2006-06-30 2007-10-17 메디칸(주) 원심분리기 및 원심분리방법

Also Published As

Publication number Publication date
PL210812B1 (pl) 2012-03-30
RU2009134199A (ru) 2011-03-20
PL381757A1 (pl) 2008-08-18
WO2008100165A1 (en) 2008-08-21
RU2451663C2 (ru) 2012-05-27
DE112008000300T5 (de) 2010-01-14
CN101636371A (zh) 2010-01-27
CN101636371B (zh) 2014-01-29

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