MX148692A - Procedimiento adiabatico mejorado para la mononitracion de benzeno con acido nitrico para producir mononitrobenzeno - Google Patents

Procedimiento adiabatico mejorado para la mononitracion de benzeno con acido nitrico para producir mononitrobenzeno

Info

Publication number
MX148692A
MX148692A MX173367A MX17336778A MX148692A MX 148692 A MX148692 A MX 148692A MX 173367 A MX173367 A MX 173367A MX 17336778 A MX17336778 A MX 17336778A MX 148692 A MX148692 A MX 148692A
Authority
MX
Mexico
Prior art keywords
nitric acid
improved adiabatic
adiabatic procedure
mononitrobenzene
benzene
Prior art date
Application number
MX173367A
Other languages
English (en)
Inventor
Vernes Alexanderson
James Bryan Trecek
Cornelius Marsden Vanderwaart
Original Assignee
American Cyanamid Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Cyanamid Co filed Critical American Cyanamid Co
Publication of MX148692A publication Critical patent/MX148692A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
MX173367A 1977-08-19 1978-05-08 Procedimiento adiabatico mejorado para la mononitracion de benzeno con acido nitrico para producir mononitrobenzeno MX148692A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/826,208 US4091042A (en) 1977-08-19 1977-08-19 Continuous adiabatic process for the mononitration of benzene

Publications (1)

Publication Number Publication Date
MX148692A true MX148692A (es) 1983-06-02

Family

ID=25245976

Family Applications (1)

Application Number Title Priority Date Filing Date
MX173367A MX148692A (es) 1977-08-19 1978-05-08 Procedimiento adiabatico mejorado para la mononitracion de benzeno con acido nitrico para producir mononitrobenzeno

Country Status (21)

Country Link
US (1) US4091042A (es)
JP (1) JPS5432424A (es)
AT (1) AT357140B (es)
AU (1) AU518647B2 (es)
BE (1) BE867355A (es)
BR (1) BR7803249A (es)
CA (1) CA1083608A (es)
CH (1) CH639936A5 (es)
CS (1) CS207645B2 (es)
DD (1) DD136960A5 (es)
DE (1) DE2821571A1 (es)
EG (1) EG13569A (es)
FR (1) FR2400501A1 (es)
GB (1) GB1597433A (es)
IN (1) IN147796B (es)
IT (1) IT1103488B (es)
MX (1) MX148692A (es)
NL (1) NL189757C (es)
PL (1) PL113312B1 (es)
PT (1) PT68105A (es)
TR (1) TR19875A (es)

