MXPA03005248A - Procedimiento de purificacion de mezclas de diisocianato de tolueno que incorpora columna de destilacion con pared divisora. - Google Patents
Procedimiento de purificacion de mezclas de diisocianato de tolueno que incorpora columna de destilacion con pared divisora.Info
- Publication number
- MXPA03005248A MXPA03005248A MXPA03005248A MXPA03005248A MXPA03005248A MX PA03005248 A MXPA03005248 A MX PA03005248A MX PA03005248 A MXPA03005248 A MX PA03005248A MX PA03005248 A MXPA03005248 A MX PA03005248A MX PA03005248 A MXPA03005248 A MX PA03005248A
- Authority
- MX
- Mexico
- Prior art keywords
- toluenediisocyanate
- purification
- dividing
- distillation column
- incorporating
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/11—Batch distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Procedimiento de purificacion de diisocianato de tolueno a partir de una alimentacion bruta de destilacion que comprende diisocianato de tolueno, un disolvente organico y menos del 2% en peso de fosgeno separando la alimentacion bruta de destilacion en una columna de destilacion con pared divisora en al menos cuatro fracciones de producto P1 - P4, siendo P1 un producto de bajo punto de ebullicion enriquecido en fosgeno, P2 un producto enriquecido en disolvente, P3 un producto de cola enriquecido en compuestos de alto punto de ebullicion, y P4 una corriente de producto de diisocianato de tolueno.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP02013460A EP1371633A1 (en) | 2002-06-14 | 2002-06-14 | Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column |
Publications (1)
Publication Number | Publication Date |
---|---|
MXPA03005248A true MXPA03005248A (es) | 2004-05-05 |
Family
ID=29558345
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MXPA03005248A MXPA03005248A (es) | 2002-06-14 | 2003-06-12 | Procedimiento de purificacion de mezclas de diisocianato de tolueno que incorpora columna de destilacion con pared divisora. |
Country Status (11)
Country | Link |
---|---|
US (1) | US7118653B2 (es) |
EP (2) | EP1371633A1 (es) |
JP (1) | JP4443149B2 (es) |
KR (1) | KR100984426B1 (es) |
CN (1) | CN1310876C (es) |
AT (1) | ATE395329T1 (es) |
BR (1) | BR0302097A (es) |
CA (1) | CA2431439A1 (es) |
DE (1) | DE60320895D1 (es) |
MX (1) | MXPA03005248A (es) |
TW (1) | TWI281912B (es) |
Families Citing this family (67)
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DE60214195T2 (de) * | 2002-10-22 | 2007-10-04 | Bayer Materialscience Ag | Verfahren zur Reinigung von Diisocyanatotoluol unter Verwendung einer Destillationskolonne mit Trennwand in der Endreinigung |
DE10260093A1 (de) * | 2002-12-19 | 2004-07-01 | Basf Ag | Verfahren zur Abtrennung von Isocyanaten aus einem Reaktionsgemisch |
US7129387B2 (en) * | 2003-03-20 | 2006-10-31 | Bp Corporation North America Inc. | Low capital implementation of distributed distillation in ethylene recovery |
JP2012233004A (ja) * | 2005-04-04 | 2012-11-29 | Mitsui Chemicals Inc | ポリイソシアネート製造設備およびポリイソシアネート製造方法 |
