BE867355A - Procede adiabatique continu de mononitration du benzene - Google Patents

Procede adiabatique continu de mononitration du benzene

Info

Publication number
BE867355A
BE867355A BE187937A BE187937A BE867355A BE 867355 A BE867355 A BE 867355A BE 187937 A BE187937 A BE 187937A BE 187937 A BE187937 A BE 187937A BE 867355 A BE867355 A BE 867355A
Authority
BE
Belgium
Prior art keywords
mononitration
benzene
adiabatic process
continuous adiabatic
continuous
Prior art date
Application number
BE187937A
Other languages
English (en)
Original Assignee
American Cyanamid Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Cyanamid Co filed Critical American Cyanamid Co
Publication of BE867355A publication Critical patent/BE867355A/fr

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/08Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
BE187937A 1977-08-19 1978-05-23 Procede adiabatique continu de mononitration du benzene BE867355A (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/826,208 US4091042A (en) 1977-08-19 1977-08-19 Continuous adiabatic process for the mononitration of benzene

Publications (1)

Publication Number Publication Date
BE867355A true BE867355A (fr) 1978-11-23

Family

ID=25245976

Family Applications (1)

Application Number Title Priority Date Filing Date
BE187937A BE867355A (fr) 1977-08-19 1978-05-23 Procede adiabatique continu de mononitration du benzene

Country Status (21)

Country Link
US (1) US4091042A (fr)
JP (1) JPS5432424A (fr)
AT (1) AT357140B (fr)
AU (1) AU518647B2 (fr)
BE (1) BE867355A (fr)
BR (1) BR7803249A (fr)
CA (1) CA1083608A (fr)
CH (1) CH639936A5 (fr)
CS (1) CS207645B2 (fr)
DD (1) DD136960A5 (fr)
DE (1) DE2821571A1 (fr)
EG (1) EG13569A (fr)
FR (1) FR2400501A1 (fr)
GB (1) GB1597433A (fr)
IN (1) IN147796B (fr)
IT (1) IT1103488B (fr)
MX (1) MX148692A (fr)
NL (1) NL189757C (fr)
PL (1) PL113312B1 (fr)
PT (1) PT68105A (fr)
TR (1) TR19875A (fr)

