TW201121938A - Manufacture of difluoroethylene carbonate, trifluoroethylene carbonate and tetrafluoroethylene carbonate - Google Patents
Manufacture of difluoroethylene carbonate, trifluoroethylene carbonate and tetrafluoroethylene carbonate Download PDFInfo
- Publication number
- TW201121938A TW201121938A TW099132421A TW99132421A TW201121938A TW 201121938 A TW201121938 A TW 201121938A TW 099132421 A TW099132421 A TW 099132421A TW 99132421 A TW99132421 A TW 99132421A TW 201121938 A TW201121938 A TW 201121938A
- Authority
- TW
- Taiwan
- Prior art keywords
- carbonate
- ethyl
- ethyl ester
- difluoroextension
- starting material
- Prior art date
Links
- VUZHZBFVQSUQDP-UHFFFAOYSA-N 4,4,5,5-tetrafluoro-1,3-dioxolan-2-one Chemical compound FC1(F)OC(=O)OC1(F)F VUZHZBFVQSUQDP-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 title claims description 24
- DSMUTQTWFHVVGQ-UHFFFAOYSA-N 4,5-difluoro-1,3-dioxolan-2-one Chemical compound FC1OC(=O)OC1F DSMUTQTWFHVVGQ-UHFFFAOYSA-N 0.000 title abstract 2
- CRJXZTRTJWAKMU-UHFFFAOYSA-N 4,4,5-trifluoro-1,3-dioxolan-2-one Chemical compound FC1OC(=O)OC1(F)F CRJXZTRTJWAKMU-UHFFFAOYSA-N 0.000 title description 2
- 238000006243 chemical reaction Methods 0.000 claims abstract description 46
- 239000011737 fluorine Substances 0.000 claims abstract description 39
- 229910052731 fluorine Inorganic materials 0.000 claims abstract description 39
- 238000003682 fluorination reaction Methods 0.000 claims abstract description 18
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims abstract 7
- 239000007858 starting material Substances 0.000 claims description 36
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 33
- 125000004494 ethyl ester group Chemical group 0.000 claims description 30
- 239000000203 mixture Substances 0.000 claims description 28
- CQDGTJPVBWZJAZ-UHFFFAOYSA-N monoethyl carbonate Chemical compound CCOC(O)=O CQDGTJPVBWZJAZ-UHFFFAOYSA-N 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 27
- PBWZKZYHONABLN-UHFFFAOYSA-M difluoroacetate Chemical compound [O-]C(=O)C(F)F PBWZKZYHONABLN-UHFFFAOYSA-M 0.000 claims description 23
- DTQVDTLACAAQTR-UHFFFAOYSA-M Trifluoroacetate Chemical compound [O-]C(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-M 0.000 claims description 22
- 239000011521 glass Substances 0.000 claims description 18
- HJGJHDZQLWWMRT-UHFFFAOYSA-N 2,2,2-trifluoroethyl hydrogen carbonate Chemical compound OC(=O)OCC(F)(F)F HJGJHDZQLWWMRT-UHFFFAOYSA-N 0.000 claims description 15
- -1 tetrafluoroethylene ethyl carbonate Chemical compound 0.000 claims description 15
- 150000001875 compounds Chemical class 0.000 claims description 11
- GZKHDVAKKLTJPO-UHFFFAOYSA-N ethyl 2,2-difluoroacetate Chemical compound CCOC(=O)C(F)F GZKHDVAKKLTJPO-UHFFFAOYSA-N 0.000 claims description 10
- 239000002841 Lewis acid Substances 0.000 claims description 9
- 150000007517 lewis acids Chemical class 0.000 claims description 9
- 239000007791 liquid phase Substances 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 239000002904 solvent Substances 0.000 claims description 8
