UA103301C2 - Process for producing bisphenol a - Google Patents

Process for producing bisphenol a

Info

Publication number
UA103301C2
UA103301C2 UAA200908556A UAA200908556A UA103301C2 UA 103301 C2 UA103301 C2 UA 103301C2 UA A200908556 A UAA200908556 A UA A200908556A UA A200908556 A UAA200908556 A UA A200908556A UA 103301 C2 UA103301 C2 UA 103301C2
Authority
UA
Ukraine
Prior art keywords
acetone
crystallization
subjected
phenol
solvent
Prior art date
Application number
UAA200908556A
Other languages
Russian (ru)
Ukrainian (uk)
Inventor
Богуслав ТКАЧ
Тереза РДЕСИНСКА-ЦВИК
Камиль КУЛЕША
Анджей Крюгер
Станислав Матия
Мария Майхжак
Войцех БАЛЬЦЕРОВЯК
Божена Банас
Алина ИВАНЕЙКО
Ежи Ясинкевич
Original Assignee
Институт Ценжкей Синтези Органичней Блаховня
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Институт Ценжкей Синтези Органичней Блаховня filed Critical Институт Ценжкей Синтези Органичней Блаховня
Publication of UA103301C2 publication Critical patent/UA103301C2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/11—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
    • C07C37/20—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention relates to producing bisplienol A from phenol and acetone by way of catalytic condensation in the presence of promoted, sulfonated ion- exchange resins, with using fractional crystallization to isolate the p,p'-BPA isomer. The condensation reaction of acetone and phenol is carried out in a multi stage reaction system with the interstage control of reaction temperature and acetone concentration as well as with the control of water concentration before the last stage of the reaction system. A part of post-crystallization liquors from solvent crystallizations is recycled to the last reactor. Water and acetone are evaporated from the post-reaction mixture which, subsequently, is mixed with the effluent solution from fractional crystallization dissolved in the isomerizate obtained in the process of isomerization of a part of the stream of concentrated liquors after solvent crystallization, the resulting stream is subjected to solvent crystallization, the isolated bisphenol A/phenol adduct is subjected to thermal decomposition, and the resulting raw bisphenol A is subjected to fractional crystallization.
UAA200908556A 2007-02-14 2008-02-14 Process for producing bisphenol a UA103301C2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PL381757A PL210812B1 (en) 2007-02-14 2007-02-14 The manner of obtaining of bisphenol A
PCT/PL2008/000016 WO2008100165A1 (en) 2007-02-14 2008-02-14 Process for producing bisphenol a

Publications (1)

Publication Number Publication Date
UA103301C2 true UA103301C2 (en) 2013-10-10

Family

ID=39233566

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA200908556A UA103301C2 (en) 2007-02-14 2008-02-14 Process for producing bisphenol a

Country Status (6)