Families Citing this family (72)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4241229A (en) * 1979-08-08 1980-12-23 American Cyanamid Company Recovery of nitrated aromatic compounds from nitration wash liquors
JPS5785332A (en) * 1980-11-17 1982-05-28 Mitsui Toatsu Chem Inc Ortho-alkylation of phenolic compound
DE3409719A1 (de) * 1984-03-16 1985-09-19 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von dinitrotoluol
DE3409717C2 (de) * 1984-03-16 1994-03-31 Bayer Ag Verfahren zur Herstellung von Nitrobenzol
US4973770A (en) * 1988-12-15 1990-11-27 C-I-L, Inc. Manufacture of organic nitro compounds
US5313009A (en) * 1990-01-04 1994-05-17 Nrm International Technologies C.V. Nitration process
TW236610B (en) * 1992-11-13 1994-12-21 Bayer Ag Preparation of dinitrotoluene
DE4309140C2 (de) * 1993-03-22 2001-09-20 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4410417A1 (de) * 1994-02-14 1995-08-17 Bayer Ag Verfahren zur adiabatischen Herstellung von Mononitrotoluolen
DE4411064A1 (de) * 1994-03-30 1995-10-05 Bayer Ag Verfahren zur adiabatischen Herstellung von Mononitrohalogenbenzolen
DE4428462A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4428459A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4437047A1 (de) 1994-10-17 1996-04-18 Bayer Ag Verfahren zur Dinitrierung von aromatischen Verbindungen
US5763687A (en) 1995-12-15 1998-06-09 Mitsui Chemicals, Inc. Preparation process for aromatic mononitro compounds
BR0109028A (pt) * 2000-03-02 2003-03-05 Dow Global Technologies Inc Reator tubular, processo para conduzir reações polifásicas lìquido/ lìquido num reator tubular, e processo para compostos aromáticos com nitração no anel num reator tubular
US20060078893A1 (en) 2004-10-12 2006-04-13 Medical Research Council Compartmentalised combinatorial chemistry by microfluidic control
GB0307428D0 (en) 2003-03-31 2003-05-07 Medical Res Council Compartmentalised combinatorial chemistry
GB0307403D0 (en) 2003-03-31 2003-05-07 Medical Res Council Selection by compartmentalised screening
US20050221339A1 (en) 2004-03-31 2005-10-06 Medical Research Council Harvard University Compartmentalised screening by microfluidic control
US7968287B2 (en) 2004-10-08 2011-06-28 Medical Research Council Harvard University In vitro evolution in microfluidic systems
DE102005057555B3 (de) * 2005-11-21 2007-05-16 Meissner Gmbh & Co Kg Josef Verfahren zur Herstellung von Salpetersäureestern einwertiger Alkohole
JP2009536313A (ja) 2006-01-11 2009-10-08 レインダンス テクノロジーズ, インコーポレイテッド ナノリアクターの形成および制御において使用するマイクロ流体デバイスおよび方法
DE102006021857A1 (de) 2006-05-09 2007-11-15 Otto Bock Healthcare Ip Gmbh & Co. Kg Verfahren zum Gießen eines Prothesenschaftes
US20080014589A1 (en) 2006-05-11 2008-01-17 Link Darren R Microfluidic devices and methods of use thereof
US9562837B2 (en) 2006-05-11 2017-02-07 Raindance Technologies, Inc. Systems for handling microfludic droplets
US9012390B2 (en) 2006-08-07 2015-04-21 Raindance Technologies, Inc. Fluorocarbon emulsion stabilizing surfactants
US8772046B2 (en) 2007-02-06 2014-07-08 Brandeis University Manipulation of fluids and reactions in microfluidic systems
US8592221B2 (en) 2007-04-19 2013-11-26 Brandeis University Manipulation of fluids, fluid components and reactions in microfluidic systems
DE102007059513A1 (de) 2007-12-11 2009-06-18 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
US12038438B2 (en) 2008-07-18 2024-07-16 Bio-Rad Laboratories, Inc. Enzyme quantification
WO2010009365A1 (fr) 2008-07-18 2010-01-21 Raindance Technologies, Inc. Bibliothèque de gouttelettes
DE102008048713A1 (de) * 2008-09-24 2010-03-25 Bayer Materialscience Ag Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
JP5497052B2 (ja) 2008-11-10 2014-05-21 ノラム インターナショナル リミテッド モノニトロベンゼンを製造するための断熱的方法