- 229910052782 aluminium Inorganic materials 0.000 claims description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 239000000919 ceramic Substances 0.000 claims description 4
- 238000005530 etching Methods 0.000 claims description 4
- MUPRUEGWJTZSMK-UHFFFAOYSA-N ethyl fluoro carbonate Chemical compound CCOC(=O)OF MUPRUEGWJTZSMK-UHFFFAOYSA-N 0.000 claims description 4
- 239000002243 precursor Substances 0.000 claims description 4
- 239000004065 semiconductor Substances 0.000 claims description 4
- 239000010935 stainless steel Substances 0.000 claims description 4
- 229910001220 stainless steel Inorganic materials 0.000 claims description 4
- 229910000856 hastalloy Inorganic materials 0.000 claims description 3
- 229910001026 inconel Inorganic materials 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 229910000838 Al alloy Inorganic materials 0.000 claims description 2
- 239000003507 refrigerant Substances 0.000 claims description 2
- 238000003786 synthesis reaction Methods 0.000 claims description 2
- 239000002861 polymer material Substances 0.000 claims 3
- JXUSJTKKDOYWEZ-UHFFFAOYSA-N carbonic acid 2,2-difluoroacetic acid Chemical compound C(O)(O)=O.FC(C(=O)O)F JXUSJTKKDOYWEZ-UHFFFAOYSA-N 0.000 claims 2
- 229910000640 Fe alloy Inorganic materials 0.000 claims 1
- QEWYKACRFQMRMB-UHFFFAOYSA-N fluoroacetic acid Chemical compound OC(=O)CF QEWYKACRFQMRMB-UHFFFAOYSA-N 0.000 claims 1
- 229920000620 organic polymer Polymers 0.000 claims 1
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 abstract description 3
- MIZLGWKEZAPEFJ-UHFFFAOYSA-N 1,1,2-trifluoroethene Chemical group FC=C(F)F MIZLGWKEZAPEFJ-UHFFFAOYSA-N 0.000 abstract 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 32
- 239000007789 gas Substances 0.000 description 27
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 23
- 239000011541 reaction mixture Substances 0.000 description 18
- 229910052757 nitrogen Inorganic materials 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 239000003085 diluting agent Substances 0.000 description 7
- 239000001307 helium Substances 0.000 description 7
- 229910052734 helium Inorganic materials 0.000 description 7
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 7
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 6
- 238000004821 distillation Methods 0.000 description 6
- 239000011261 inert gas Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 238000003860 storage Methods 0.000 description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 5
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 5
- 238000000354 decomposition reaction Methods 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000000654 additive Substances 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 4
- SDKYSKTZHSYGLF-UHFFFAOYSA-N carbonic acid;2,2,2-trifluoroacetic acid Chemical compound OC(O)=O.OC(=O)C(F)(F)F SDKYSKTZHSYGLF-UHFFFAOYSA-N 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 4
- 229910004014 SiF4 Inorganic materials 0.000 description 3
