NO20081132L - Fremgangsmate for fremstilling av dioksolan - Google Patents

Fremgangsmate for fremstilling av dioksolan

Info

Publication number
NO20081132L
NO20081132L NO20081132A NO20081132A NO20081132L NO 20081132 L NO20081132 L NO 20081132L NO 20081132 A NO20081132 A NO 20081132A NO 20081132 A NO20081132 A NO 20081132A NO 20081132 L NO20081132 L NO 20081132L
Authority
NO
Norway
Prior art keywords
distillation column
reactive distillation
dioxolane
region
ethylene glycol
Prior art date
Application number
NO20081132A
Other languages
English (en)
Inventor
Eckhard Strofer
Achim Stammer
Neven Lang
Markus Siegert
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of NO20081132L publication Critical patent/NO20081132L/no

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
    • C07D317/12—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Battery Electrode And Active Subsutance (AREA)

Abstract

En fremgangsmåte for fremstilling av dioksolan ved omsetning av etylenglykol (1) med formaldehyd i vandig oppløsning (2) i nærvær av katalysatorer, hvori reaksjonen gjennomføres i en reaktiv destillasjonskolonne (RDK), hvor utgangsmaterialene etylenglykol (1) og vandig formaldehydløsning (2) føres inn i den reaktive destillasjonskolonne (RDK) i midtregionen av kolonnen og en dioksolanomfattende strøm (3) tas ut fra den øvre region av den reaktive destillasjonskolonne (RDK) og en bunnstrøm (4) omfattende komponenter med kokepunkter høyere enn kokepunktet av dioksolan tas ut, er beskrevet.
NO20081132A 2005-09-07 2008-03-04 Fremgangsmate for fremstilling av dioksolan NO20081132L (no)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102005042505A DE102005042505A1 (de) 2005-09-07 2005-09-07 Verfahren zur Herstellung von Dioxolan
PCT/EP2006/066086 WO2007028809A1 (de) 2005-09-07 2006-09-06 Verfahren zur herstellung von dioxolan

Publications (1)

Publication Number Publication Date
NO20081132L true NO20081132L (no) 2008-05-08

Family

ID=37735624

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20081132A NO20081132L (no) 2005-09-07 2008-03-04 Fremgangsmate for fremstilling av dioksolan

Country Status (16)