Families Citing this family (72)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4241229A (en) * 1979-08-08 1980-12-23 American Cyanamid Company Recovery of nitrated aromatic compounds from nitration wash liquors
JPS5785332A (en) * 1980-11-17 1982-05-28 Mitsui Toatsu Chem Inc Ortho-alkylation of phenolic compound
DE3409719A1 (de) * 1984-03-16 1985-09-19 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von dinitrotoluol
DE3409717C2 (de) * 1984-03-16 1994-03-31 Bayer Ag Verfahren zur Herstellung von Nitrobenzol
US4973770A (en) * 1988-12-15 1990-11-27 C-I-L, Inc. Manufacture of organic nitro compounds
US5313009A (en) * 1990-01-04 1994-05-17 Nrm International Technologies C.V. Nitration process
TW236610B (en) * 1992-11-13 1994-12-21 Bayer Ag Preparation of dinitrotoluene
DE4309140C2 (de) * 1993-03-22 2001-09-20 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4410417A1 (de) * 1994-02-14 1995-08-17 Bayer Ag Verfahren zur adiabatischen Herstellung von Mononitrotoluolen
DE4411064A1 (de) * 1994-03-30 1995-10-05 Bayer Ag Verfahren zur adiabatischen Herstellung von Mononitrohalogenbenzolen
DE4428462A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4428459A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4437047A1 (de) 1994-10-17 1996-04-18 Bayer Ag Verfahren zur Dinitrierung von aromatischen Verbindungen
US5763687A (en) 1995-12-15 1998-06-09 Mitsui Chemicals, Inc. Preparation process for aromatic mononitro compounds
BR0109028A (pt) * 2000-03-02 2003-03-05 Dow Global Technologies Inc Reator tubular, processo para conduzir reações polifásicas lìquido/ lìquido num reator tubular, e processo para compostos aromáticos com nitração no anel num reator tubular
US20060078893A1 (en) 2004-10-12 2006-04-13 Medical Research Council Compartmentalised combinatorial chemistry by microfluidic control
GB0307428D0 (en) 2003-03-31 2003-05-07 Medical Res Council Compartmentalised combinatorial chemistry
GB0307403D0 (en) 2003-03-31 2003-05-07 Medical Res Council Selection by compartmentalised screening
US20050221339A1 (en) 2004-03-31 2005-10-06 Medical Research Council Harvard University Compartmentalised screening by microfluidic control
US7968287B2 (en) 2004-10-08 2011-06-28 Medical Research Council Harvard University In vitro evolution in microfluidic systems
DE102005057555B3 (de) * 2005-11-21 2007-05-16 Meissner Gmbh & Co Kg Josef Verfahren zur Herstellung von Salpetersäureestern einwertiger Alkohole
JP2009536313A (ja) 2006-01-11 2009-10-08 レインダンス テクノロジーズ， インコーポレイテッド ナノリアクターの形成および制御において使用するマイクロ流体デバイスおよび方法
DE102006021857A1 (de) 2006-05-09 2007-11-15 Otto Bock Healthcare Ip Gmbh & Co. Kg Verfahren zum Gießen eines Prothesenschaftes
US20080014589A1 (en) 2006-05-11 2008-01-17 Link Darren R Microfluidic devices and methods of use thereof
US9562837B2 (en) 2006-05-11 2017-02-07 Raindance Technologies, Inc. Systems for handling microfludic droplets
US9012390B2 (en) 2006-08-07 2015-04-21 Raindance Technologies, Inc. Fluorocarbon emulsion stabilizing surfactants
US8772046B2 (en) 2007-02-06 2014-07-08 Brandeis University Manipulation of fluids and reactions in microfluidic systems
US8592221B2 (en) 2007-04-19 2013-11-26 Brandeis University Manipulation of fluids, fluid components and reactions in microfluidic systems
DE102007059513A1 (de) 2007-12-11 2009-06-18 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
US12038438B2 (en) 2008-07-18 2024-07-16 Bio-Rad Laboratories, Inc. Enzyme quantification
WO2010009365A1 (en) 2008-07-18 2010-01-21 Raindance Technologies, Inc. Droplet libraries
DE102008048713A1 (de) * 2008-09-24 2010-03-25 Bayer Materialscience Ag Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
JP5497052B2 (ja) 2008-11-10 2014-05-21 ノラム インターナショナル リミテッド モノニトロベンゼンを製造するための断熱的方法
KR101585704B1 (ko) * 2008-11-14 2016-01-14 노람 인터내셔널 리미티드 모노니트로벤젠의 생산에서 디니트로벤젠 부산물의 형성을 감소시키는 방법
CN101759568A (zh) * 2008-12-25 2010-06-30 南化集团研究院 硝基苯的绝热生产方法
DE102009005324B4 (de) 2009-01-16 2014-04-03 Plinke Gmbh Verfahren zur adiabatischen Nitrierung von Benzol
