TW201231402A - Process for preparing precursors for transition metal mixed oxides - Google Patents
Process for preparing precursors for transition metal mixed oxides Download PDFInfo
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- TW201231402A TW201231402A TW100143392A TW100143392A TW201231402A TW 201231402 A TW201231402 A TW 201231402A TW 100143392 A TW100143392 A TW 100143392A TW 100143392 A TW100143392 A TW 100143392A TW 201231402 A TW201231402 A TW 201231402A
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- Taiwan
- Prior art keywords
- transition metal
- group
- doc
- present
- carbonate
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- 229910052723 transition metal Inorganic materials 0.000 title claims abstract description 68
- 150000003624 transition metals Chemical class 0.000 title claims abstract description 55
- 239000002243 precursor Substances 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title abstract description 5
- 229910000299 transition metal carbonate Inorganic materials 0.000 claims abstract description 14
- -1 X-type i-ion Inorganic materials 0.000 claims description 41
- 238000000034 method Methods 0.000 claims description 33
- 239000000243 solution Substances 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 16
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 14
- 239000007864 aqueous solution Substances 0.000 claims description 14
- 239000007772 electrode material Substances 0.000 claims description 13
- 229910052759 nickel Inorganic materials 0.000 claims description 13
- 229910052751 metal Inorganic materials 0.000 claims description 11
- 239000002184 metal Substances 0.000 claims description 11
- 229910052744 lithium Inorganic materials 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 9
- 229910052748 manganese Inorganic materials 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- 239000011734 sodium Substances 0.000 claims description 8
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 7
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- 229910002651 NO3 Inorganic materials 0.000 claims description 5
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- 229910052747 lanthanoid Inorganic materials 0.000 claims description 4
- 150000002602 lanthanoids Chemical class 0.000 claims description 4
- 230000000737 periodic effect Effects 0.000 claims description 4
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- 229910001416 lithium ion Inorganic materials 0.000 claims description 3
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- 229910052725 zinc Inorganic materials 0.000 claims description 3
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- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
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- 238000010891 electric arc Methods 0.000 description 1
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- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 1
- UIWXSTHGICQLQT-UHFFFAOYSA-N ethenyl propanoate Chemical compound CCC(=O)OC=C UIWXSTHGICQLQT-UHFFFAOYSA-N 0.000 description 1
- 125000004494 ethyl ester group Chemical group 0.000 description 1
- JBTWLSYIZRCDFO-UHFFFAOYSA-N ethyl methyl carbonate Chemical compound CCOC(=O)OC JBTWLSYIZRCDFO-UHFFFAOYSA-N 0.000 description 1
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- XTHFKEDIFFGKHM-UHFFFAOYSA-N ethylene glycol dimethyl ether Natural products COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 1
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- 125000003983 fluorenyl group Chemical group C1(=CC=CC=2C3=CC=CC=C3CC12)* 0.000 description 1
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- 238000007429 general method Methods 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 description 1
- 229920001903 high density polyethylene Polymers 0.000 description 1