- STSCVKRWJPWALQ-UHFFFAOYSA-N TRIFLUOROACETIC ACID ETHYL ESTER Chemical compound CCOC(=O)C(F)(F)F STSCVKRWJPWALQ-UHFFFAOYSA-N 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- ABTOQLMXBSRXSM-UHFFFAOYSA-N silicon tetrafluoride Chemical compound F[Si](F)(F)F ABTOQLMXBSRXSM-UHFFFAOYSA-N 0.000 description 3
- DYLIWHYUXAJDOJ-OWOJBTEDSA-N (e)-4-(6-aminopurin-9-yl)but-2-en-1-ol Chemical compound NC1=NC=NC2=C1N=CN2C\C=C\CO DYLIWHYUXAJDOJ-OWOJBTEDSA-N 0.000 description 2
- IUHZCKVTAFBZNR-UHFFFAOYSA-N 2,2-difluoroethyl hydrogen carbonate Chemical compound OC(=O)OCC(F)F IUHZCKVTAFBZNR-UHFFFAOYSA-N 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 239000004813 Perfluoroalkoxy alkane Substances 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000004817 gas chromatography Methods 0.000 description 2
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 229910001416 lithium ion Inorganic materials 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
- 229910052756 noble gas Inorganic materials 0.000 description 2
- 229920011301 perfluoro alkoxyl alkane Polymers 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 125000004205 trifluoroethyl group Chemical group [H]C([H])(*)C(F)(F)F 0.000 description 2
- AEVUQUSVRLQLQG-UHFFFAOYSA-N 2-fluoroethyl hydrogen carbonate Chemical compound OC(=O)OCCF AEVUQUSVRLQLQG-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 229910001290 LiPF6 Inorganic materials 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 239000002033 PVDF binder Substances 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
- 229910018557 Si O Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- SYHPANJAVIEQQL-UHFFFAOYSA-N dicarboxy carbonate Chemical compound OC(=O)OC(=O)OC(O)=O SYHPANJAVIEQQL-UHFFFAOYSA-N 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- UHCBBWUQDAVSMS-UHFFFAOYSA-N fluoroethane Chemical compound CCF UHCBBWUQDAVSMS-UHFFFAOYSA-N 0.000 description 1
- WBJINCZRORDGAQ-UHFFFAOYSA-N formic acid ethyl ester Natural products CCOC=O WBJINCZRORDGAQ-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 description 1
- 150000002835 noble gases Chemical class 0.000 description 1
- 150000005677 organic carbonates Chemical class 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229920001281 polyalkylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 1
- 125000006337 tetrafluoro ethyl group Chemical group 0.000 description 1
- TXEYQDLBPFQVAA-UHFFFAOYSA-N tetrafluoromethane Chemical compound FC(F)(F)F TXEYQDLBPFQVAA-UHFFFAOYSA-N 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/109—Esters; Ether-esters of carbonic acid, e.g. R-O-C(=O)-O-R
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/34—Oxygen atoms
- C07D317/36—Alkylene carbonates; Substituted alkylene carbonates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/42—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Secondary Cells (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09171491 | 2009-09-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TW201121938A true TW201121938A (en) | 2011-07-01 |
Family
ID=41666439
