TW202231349A - 空心粒子的製造方法及空心粒子 - Google Patents
空心粒子的製造方法及空心粒子 Download PDFInfo
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- TW202231349A TW202231349A TW110140187A TW110140187A TW202231349A TW 202231349 A TW202231349 A TW 202231349A TW 110140187 A TW110140187 A TW 110140187A TW 110140187 A TW110140187 A TW 110140187A TW 202231349 A TW202231349 A TW 202231349A
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- hollow particles
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- hydrophobic solvent
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- C08F12/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
- C08F12/34—Monomers containing two or more unsaturated aliphatic radicals
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- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
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- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
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- C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
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- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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| WO2023106307A1 (ja) * | 2021-12-10 | 2023-06-15 | 日本ゼオン株式会社 | 中空粒子、樹脂組成物、及び樹脂成形体 |
| WO2023228964A1 (ja) * | 2022-05-26 | 2023-11-30 | 日本ゼオン株式会社 | 中空粒子、樹脂組成物、樹脂成形体、封止用樹脂組成物、硬化物、及び半導体装置 |
| US20250282116A1 (en) * | 2022-06-21 | 2025-09-11 | Resonac Corporation | Sheet comprising thermal insulation layer and adhesive layer |
| US20260078240A1 (en) | 2022-08-30 | 2026-03-19 | Zeon Corporation | Hollow particles, resin composition and molded body |
| EP4613783A1 (en) * | 2022-10-31 | 2025-09-10 | Zeon Corporation | Hollow particles, manufacturing method of hollow particles, resin composition and resin structure |
| WO2024203876A1 (ja) | 2023-03-24 | 2024-10-03 | 積水化成品工業株式会社 | 中空樹脂粒子、その製造方法、およびその用途 |
Family Cites Families (25)
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|---|---|---|---|---|
| JP2000313818A (ja) | 1999-03-03 | 2000-11-14 | Jsr Corp | 架橋樹脂粒子、有機絶縁材用組成物、有機絶縁材、封止材、および回路基板 |
| JP2000315845A (ja) * | 1999-04-28 | 2000-11-14 | Jsr Corp | 回路基板 |
| US6146749A (en) * | 1999-05-03 | 2000-11-14 | Jsr Corporation | Low dielectric composition, insulating material, sealing material, and circuit board |
| JP2003181274A (ja) * | 2001-12-18 | 2003-07-02 | Sekisui Chem Co Ltd | 中空ポリマー粒子の製造方法 |
| JP4171489B2 (ja) * | 2003-01-28 | 2008-10-22 | 松下電工株式会社 | 中空粒子を含有する樹脂組成物、同組成物を含むプリプレグおよび積層板 |
| JP3600845B2 (ja) | 2004-03-08 | 2004-12-15 | 財団法人新産業創造研究機構 | 中空高分子微粒子及びその製造法 |
| JP4626194B2 (ja) * | 2004-06-22 | 2011-02-02 | パナソニック電工株式会社 | 電気絶縁性樹脂組成物、プリプレグ、積層板及び多層プリント配線板 |
| JP4884053B2 (ja) * | 2006-03-31 | 2012-02-22 | 株式会社スマート粒子創造工房 | 内部に空隙を有する微粒子の製造方法 |
| JP2008115280A (ja) * | 2006-11-06 | 2008-05-22 | Hitachi Ltd | 低誘電損失樹脂組成物、その硬化物およびそれを用いた電子部品 |
| EP2098550A4 (en) * | 2006-12-28 | 2010-02-03 | Zeon Corp | POLYMERIZABLE COMPOSITION |
| JP2008231241A (ja) * | 2007-03-20 | 2008-10-02 | Sanyo Chem Ind Ltd | 中空樹脂粒子 |
| JP5727962B2 (ja) * | 2012-04-16 | 2015-06-03 | 三光株式会社 | 非膨張型中空ポリマー微粒子の製造方法 |
| KR101597346B1 (ko) * | 2014-05-30 | 2016-02-25 | (주) 유니플라텍 | 저비중 도전 입자를 포함하는 코팅제 조성물을 이용한 전자파 차폐 필름 |
| JP6641724B2 (ja) * | 2015-05-11 | 2020-02-05 | コニカミノルタ株式会社 | 中空樹脂粒子およびその製造方法 |
| JP7107634B2 (ja) * | 2015-12-28 | 2022-07-27 | ジャパンコーティングレジン株式会社 | 中空ポリマー粒子、ポリマー粒子懸濁液の製造方法、および中空ポリマー粒子の製造方法 |
| US11760857B2 (en) * | 2017-08-01 | 2023-09-19 | Zeon Corporation | Method for producing latex and method for producing hollow resin particles |
| EP4234650B1 (en) * | 2018-03-30 | 2024-11-27 | Zeon Corporation | Hollow resin particles and sheet |
| JP7294345B2 (ja) * | 2018-09-28 | 2023-06-20 | 日本ゼオン株式会社 | 樹脂組成物及びその成形体 |
| EP3922650A4 (en) * | 2019-02-06 | 2022-10-26 | Zeon Corporation | PROCESS FOR MANUFACTURING HOLLOW RESIN PARTICLES |
| JP7342376B2 (ja) * | 2019-02-25 | 2023-09-12 | 日本ゼオン株式会社 | 中空樹脂粒子の製造方法 |
| EP3992213A4 (en) * | 2019-06-27 | 2023-07-26 | Zeon Corporation | PROCESS FOR PRODUCTION OF HOLLOW RESIN PARTICLES |
| US12485399B2 (en) * | 2019-12-06 | 2025-12-02 | Zeon Corporation | Hollow particles, resin composition and molded body |
| WO2021112117A1 (ja) * | 2019-12-06 | 2021-06-10 | 日本ゼオン株式会社 | 中空粒子の製造方法 |
| CN116194495B (zh) * | 2020-09-30 | 2024-06-28 | 日本瑞翁株式会社 | 中空颗粒 |
| WO2022071276A1 (ja) * | 2020-09-30 | 2022-04-07 | 日本ゼオン株式会社 | 中空粒子の製造方法 |
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2021
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- 2021-10-26 US US18/031,815 patent/US20230383021A1/en active Pending
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- 2021-10-26 JP JP2022559152A patent/JPWO2022092076A1/ja active Pending
- 2021-10-26 CN CN202180070712.9A patent/CN116390958A/zh active Pending
- 2021-10-26 WO PCT/JP2021/039457 patent/WO2022092076A1/ja not_active Ceased
- 2021-10-29 TW TW110140187A patent/TW202231349A/zh unknown
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| EP4238998A4 (en) | 2025-03-26 |
| JPWO2022092076A1 (https=) | 2022-05-05 |
| KR20230098160A (ko) | 2023-07-03 |
| WO2022092076A1 (ja) | 2022-05-05 |
| CN116390958A (zh) | 2023-07-04 |
| US20230383021A1 (en) | 2023-11-30 |
| EP4238998A1 (en) | 2023-09-06 |
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