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- 235000003642 hunger Nutrition 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
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- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 description 1
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- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
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- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- 229910001540 lithium hexafluoroarsenate(V) Inorganic materials 0.000 description 1
- IIPYXGDZVMZOAP-UHFFFAOYSA-N lithium nitrate Inorganic materials [Li+].[O-][N+]([O-])=O IIPYXGDZVMZOAP-UHFFFAOYSA-N 0.000 description 1
- 229920001684 low density polyethylene Polymers 0.000 description 1
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- 239000011777 magnesium Substances 0.000 description 1
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- 235000007079 manganese sulphate Nutrition 0.000 description 1
- UOGMEBQRZBEZQT-UHFFFAOYSA-L manganese(2+);diacetate Chemical compound [Mn+2].CC([O-])=O.CC([O-])=O UOGMEBQRZBEZQT-UHFFFAOYSA-L 0.000 description 1
- 229910000357 manganese(II) sulfate Inorganic materials 0.000 description 1
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- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
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- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 1
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- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 1
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- 229910052698 phosphorus Chemical group 0.000 description 1
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- 239000011148 porous material Substances 0.000 description 1
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 description 1
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- XJMOSONTPMZWPB-UHFFFAOYSA-M propidium iodide Chemical compound [I-].[I-].C12=CC(N)=CC=C2C2=CC=C(N)C=C2[N+](CCC[N+](C)(CC)CC)=C1C1=CC=CC=C1 XJMOSONTPMZWPB-UHFFFAOYSA-M 0.000 description 1
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- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
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- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
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- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
- C01B13/14—Methods for preparing oxides or hydroxides in general
- C01B13/18—Methods for preparing oxides or hydroxides in general by thermal decomposition of compounds, e.g. of salts or hydroxides
- C01B13/185—Preparing mixtures of oxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/60—Preparation of carbonates or bicarbonates in general
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Complex oxides containing nickel and at least one other metal element
- C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Complex oxides containing nickel and at least one other metal element
- C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
- C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
- C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
- C01P2004/13—Nanotubes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Nanotechnology (AREA)
- Manufacturing & Machinery (AREA)
- Physics & Mathematics (AREA)
- Composite Materials (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10192582 | 2010-11-25 |
Publications (1)
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|---|---|
| TW201231402A true TW201231402A (en) | 2012-08-01 |
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| EP (1) | EP2458665A3 (enExample) |
| JP (1) | JP6203053B2 (enExample) |
| KR (1) | KR101890105B1 (enExample) |
| CN (1) | CN103229337B (enExample) |
| TW (1) | TW201231402A (enExample) |
| WO (1) | WO2012070011A1 (enExample) |