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW099132421A TW201121938A (en) | 2009-09-28 | 2010-09-24 | Manufacture of difluoroethylene carbonate, trifluoroethylene carbonate and tetrafluoroethylene carbonate |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US20120253058A1 (https=) |
| EP (2) | EP2483261A2 (https=) |
| JP (2) | JP2013505919A (https=) |
| KR (2) | KR20120092603A (https=) |
| CN (2) | CN102639521A (https=) |
| TW (1) | TW201121938A (https=) |
| WO (2) | WO2011036293A2 (https=) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014515168A (ja) * | 2011-04-26 | 2014-06-26 | ソルヴェイ（ソシエテ アノニム） | リチウム空気バッテリセル |
| EP2602241A1 (en) | 2011-12-07 | 2013-06-12 | Solvay Sa | Process for the manufacture of 1, 1'-difluorosubstituted dialkyl carbonates, isomers thereof and electrolyte compositions containing them |
| KR20150064748A (ko) | 2012-10-09 | 2015-06-11 | 솔베이(소시에떼아노님) | 플루오르화 유기 카보네이트의 정제 방법 |
| CN104718198A (zh) * | 2012-10-09 | 2015-06-17 | 索尔维公司 | 纯化的氟取代的有机碳酸酯的制备 |
| EP2824096A1 (en) * | 2013-07-09 | 2015-01-14 | Solvay SA | Fluorinated carbonates comprising double bond-containing groups, methods for their manufacture and uses thereof |
| CN108886167B (zh) * | 2016-04-12 | 2022-03-08 | 大金工业株式会社 | 电解液、电化学装置、锂离子二次电池及组件 |
| CN108250176A (zh) * | 2016-12-19 | 2018-07-06 | 上海惠和化德生物科技有限公司 | 一种氟代碳酸乙烯酯的快速连续流合成工艺 |
| US11127979B2 (en) | 2018-03-16 | 2021-09-21 | Uchicago Argonne, Llc | Polyfluorinated carbonate electrolyte for high-voltage lithium batteries |
| CN111635313B (zh) * | 2020-06-05 | 2022-10-11 | 扬州大学 | 一种硒催化乙酸甲酯氧化制电解液溶剂碳酸二甲酯的方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3455954A (en) * | 1966-03-31 | 1969-07-15 | Minnesota Mining & Mfg | Cyclic fluorocarbonates |
| CA2087390A1 (en) * | 1992-02-12 | 1993-08-13 | Jack E. Richman | Preparation of fluorinated functional compounds |
| JP3541476B2 (ja) | 1995-02-16 | 2004-07-14 | 旭硝子株式会社 | 電気二重層キャパシタ |
| JP4531153B2 (ja) * | 1999-04-28 | 2010-08-25 | 関東電化工業株式会社 | ４−フルオロ−１，３−ジオキソラン−２−オンの製造方法 |
| JP4431212B2 (ja) * | 1999-06-02 | 2010-03-10 | 関東電化工業株式会社 | 含フッ素環状炭酸エステルの製造方法 |
| JP2004161638A (ja) * | 2002-11-11 | 2004-06-10 | Mitsubishi Chemicals Corp | フッ素含環状化合物の製造方法 |
| DE10308149A1 (de) * | 2003-02-26 | 2004-09-09 | Solvay Fluor Und Derivate Gmbh | Verfahren zur Herstellung von 4-Fluor-1, 3-dioxolan-2-on |
| KR100655225B1 (ko) * | 2005-01-24 | 2006-12-08 | 울산화학주식회사 | 4-플루오로에틸렌카보네이트의 제조방법 및 장치 |
| JP5061635B2 (ja) * | 2007-02-15 | 2012-10-31 | ダイキン工業株式会社 | ４−フルオロ−１，３−ジオキソラン−２−オンの製造法 |
| CN100558721C (zh) * | 2007-06-01 | 2009-11-11 | 张家港市华盛化学有限公司 | 氟代环状碳酸酯的制备方法 |
| JP5135926B2 (ja) * | 2007-07-13 | 2013-02-06 | ダイキン工業株式会社 | ４−フルオロ−１，３−ジオキソラン−２−オンの製造方法 |
| JP5358974B2 (ja) * | 2008-02-28 | 2013-12-04 | ダイキン工業株式会社 | フッ素化１，３−ジオキソラン−２−オンの製造方法 |
| JP5600876B2 (ja) * | 2008-02-28 | 2014-10-08 | ダイキン工業株式会社 | ４−フルオロ−１，３−ジオキソラン−２−オンの製造方法 |
| US20110009660A1 (en) * | 2008-03-27 | 2011-01-13 | Solvay Flour Gmbh | Process for the removal of HF from HF containing organic carbonates |
| WO2009118368A1 (en) * | 2008-03-27 | 2009-10-01 | Solvay Fluor Gmbh | Preparation of fluorinated organic carbonates depleted in hf using a specific absorbent |