CN102333756B (zh) * 2009-02-26 2015-11-25 巴斯夫欧洲公司 制备硝化芳香族化合物及其混合物的方法
US8528589B2 (en) 2009-03-23 2013-09-10 Raindance Technologies, Inc. Manipulation of microfluidic droplets
WO2011042564A1 (en) 2009-10-09 2011-04-14 Universite De Strasbourg Labelled silica-based nanomaterial with enhanced properties and uses thereof
US10837883B2 (en) 2009-12-23 2020-11-17 Bio-Rad Laboratories, Inc. Microfluidic systems and methods for reducing the exchange of molecules between droplets
DE102010006984A1 (de) 2010-02-05 2011-08-11 Bayer MaterialScience AG, 51373 Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
US9366632B2 (en) 2010-02-12 2016-06-14 Raindance Technologies, Inc. Digital analyte analysis
US9399797B2 (en) 2010-02-12 2016-07-26 Raindance Technologies, Inc. Digital analyte analysis
US10351905B2 (en) 2010-02-12 2019-07-16 Bio-Rad Laboratories, Inc. Digital analyte analysis
WO2011100604A2 (en) 2010-02-12 2011-08-18 Raindance Technologies, Inc. Digital analyte analysis
DE102010038519A1 (de) 2010-07-28 2012-02-02 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
US9562897B2 (en) 2010-09-30 2017-02-07 Raindance Technologies, Inc. Sandwich assays in droplets
US9364803B2 (en) 2011-02-11 2016-06-14 Raindance Technologies, Inc. Methods for forming mixed droplets
EP3736281A1 (en) 2011-02-18 2020-11-11 Bio-Rad Laboratories, Inc. Compositions and methods for molecular labeling
EP2705020B1 (de) 2011-05-19 2015-04-08 Josef Meissner GmbH & Co. KG Verfahren und vorrichtung zur aufreinigung von nitrierprodukten
EP2714970B1 (en) 2011-06-02 2017-04-19 Raindance Technologies, Inc. Enzyme quantification
US8841071B2 (en) 2011-06-02 2014-09-23 Raindance Technologies, Inc. Sample multiplexing
CN102311347B (zh) * 2011-06-28 2013-08-14 江苏科圣化工装备工程有限公司 由焦化苯连续生产混二硝基苯的装置及方法
US8658430B2 (en) 2011-07-20 2014-02-25 Raindance Technologies, Inc. Manipulating droplet size
WO2013054181A1 (en) 2011-10-14 2013-04-18 Council Of Scientific & Industrial Research Continuous two step flow synthesis of m-amino acetophenone
CN102516082B (zh) * 2011-11-28 2013-11-06 万华化学集团股份有限公司 由苯与混酸反应制备硝基苯以及洗涤粗硝基苯产物的方法
EP2809644B1 (de) * 2012-01-31 2016-09-28 Covestro Deutschland AG Verfahren und anlage zur herstellung von nitrobenzol
US8907144B2 (en) * 2012-03-22 2014-12-09 Noram International Limited Process for adiabatic production of mononitrotoluene
EP2877443B1 (de) 2012-07-27 2016-05-11 Covestro Deutschland AG Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
WO2014016292A1 (de) 2012-07-27 2014-01-30 Bayer Materialscience Ag Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
KR102066764B1 (ko) 2012-07-27 2020-01-15 코베스트로 도이칠란드 아게 단열 니트로화에 의한 니트로벤젠의 제조방법
EP2991966B1 (de) * 2013-04-29 2017-07-12 Covestro Deutschland AG Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
US11901041B2 (en) 2013-10-04 2024-02-13 Bio-Rad Laboratories, Inc. Digital analysis of nucleic acid modification
US9944977B2 (en) 2013-12-12 2018-04-17 Raindance Technologies, Inc. Distinguishing rare variations in a nucleic acid sequence from a sample
US11193176B2 (en) 2013-12-31 2021-12-07 Bio-Rad Laboratories, Inc. Method for detecting and quantifying latent retroviral RNA species
US10647981B1 (en) 2015-09-08 2020-05-12 Bio-Rad Laboratories, Inc. Nucleic acid library generation methods and compositions
DE102017110084B4 (de) 2017-02-03 2019-07-04 Josef Meissner Gmbh & Co. Kg Verfahren und Anlage zur adiabatischen Nitrierung von Aromaten
KR102597388B1 (ko) 2017-03-07 2023-11-03 코베스트로 도이칠란트 아게 니트로벤젠의 제조 방법
WO2020011817A1 (de) 2018-07-12 2020-01-16 Covestro Deutschland Ag Verfahren zur herstellung von nitrobenzol durch adiabatisch betriebene nitrierung von benzol
DE102018217955B4 (de) * 2018-10-19 2020-06-04 Plinke Gmbh Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens
CN111393299A (zh) * 2020-05-06 2020-07-10 沈阳感光化工研究院有限公司 一种使用微通道连续流反应器对硝基苯进行硝化的方法
WO2024003050A1 (en) 2022-06-28 2024-01-04 Basf Se Process for producing nitrobenzene