Country Link
US (1) US7754900B2 (no)
EP (1) EP1931650B1 (no)
JP (1) JP5473329B2 (no)
KR (1) KR101346404B1 (no)
CN (1) CN101282958B (no)
AT (1) ATE489376T1 (no)
AU (1) AU2006289088A1 (no)
BR (1) BRPI0615856A2 (no)
CA (1) CA2623594A1 (no)
DE (2) DE102005042505A1 (no)
MX (1) MX2008003115A (no)
MY (1) MY145876A (no)
NO (1) NO20081132L (no)
PL (1) PL1931650T3 (no)
WO (1) WO2007028809A1 (no)
ZA (1) ZA200802716B (no)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8212069B2 (en) 2006-10-26 2012-07-03 Ralf Boehling Process for preparing isocyanates
JP2012116920A (ja) * 2010-11-30 2012-06-21 Polyplastics Co ポリオキシメチレン樹脂の製造方法
CN102267972B (zh) * 2011-06-15 2013-03-13 四川之江化工新材料有限公司 基于反应-分离耦合生产1,3-二氧戊环的方法
US8785697B2 (en) 2011-06-24 2014-07-22 Eastman Chemical Company Nickel modified catalyst for the production of hydroxy ether hydrocarbons by vapor phase hydrogenolysis of cyclic acetals and ketals
US8829207B2 (en) 2011-06-24 2014-09-09 Eastman Chemical Company Production of cyclic acetals by reactive distillation
US8969598B2 (en) 2011-06-24 2015-03-03 Eastman Chemical Company Production of cyclic acetals or ketals using liquid-phase acid catalysts
US9388105B2 (en) 2011-06-24 2016-07-12 Eastman Chemical Company Production of hydroxy ether hydrocarbons by liquid phase hydrogenolysis of cyclic acetals or cyclic ketals
US8829206B2 (en) 2011-06-24 2014-09-09 Eastman Chemical Company Production of cyclic acetals or ketals using solid acid catalysts
US9000229B2 (en) 2011-06-24 2015-04-07 Eastman Chemical Company Production of hydroxy ether hydrocarbons by vapor phase hydrogenolysis of cyclic acetals and ketals
US9056313B2 (en) 2011-06-24 2015-06-16 Eastman Chemical Company Catalysts for the production of hydroxy ether hydrocarbons by vapor phase hydrogenolysis of cyclic acetals and ketals
CN102276575B (zh) * 2011-07-29 2015-01-07 北京旭阳化工技术研究院有限公司 一种制备1,3-二氧戊环的方法
CN102794185B (zh) * 2012-08-28 2014-07-23 四川之江高新材料股份有限公司 制备1,3-二氧戊环的方法及所用催化剂和装置
CN105693687B (zh) * 2016-03-10 2020-11-17 天津大学 一种二醇缩醛/酮反应的高效反应精馏方法及装置
CN105693686B (zh) * 2016-03-10 2020-11-17 天津大学 4emd生产的反应精馏方法及装置
WO2019092495A1 (en) 2017-11-09 2019-05-16 Braskem S.A. Process for the recovery of ketones and glycols from fermentation
CN108516968A (zh) * 2018-05-03 2018-09-11 开封龙宇化工有限公司 一种回收二氧五环重沸塔底部物料的装置及工艺流程
KR20210013132A (ko) 2018-05-18 2021-02-03 바스프 에스이 디옥솔란의 제조 방법
KR20210013131A (ko) 2018-05-18 2021-02-03 바스프 에스이 디옥솔란의 제조 방법
CN111978284A (zh) * 2020-08-14 2020-11-24 中化学科学技术研究有限公司 一种二氧五环制备工艺及制备系统
CN115260147A (zh) * 2022-08-22 2022-11-01 凯瑞环保科技股份有限公司 一种利用萃取催化精馏合成二氧戊环的工艺装置和方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1279025B (de) * 1965-01-22 1968-10-03 Basf Ag Verfahren zur kontinuierlichen Reinigung von Dioxolan
DE1914209A1 (de) * 1969-03-20 1970-10-08 Basf Ag Verfahren zur kontinuierlichen Herstellung von Acetalen
JP3098300B2 (ja) * 1991-12-05 2000-10-16 旭化成工業株式会社 １，３ジオキソランの精製法
JPH05271217A (ja) * 1992-03-25 1993-10-19 Asahi Chem Ind Co Ltd １，３ジオキソランの製造方法
JP2922848B2 (ja) * 1996-06-14 1999-07-26 株式会社日本触媒 芳香族炭酸エステルの製造方法
JPH1053552A (ja) * 1996-08-12 1998-02-24 Mitsubishi Chem Corp 二量化アルデヒドの製造方法
US5877363A (en) * 1996-09-23 1999-03-02 Catalytic Distillation Technologies Process for concurrent selective hydrogenation of acetylenes and 1,2 butadine in hydrocarbon streams
DE10004311A1 (de) * 2000-02-01 2001-08-02 Basf Ag Destillative Reinigung von Ammoniak
US6548681B1 (en) * 2001-06-26 2003-04-15 Board Of Trustees Of Michigan State University Process for the recovery of a polyol from an aqueous solution
MXPA05005846A (es) * 2002-12-04 2005-08-29 Fluor Corp Sistemas mejorados de destilacion.
DE10260092A1 (de) * 2002-12-19 2004-07-01 Basf Ag Verfahren zur Reinigung von Isocyanaten
DE10322655A1 (de) * 2003-05-20 2004-12-09 Basf Ag Verfahren zur Gewinnung von Roh-1,3-Butadien aus einem C4-Schnitt

Also Published As

Publication number Publication date
ATE489376T1 (de) 2010-12-15
DE502006008398D1 (de) 2011-01-05
AU2006289088A1 (en) 2007-03-15
DE102005042505A1 (de) 2007-03-08
EP1931650B1 (de) 2010-11-24
US20080255376A1 (en) 2008-10-16
MY145876A (en) 2012-05-15
BRPI0615856A2 (pt) 2012-12-18
JP2009507808A (ja) 2009-02-26
ZA200802716B (en) 2009-09-30
MX2008003115A (en) 2008-04-30
US7754900B2 (en) 2010-07-13
KR101346404B1 (ko) 2014-01-02
JP5473329B2 (ja) 2014-04-16
EP1931650A1 (de) 2008-06-18
WO2007028809A1 (de) 2007-03-15
CN101282958A (zh) 2008-10-08
CA2623594A1 (en) 2007-03-15
KR20080043392A (ko) 2008-05-16
CN101282958B (zh) 2012-07-04
PL1931650T3 (pl) 2011-05-31

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