Country Link
CN (1) CN101636371B (en)
DE (1) DE112008000300T5 (en)
PL (1) PL210812B1 (en)
RU (1) RU2451663C2 (en)
UA (1) UA103301C2 (en)
WO (1) WO2008100165A1 (en)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20140038973A (en) * 2011-05-02 2014-03-31 사빅 이노베이티브 플라스틱스 아이피 비.브이. High purity bisphenol a and polycarbonate materials prepared therefrom
US8735634B2 (en) 2011-05-02 2014-05-27 Sabic Innovative Plastics Ip B.V. Promoter catalyst system with solvent purification
US20120283485A1 (en) * 2011-05-02 2012-11-08 Umesh Krishna Hasyagar Robust promoter catalyst system
KR20140043362A (en) * 2011-05-02 2014-04-09 사빅 이노베이티브 플라스틱스 아이피 비.브이. High purity bisphenol-a and polycarbonate materials prepared thereform
US9290618B2 (en) 2011-08-05 2016-03-22 Sabic Global Technologies B.V. Polycarbonate compositions having enhanced optical properties, methods of making and articles comprising the polycarbonate compositions
CN103172658B (en) * 2011-12-26 2016-01-20 宜昌人福药业有限责任公司 A kind of applicable medicinal prodrug crystal formation, preparation method and medicinal compositions
CN104205376B (en) 2012-02-03 2018-04-27 沙特基础全球技术有限公司 LED device and for producing its method for including transition material chemistry
WO2013130606A2 (en) 2012-02-29 2013-09-06 Sabic Innovative Plastics Ip B.V. Polycarbonate made from low sulfur bisphenol a and containing converions material chemistry, and articles made therefrom
WO2013130610A1 (en) 2012-02-29 2013-09-06 Sabic Innovative Plastics Ip B.V. Polycarbonate compositions containing conversions material chemistry and having enhanced optical properties, methods of making and articles comprising the same
US9346949B2 (en) 2013-02-12 2016-05-24 Sabic Global Technologies B.V. High reflectance polycarbonate
PL219656B1 (en) * 2012-08-23 2015-06-30 Inst Ciężkiej Syntezy Organicznej Blachownia Method for transmitting by-products in the synthesis of bisphenol A
WO2014066784A1 (en) 2012-10-25 2014-05-01 Sabic Innovative Plastics Ip B.V. Light emitting diode devices, method of manufacture, uses thereof
WO2014186548A1 (en) 2013-05-16 2014-11-20 Sabic Innovative Plastics Ip B.V. Branched polycarbonate compositions having conversion material chemistry and articles thereof
US9772086B2 (en) 2013-05-29 2017-09-26 Sabic Innovative Plastics Ip B.V. Illuminating devices with color stable thermoplastic light transmitting articles
PL221981B1 (en) 2013-07-22 2016-06-30 Hreczuch Wiesław MEXEO Method for obtaining bisphenol A
RU2560183C1 (en) * 2014-08-08 2015-08-20 Общество с ограниченной ответственностью "Научно-производственное объединение ЕВРОХИМ" Method of obtaining catalyst for decomposition of alkylaromatic hydroperoxides
CN107793296B (en) * 2015-08-12 2021-05-18 南通星辰合成材料有限公司 Method for preparing bisphenol A by adopting combined process of suspension crystallization and falling film crystallization
EP3558916B1 (en) * 2016-12-20 2021-06-09 SABIC Global Technologies B.V. Method for manufacturing of bisphenol a
CN112409573B (en) * 2019-08-23 2023-06-20 南通星辰合成材料有限公司 Byproduct polyphenol epoxy resin and preparation method and application thereof
CN116535648B (en) * 2023-07-04 2024-05-03 山东浩然特塑股份有限公司 Preparation method of polysulfone resin
CN117717980B (en) * 2023-12-14 2024-08-23 天津大学 Bisphenol A production process and device

Family Cites Families (16)

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Publication number Priority date Publication date Assignee Title
US3049569A (en) * 1958-10-20 1962-08-14 Union Carbide Corp Production of 2, 2-bis(4-hydroxyphenyl) propane
GB1578952A (en) * 1977-07-11 1980-11-12 Shell Int Research Preparation of bisphenols
GB1578225A (en) * 1977-07-11 1980-11-05 Shell Int Research Preparation of bisphenols
SU798085A1 (en) * 1978-12-27 1981-01-23 Предприятие П/Я Р-6830 Method of isolating diphenylpropane
US4590303A (en) * 1985-06-03 1986-05-20 General Electric Company Method for making bisphenol
US4954661A (en) * 1988-03-11 1990-09-04 Mitsui Toatsu Chemicals, Inc. Process for preparing high-purity bisphenol A
PL164289B1 (en) * 1990-11-24 1994-07-29 Inst Ciezkiej Syntezy Orga Method of obtaining high purity bisphenol a
JPH08333290A (en) * 1995-06-12 1996-12-17 Mitsubishi Chem Corp Production of bisphenol a
US5783733A (en) * 1996-06-13 1998-07-21 General Electric Company Process for manufacture of bisphenol
USH1943H1 (en) * 1998-12-15 2001-02-06 General Electric Co. Process for the manufacture of bisphenol-A
US6133486A (en) 1998-12-30 2000-10-17 General Electric Company Phenol recovery from BPA process waste streams
TW530045B (en) 1999-04-13 2003-05-01 Idemitsu Petrochemical Co Method of producing bisphenol A
US6858759B2 (en) 2002-12-20 2005-02-22 General Electric Company Process for manufacture of bisphenols
PL207733B1 (en) * 2003-09-28 2011-01-31 China Petroleum & Chem Corp Method for preparing bisphenol a
KR20080077104A (en) * 2005-10-07 2008-08-21 바져 라이센싱 엘엘씨 Bisphenol-a plant yield enhancement
KR100767448B1 (en) 2006-06-30 2007-10-17 메디칸(주) Centrifuge and centrifuging method

Also Published As

Publication number Publication date
PL381757A1 (en) 2008-08-18
DE112008000300T5 (en) 2010-01-14
RU2451663C2 (en) 2012-05-27
WO2008100165A1 (en) 2008-08-21
PL210812B1 (en) 2012-03-30
CN101636371B (en) 2014-01-29
CN101636371A (en) 2010-01-27
RU2009134199A (en) 2011-03-20

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