JP2006312619A (ja) * | 2005-04-04 | 2006-11-16 | Mitsui Chemicals Polyurethanes Inc | ポリイソシアネート製造設備およびポリイソシアネート製造方法 |
DE102005025282A1 (de) * | 2005-06-02 | 2006-12-07 | Bayer Materialscience Ag | Datenverarbeitungssystem und Verfahren zur Regelung einer Anlage |
DE102005032430A1 (de) * | 2005-07-12 | 2007-01-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiamin |
JP2009508904A (ja) * | 2005-09-22 | 2009-03-05 | ハンツマン・インターナショナル・エルエルシー | ポリイソシアネートの製造法 |
DE102006009953A1 (de) * | 2006-03-03 | 2007-09-06 | Wacker Chemie Ag | Verfahren zur Wiederverwertung von hochsiedenden Verbindungen innerhalb eines Chlorsilanverbundes |
DE102006022448A1 (de) * | 2006-05-13 | 2007-11-15 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten |
US8030522B2 (en) * | 2006-06-07 | 2011-10-04 | Bayer Materialscience Llc | Process for the production of toluene diisocyanate |
US7528290B2 (en) * | 2006-12-28 | 2009-05-05 | Uop Llc | Apparatuses and methods for separating butene-1 from a mixed C4 feed |
DE102007020444A1 (de) | 2007-04-27 | 2008-11-06 | Bayer Materialscience Ag | Verfahren zur Oxidation eines Chlorwasserstoffenthaltenden Gasgemisches |
JP5479675B2 (ja) * | 2007-11-14 | 2014-04-23 | 三井化学株式会社 | トルエンジイソシアネートの製造方法 |
DE102007055266A1 (de) * | 2007-11-20 | 2009-05-28 | Bayer Materialscience Ag | Verfahren zur Reinigung von Diarylcarbonaten |
US8901346B2 (en) | 2008-10-02 | 2014-12-02 | Dow Global Technologies Llc | Apparatus, systems, and methods for purification of isocyanate mixtures |
US20100101273A1 (en) * | 2008-10-27 | 2010-04-29 | Sechrist Paul A | Heat Pump for High Purity Bottom Product |
BRPI1015061A2 (pt) | 2009-06-26 | 2016-04-19 | Basf Se | "processo para a preparação contínua de isocianatos" |
CN101780343B (zh) * | 2010-03-08 | 2014-09-10 | 沈阳金建科技开发有限公司 | 有害溶剂动态纯化再生器及其应用 |
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SG11201506454TA (en) * | 2013-02-21 | 2015-09-29 | Gtc Technology Us Llc | Separation processes using divided columns |
KR101425650B1 (ko) * | 2013-03-26 | 2014-08-01 | 동아대학교 산학협력단 | 분리벽형 증류탑을 이용한 해상 액화천연가스 분별증류장치 |
EP2829533A1 (de) | 2013-07-26 | 2015-01-28 | Bayer MaterialScience AG | Verfahren zur herstellung von isocyanaten |
KR20160044473A (ko) * | 2013-08-19 | 2016-04-25 | 코베스트로 도이칠란트 아게 | 이소시아네이트 제조로부터의 증류 잔류물로부터 유기 이소시아네이트를 수득하는 방법 |
CN103432761B (zh) * | 2013-08-20 | 2015-07-29 | 李群 | 分离二氯苯同分异构体的精馏方法 |
US20150052940A1 (en) * | 2013-08-23 | 2015-02-26 | Uop Llc | Fractionation system and method including depropanizer column and bottoms stripping column |
US9504934B2 (en) | 2013-10-27 | 2016-11-29 | Purdue Research Foundation | Multicomponent dividing wall columns |
PT3122718T (pt) | 2014-03-27 | 2018-03-27 | Covestro Deutschland Ag | Processo para a produção de isocianatos |
JP6621760B2 (ja) | 2014-03-27 | 2019-12-18 | コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag | 気相ホスゲン化プラントの運転方法 |
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EP2952237A1 (en) | 2014-06-02 | 2015-12-09 | Sulzer Chemtech AG | Method for purification of benzoic acid |