| EP2196464A1 (en) * | 2008-12-15 | 2010-06-16 | Solvay Fluor GmbH | Container containing fluorinated organic carbonates |
-
2010
- 2010-09-24 TW TW099132421A patent/TW201121938A/zh unknown
- 2010-09-27 WO PCT/EP2010/064269 patent/WO2011036293A2/en not_active Ceased
- 2010-09-27 CN CN2010800428476A patent/CN102639521A/zh active Pending
- 2010-09-27 KR KR1020127010849A patent/KR20120092603A/ko not_active Withdrawn
- 2010-09-27 EP EP10759630A patent/EP2483261A2/en not_active Withdrawn
- 2010-09-27 EP EP10759629A patent/EP2483260A2/en not_active Withdrawn
- 2010-09-27 JP JP2012530285A patent/JP2013505919A/ja active Pending
- 2010-09-27 US US13/497,316 patent/US20120253058A1/en not_active Abandoned
- 2010-09-27 JP JP2012530288A patent/JP2013505921A/ja active Pending
- 2010-09-27 US US13/497,333 patent/US20120177987A1/en not_active Abandoned
- 2010-09-27 CN CN201080042843.8A patent/CN102548978B/zh not_active Expired - Fee Related
- 2010-09-27 WO PCT/EP2010/064221 patent/WO2011036283A2/en not_active Ceased
- 2010-09-27 KR KR1020127010853A patent/KR20120099420A/ko not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| CN102548978A (zh) | 2012-07-04 |
| US20120177987A1 (en) | 2012-07-12 |
| US20120253058A1 (en) | 2012-10-04 |
| WO2011036293A2 (en) | 2011-03-31 |
| CN102548978B (zh) | 2014-01-29 |
| WO2011036293A3 (en) | 2011-05-19 |
| WO2011036283A2 (en) | 2011-03-31 |
| EP2483260A2 (en) | 2012-08-08 |
| JP2013505921A (ja) | 2013-02-21 |
| CN102639521A (zh) | 2012-08-15 |
| JP2013505919A (ja) | 2013-02-21 |
| KR20120092603A (ko) | 2012-08-21 |
| EP2483261A2 (en) | 2012-08-08 |
| KR20120099420A (ko) | 2012-09-10 |
| WO2011036283A3 (en) | 2011-05-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| TW201121938A (en) | Manufacture of difluoroethylene carbonate, trifluoroethylene carbonate and tetrafluoroethylene carbonate | |
| JP6256462B2 (ja) | 高純度２−フルオロブタン | |
| US10011553B2 (en) | Method for producing dry etching gas | |
| TW201500331A (zh) | 高純度１－氟丁烷及電漿蝕刻方法 | |
| US9984896B2 (en) | High-purity fluorinated hydrocarbon, use as a plasma etching gas, and plasma etching method | |
| JP4765630B2 (ja) | フッ化カルボニルの製造方法および製造装置 | |
| CN102596867A (zh) | 含氟化合物的纯化方法 | |
| JP2013112612A (ja) | 半導体ガスの製造方法 | |
| CN102770405B (zh) | 二氟乙酸酯的制造方法 | |
| JP5652179B2 (ja) | 半導体ガスの製造方法 | |
| JP2002255868A (ja) | パーフルオロカーボン類の製造方法およびその用途 | |
| JPWO2007063938A1 (ja) | 不飽和フッ素化炭素化合物の精製方法、フルオロカーボン膜の成膜方法、及び半導体装置の製造方法 | |
| TWI703114B (zh) | 氟化甲烷之製造方法 | |
| CN110650937A (zh) | 八氟环戊烯的制造方法 | |
| JP2003267712A (ja) | 二フッ化カルボニルの製造方法 | |
| JP2022184047A (ja) | フッ化炭化水素の製造方法 | |
| RU2135451C1 (ru) | Способ получения перфторалканов | |
| WO2018235567A1 (ja) | オクタフルオロシクロペンテンの製造方法 | |
| WO2008107578A1 (fr) | Procede de fabrication du 1,1-difluoroethane | |
| JP2017078069A (ja) | フッ化メチルの製造方法 | |
| CN106542981A (zh) | 全氟九碳酮的制备方法 | |
| JP2024074671A (ja) | 含フッ素化合物の製造方法 | |
| WO1998056742A1 (en) | Azeotropic mixture of perfluoroalkyl iodide and hydrogen fluoride, and method for isolating and purifying perfluoroalkyl iodides | |
| TWM682139U (zh) | 六氟丁二烯製備系統 | |
| JPH0338543A (ja) | ブロモジフルオロアセチルフルオリドの製造方法 |