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| JP7078346B2 (ja) * | 2016-02-15 | 2022-05-31 | 信越化学工業株式会社 | 負極活物質及びリチウムイオン二次電池の製造方法 |
| CN108630923A (zh) * | 2018-04-28 | 2018-10-09 | 南开大学 | 梯度钠离子掺杂的镍钴铝酸锂正极材料、制备方法和锂电池 |
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| JPH05325969A (ja) * | 1992-05-25 | 1993-12-10 | Hitachi Maxell Ltd | リチウム二次電池の製造方法 |
| JPH05343066A (ja) * | 1992-06-09 | 1993-12-24 | Mitsui Mining & Smelting Co Ltd | リチウム二次電池用正極活物質 |
| JPH07196323A (ja) * | 1993-12-28 | 1995-08-01 | Sumitomo Metal Mining Co Ltd | ナトリウム含有量の少ない酸化コバルトの製造法 |
| JP3562187B2 (ja) * | 1996-12-27 | 2004-09-08 | ソニー株式会社 | 非水電解液二次電池 |
| JPH10321224A (ja) * | 1997-05-16 | 1998-12-04 | Nikki Kagaku Kk | リチウム電池正極材及びその製造方法 |
| JPH11167919A (ja) * | 1997-12-05 | 1999-06-22 | Nikki Chemcal Co Ltd | 高安定性リチウムイオン二次電池用正極材、製造方法およびその用途 |
| JP2002060225A (ja) * | 2000-08-18 | 2002-02-26 | Ishihara Sangyo Kaisha Ltd | コバルト酸リチウム凝集体、コバルト酸化物凝集体及びそれらの製造方法並びに該コバルト酸リチウム凝集体を用いてなるリチウム電池 |
| JP3827545B2 (ja) * | 2001-09-13 | 2006-09-27 | 松下電器産業株式会社 | 正極活物質、その製造方法および非水電解質二次電池 |
| US7435402B2 (en) * | 2002-11-01 | 2008-10-14 | U Chicago Argonne Llc | Method and apparatus for preparation of spherical metal carbonates and lithium metal oxides for lithium rechargeable batteries |
| TWI279019B (en) * | 2003-01-08 | 2007-04-11 | Nikko Materials Co Ltd | Material for lithium secondary battery positive electrode and manufacturing method thereof |
| US7041239B2 (en) * | 2003-04-03 | 2006-05-09 | Valence Technology, Inc. | Electrodes comprising mixed active particles |
| JP2005097087A (ja) * | 2003-07-18 | 2005-04-14 | Tosoh Corp | 新規なリチウム・ニッケル・マンガン複合酸化物およびその製造方法 |
| KR100575065B1 (ko) * | 2004-03-29 | 2006-04-28 | 학교법인 한양학원 | 고율특성과 열적 안정성이 향상된 리튬이차전지용 양극활물질 제조방법 및 그 방법으로 제조된 리튬이차전지양극 활물질 |
| JP5021892B2 (ja) * | 2004-06-17 | 2012-09-12 | Ｊｘ日鉱日石金属株式会社 | リチウムイオン二次電池正極材料用前駆体とその製造方法並びにそれを用いた正極材料の製造方法 |
| JP4839633B2 (ja) * | 2005-02-28 | 2011-12-21 | パナソニック株式会社 | 非水電解質二次電池および非水電解質二次電池用正極活物質の製造方法 |
| US7648693B2 (en) * | 2005-04-13 | 2010-01-19 | Lg Chem, Ltd. | Ni-based lithium transition metal oxide |
| US8062792B2 (en) * | 2005-04-26 | 2011-11-22 | Uchicago Argonne Llc | Processes for making dense, spherical active materials for lithium-ion cells |
| JP4768562B2 (ja) * | 2005-09-27 | 2011-09-07 | 石原産業株式会社 | リチウム・遷移金属複合酸化物及びその製造方法並びにそれを用いてなるリチウム電池 |
| JP4968944B2 (ja) | 2008-02-01 | 2012-07-04 | 日本化学工業株式会社 | 複合炭酸塩およびその製造方法 |
| JP4968945B2 (ja) | 2008-02-01 | 2012-07-04 | 日本化学工業株式会社 | 複合炭酸塩およびその製造方法 |
| JPWO2009098835A1 (ja) * | 2008-02-04 | 2011-05-26 | パナソニック株式会社 | リチウム含有遷移金属酸化物の製造方法 |
| JP5225708B2 (ja) * | 2008-02-27 | 2013-07-03 | 日本化学工業株式会社 | リチウム二次電池正極活物質用リチウムニッケルマンガンコバルト複合酸化物、その製造方法及びリチウム二次電池 |
| EP2196434A1 (en) * | 2008-12-12 | 2010-06-16 | Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. | Phosphate based compound, use of the compound in an electrochemical storage device and methods for its preparation |
| JP5648828B2 (ja) * | 2010-04-26 | 2015-01-07 | 日産自動車株式会社 | リチウムイオン二次電池 |
-
2011
- 2011-11-24 EP EP20110190504 patent/EP2458665A3/de not_active Withdrawn
- 2011-11-24 CN CN201180056978.4A patent/CN103229337B/zh not_active Expired - Fee Related
- 2011-11-24 WO PCT/IB2011/055280 patent/WO2012070011A1/en not_active Ceased
- 2011-11-24 KR KR1020137016440A patent/KR101890105B1/ko not_active Expired - Fee Related
- 2011-11-24 JP JP2013540472A patent/JP6203053B2/ja not_active Expired - Fee Related
- 2011-11-25 TW TW100143392A patent/TW201231402A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| KR101890105B1 (ko) | 2018-08-21 |
| EP2458665A2 (de) | 2012-05-30 |
| CN103229337B (zh) | 2016-01-20 |
| KR20130121132A (ko) | 2013-11-05 |
| CN103229337A (zh) | 2013-07-31 |
| EP2458665A3 (de) | 2015-05-06 |
| JP2014503942A (ja) | 2014-02-13 |
| WO2012070011A1 (en) | 2012-05-31 |
| JP6203053B2 (ja) | 2017-09-27 |
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