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CN105457324B (zh) | 2014-08-20 | 2019-12-27 | 科思创德国股份有限公司 | 隔板精馏塔 |
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HUE055741T2 (hu) | 2016-08-17 | 2021-12-28 | Covestro Intellectual Property Gmbh & Co Kg | Eljárás és berendezés különféle vegyi termékek elõállítására |
CN109641175B (zh) | 2016-09-01 | 2021-07-30 | 科思创德国股份有限公司 | 制备异氰酸酯的方法 |
KR102039089B1 (ko) * | 2016-12-15 | 2019-11-26 | 한화케미칼 주식회사 | 톨루엔디이소시아네이트 정제 방법 |
KR102596786B1 (ko) | 2016-12-21 | 2023-11-02 | 코베스트로 도이칠란트 아게 | 이소시아네이트를 제조하는 방법 |
US10836713B2 (en) * | 2017-06-08 | 2020-11-17 | Covestro Deutschland Ag | Method for producing isocyanates in the gas phase |
HUE060475T2 (hu) | 2017-06-08 | 2023-03-28 | Covestro Intellectual Property Gmbh & Co Kg | Eljárás izocianátok elõállítására |
US11365172B2 (en) | 2017-07-03 | 2022-06-21 | Covestro Deutschland Ag | Production plant for producing a chemical product by reacting H-functional reactants with phosgene, and method for operating same with an interruption to production |
WO2019241800A1 (en) * | 2018-06-15 | 2019-12-19 | Board Of Regents, The University Of Texas System | Distillation methods |
US10626084B2 (en) | 2018-08-03 | 2020-04-21 | Covestro Llc | Method for producing two isocyanates |
JP2022526915A (ja) | 2019-04-02 | 2022-05-27 | コベストロ・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツング・アンド・コー・カーゲー | 乾燥装置及びその使用法並びに乾燥装置を使用してイソシアネートを生成するプロセス |
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WO2022045960A1 (en) * | 2020-08-28 | 2022-03-03 | Sui Jianjun | Method and device for purification of p-dichlorobenzene |
KR20220095866A (ko) * | 2020-12-30 | 2022-07-07 | 한화솔루션 주식회사 | 이소시아네이트 화합물의 제조 방법 |
CN112569620B (zh) * | 2021-01-09 | 2022-04-01 | 福州大学 | 一种利用隔壁反应精馏塔制备环戊基甲醚的工艺系统 |
CN113262516B (zh) * | 2021-05-18 | 2022-06-24 | 河南中托力合化学有限公司 | 一种分离c16-c19正构烷烃用隔板塔的侧线采出结构 |
CN113651719B (zh) * | 2021-09-16 | 2023-08-04 | 宁夏瑞泰科技股份有限公司 | 一种六亚甲基二异氰酸酯光化液的精制方法 |
WO2023140986A1 (en) | 2022-01-19 | 2023-07-27 | Exxonmobil Chemical Patents Inc. | Compositions containing tri-cyclopentadiene and processes for making same |
CN116217439A (zh) * | 2023-01-03 | 2023-06-06 | 万华化学集团股份有限公司 | 一种光气化制备mdi的循环溶剂及其提纯方法 |
CN116789568A (zh) * | 2023-06-20 | 2023-09-22 | 沧州大化股份有限公司 | 一种降低甲苯二异氰酸酯中水解氯含量的方法 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2471134A (en) | 1946-07-17 | 1949-05-24 | Standard Oil Dev Co | Fractionation apparatus |
US2908704A (en) * | 1957-08-07 | 1959-10-13 | Du Pont | Process of preparing isocyanates |
US3287387A (en) * | 1963-07-29 | 1966-11-22 | Olin Mathieson | Process for the production of aromatic isocyanates |
US3321283A (en) * | 1963-12-23 | 1967-05-23 | Mobay Chemical Corp | Apparatus for conducting rapid chemical reactions |
US3499021A (en) * | 1966-10-19 | 1970-03-03 | Olin Mathieson | Toluene diisocyanate process |
AT277982B (de) * | 1966-11-18 | 1970-01-12 | Chemokomplex Vegyipari Gep Es | Verfahren zur halbkontinuierlichen oder kontinuierlichen Herstellung von aromatischen Mono- und Diisocyanaten |