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3087971A (en) * 1953-12-07 1963-04-30 Samuelsen Eirik Method for trinitrotoluene manufacture
GB1081091A (en) * 1964-01-08 1967-08-31 Ici Ltd Improvements in or relating to the preparation of dinitrotoluenes
US3928475A (en) * 1974-08-09 1975-12-23 Du Pont Azeotropic nitration of benzene
US4021498A (en) * 1975-12-09 1977-05-03 American Cyanamid Company Adiabatic process for nitration of nitratable aromatic compounds

Also Published As

Publication number Publication date
JPS5432424A (en) 1979-03-09
CS207645B2 (en) 1981-08-31
PT68105A (en) 1978-06-01
IT1103488B (it) 1985-10-14
FR2400501B1 (es) 1984-01-27
TR19875A (tr) 1980-04-03
DD136960A5 (de) 1979-08-08
FR2400501A1 (fr) 1979-03-16
EG13569A (en) 1981-12-31
NL7805409A (nl) 1979-02-21
BR7803249A (pt) 1979-03-27
IN147796B (es) 1980-06-28
AT357140B (de) 1980-06-25
CA1083608A (en) 1980-08-12
DE2821571A1 (de) 1979-03-01
BE867355A (fr) 1978-11-23
US4091042A (en) 1978-05-23
GB1597433A (en) 1981-09-09
NL189757C (nl) 1993-07-16
IT7849331A0 (it) 1978-05-12
AU518647B2 (en) 1981-10-15
CH639936A5 (de) 1983-12-15
PL113312B1 (en) 1980-12-31
ATA369978A (de) 1979-11-15
AU3529978A (en) 1979-10-25
NL189757B (nl) 1993-02-16
PL207037A1 (pl) 1979-05-07

Similar Documents

Publication Publication Date Title
MX148692A (es) Procedimiento adiabatico mejorado para la mononitracion de benzeno con acido nitrico para producir mononitrobenzeno
AR226894A1 (es) Procedimiento para obtener(4-trifluormetil anilida de acido 5-metil isoxazol-4-carboxilico
BR7800792A (pt) Processo para efetuar a etilacao do benzeno
MX5671E (es) Procedimiento mejorado para la produccion de granulos de urea
AR219502A1 (es) Procedimiento para la produccion de urea
AR213000A1 (es) Procedimiento para preparacion de acido di-n-propil-acetico
MX5149E (es) Procedimiento mejorado para la preparacion de derivados de acido cicloalquilidenmetilfenilacetico
BR7805060A (pt) Processo para preparar acido 1r-cis-caronaldeidico
ES496849A0 (es) Procedimiento para la obtencion de amidas de acido tetrazo- liloxicarboxilico de efecto herbicida
ES494230A0 (es) Un procedimiento para la preparacion de amidas del acido po-liprenilcarboxilico
MX5006E (es) Procedimiento para la preparacion de acido ciclohexancarboxilico
MX4914E (es) Procedimiento mejorado para la produccion de acido metacrilico
MX4318E (es) Procedimiento mejorado para la obtencion de acido tereftalico purificado
ES490729A0 (es) Procedimiento para la preparacion de nuevas imidas de acido ciclobutandicarboxilico
MX4601E (es) Procedimiento para la preparacion de esteres bencilicos de acido 2-isoprofil-4-fenil-3-butenico
AR227884A1 (es) Procedimiento para la obtencion de acido(fenil-2-benzotiazolil-6)-2-propionico
BR7707125A (pt) Processo para a preparacao de acido tereftatilo
BR7803382A (pt) Anilidas de acido ciclopropanocarboxilico,processo para sua fabricacao e composicoes fungicidas contendo esses compostos
MX5206E (es) Procedimiento para la preparacion de fenoxi-alfa-vinil-bencil-esteres de acido ciclopropancarboxilico
BR7706541A (pt) Processo para a preparacao de esteres de acido n,n-dimetil-o-pirazolil-carbamico composicoes inseticidas e sua aplicacao
MX4818E (es) Procedimiento para la preparacion de amidas de acidos(2-pirimidiniltio)alcanoicos
AR218294A1 (es) Procedimiento para la preparacion de derivados de acido oleanoico
BR7707294A (pt) Processo para preparacao de acido haloalquilfosfonico
AR218348A1 (es) Procedimiento para la produccion de acido 2,5-dicetogluconico
BR7804551A (pt) Processo para fabricacao de halogenetos de acido de alfa-halogeno-alquil-carbomida