BE711392A (es) * | 1968-02-28 | 1968-07-01 | Gnii Pi Azotnoj | |
US3987075A (en) * | 1972-01-03 | 1976-10-19 | Olin Corporation | Solvent extraction and distillation technique for purification of organic isocyanates |
DE2452805A1 (de) * | 1974-11-07 | 1976-05-20 | Basf Ag | Verfahren zur abtrennung von rueckstaenden der toluylendiisocyanatherstellung |
JPH07636B2 (ja) * | 1984-12-17 | 1995-01-11 | 三井東圧化学株式会社 | N−ホルミル−α−アスパルチルフエニルアラニンの製造法 |
DE3736988C1 (de) | 1987-10-31 | 1989-03-23 | Bayer Ag | Verfahren zur kontinuierlichen Herstellung von organischen Mono- und Polyisocyanaten |
BR9200378A (pt) * | 1991-01-28 | 1992-10-13 | Dow Chemical Co | Processo para preparacao de suportes de destilacao de tolueno diisocianato reativos e de viscosidade estavel e tolueno diisocianato tendo niveis de cloretos hidrolisaveis reduzidos |
DE4217019A1 (de) | 1992-05-22 | 1993-11-25 | Bayer Ag | Verfahren zur Herstellung von aromatischen Diisocyanaten |
DE19528781A1 (de) * | 1995-08-04 | 1997-02-06 | Bayer Ag | Verfahren zur Herstellung von Toluylendiisocyanat, spezielle Gemische aus Toluylendiamin und Wasser und deren Verwendung zur Herstellung von Toluylendiisocyanat |
DE10021703A1 (de) * | 2000-05-04 | 2001-11-08 | Basf Ag | Verfahren zur destillativen Trennung von Tetrahydrofuran, gamma-Butyrolacton und/oder 1,4-Butandiol enthaltenden Gemischen |
US6713630B2 (en) * | 2001-08-03 | 2004-03-30 | Basf Aktiengesellschaft | Continuous preparation of substituted oxazoles |
-
2002
- 2002-06-14 EP EP02013460A patent/EP1371633A1/en not_active Withdrawn
-
2003
- 2003-06-02 EP EP03012498A patent/EP1371635B1/en not_active Expired - Lifetime
- 2003-06-02 AT AT03012498T patent/ATE395329T1/de not_active IP Right Cessation
- 2003-06-02 DE DE60320895T patent/DE60320895D1/de not_active Expired - Lifetime
- 2003-06-09 CA CA002431439A patent/CA2431439A1/en not_active Abandoned
- 2003-06-09 US US10/457,307 patent/US7118653B2/en not_active Expired - Lifetime
- 2003-06-12 KR KR1020030037769A patent/KR100984426B1/ko active IP Right Grant
- 2003-06-12 MX MXPA03005248A patent/MXPA03005248A/es unknown
- 2003-06-13 TW TW092116030A patent/TWI281912B/zh not_active IP Right Cessation
- 2003-06-13 BR BR0302097-5A patent/BR0302097A/pt not_active IP Right Cessation
- 2003-06-13 JP JP2003168858A patent/JP4443149B2/ja not_active Expired - Fee Related
- 2003-06-13 CN CNB031410723A patent/CN1310876C/zh not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP1371635A1 (en) | 2003-12-17 |
US7118653B2 (en) | 2006-10-10 |
KR100984426B1 (ko) | 2010-09-29 |
US20030230476A1 (en) | 2003-12-18 |
ATE395329T1 (de) | 2008-05-15 |
EP1371635B1 (en) | 2008-05-14 |
TWI281912B (en) | 2007-06-01 |
DE60320895D1 (de) | 2008-06-26 |
CN1310876C (zh) | 2007-04-18 |
JP4443149B2 (ja) | 2010-03-31 |
CA2431439A1 (en) | 2003-12-14 |
BR0302097A (pt) | 2004-09-08 |
TW200404761A (en) | 2004-04-01 |
CN1467202A (zh) | 2004-01-14 |
EP1371633A1 (en) | 2003-12-17 |
JP2004155760A (ja) | 2004-06-03 |
KR20030096037A (ko) | 2003-12-24 |
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