KR101585704B1 (ko) * 2008-11-14 2016-01-14 노람 인터내셔널 리미티드 모노니트로벤젠의 생산에서 디니트로벤젠 부산물의 형성을 감소시키는 방법
CN101759568A (zh) * 2008-12-25 2010-06-30 南化集团研究院 硝基苯的绝热生产方法
DE102009005324B4 (de) 2009-01-16 2014-04-03 Plinke Gmbh Verfahren zur adiabatischen Nitrierung von Benzol
CN102333756B (zh) * 2009-02-26 2015-11-25 巴斯夫欧洲公司 制备硝化芳香族化合物及其混合物的方法
US8528589B2 (en) 2009-03-23 2013-09-10 Raindance Technologies, Inc. Manipulation of microfluidic droplets
WO2011042564A1 (fr) 2009-10-09 2011-04-14 Universite De Strasbourg Nanomatériau marqué à base de silice à propriétés améliorées et ses utilisations
US10837883B2 (en) 2009-12-23 2020-11-17 Bio-Rad Laboratories, Inc. Microfluidic systems and methods for reducing the exchange of molecules between droplets
DE102010006984A1 (de) 2010-02-05 2011-08-11 Bayer MaterialScience AG, 51373 Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
US9366632B2 (en) 2010-02-12 2016-06-14 Raindance Technologies, Inc. Digital analyte analysis
US9399797B2 (en) 2010-02-12 2016-07-26 Raindance Technologies, Inc. Digital analyte analysis
US10351905B2 (en) 2010-02-12 2019-07-16 Bio-Rad Laboratories, Inc. Digital analyte analysis
WO2011100604A2 (fr) 2010-02-12 2011-08-18 Raindance Technologies, Inc. Analyse numérique d'analytes
DE102010038519A1 (de) 2010-07-28 2012-02-02 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
US9562897B2 (en) 2010-09-30 2017-02-07 Raindance Technologies, Inc. Sandwich assays in droplets
US9364803B2 (en) 2011-02-11 2016-06-14 Raindance Technologies, Inc. Methods for forming mixed droplets
EP3736281A1 (fr) 2011-02-18 2020-11-11 Bio-Rad Laboratories, Inc. Compositions et méthodes de marquage moléculaire
EP2705020B1 (fr) 2011-05-19 2015-04-08 Josef Meissner GmbH & Co. KG Procédé et dispositif de purification de produits de nitration
EP2714970B1 (fr) 2011-06-02 2017-04-19 Raindance Technologies, Inc. Quantification d'enzyme
US8841071B2 (en) 2011-06-02 2014-09-23 Raindance Technologies, Inc. Sample multiplexing
CN102311347B (zh) * 2011-06-28 2013-08-14 江苏科圣化工装备工程有限公司 由焦化苯连续生产混二硝基苯的装置及方法
US8658430B2 (en) 2011-07-20 2014-02-25 Raindance Technologies, Inc. Manipulating droplet size
WO2013054181A1 (fr) 2011-10-14 2013-04-18 Council Of Scientific & Industrial Research Synthèse en flux continu à deux étapes de m-aminoacétophénone
CN102516082B (zh) * 2011-11-28 2013-11-06 万华化学集团股份有限公司 由苯与混酸反应制备硝基苯以及洗涤粗硝基苯产物的方法
EP2809644B1 (fr) * 2012-01-31 2016-09-28 Covestro Deutschland AG Procédé et installation destinés à la fabrication de nitrobenzène
US8907144B2 (en) * 2012-03-22 2014-12-09 Noram International Limited Process for adiabatic production of mononitrotoluene
EP2877443B1 (fr) 2012-07-27 2016-05-11 Covestro Deutschland AG Procede destine à la fabrication de benzol nitrique par nitrification d'adiabate
WO2014016292A1 (fr) 2012-07-27 2014-01-30 Bayer Materialscience Ag Procédé de preparation de nitrobenzène par nitrification adiabatique
KR102066764B1 (ko) 2012-07-27 2020-01-15 코베스트로 도이칠란드 아게 단열 니트로화에 의한 니트로벤젠의 제조방법
EP2991966B1 (fr) * 2013-04-29 2017-07-12 Covestro Deutschland AG Procede destine à la fabrication de benzol nitrique par nitrification d'adiabate
US11901041B2 (en) 2013-10-04 2024-02-13 Bio-Rad Laboratories, Inc. Digital analysis of nucleic acid modification
US9944977B2 (en) 2013-12-12 2018-04-17 Raindance Technologies, Inc. Distinguishing rare variations in a nucleic acid sequence from a sample
US11193176B2 (en) 2013-12-31 2021-12-07 Bio-Rad Laboratories, Inc. Method for detecting and quantifying latent retroviral RNA species
US10647981B1 (en) 2015-09-08 2020-05-12 Bio-Rad Laboratories, Inc. Nucleic acid library generation methods and compositions
DE102017110084B4 (de) 2017-02-03 2019-07-04 Josef Meissner Gmbh & Co. Kg Verfahren und Anlage zur adiabatischen Nitrierung von Aromaten
KR102597388B1 (ko) 2017-03-07 2023-11-03 코베스트로 도이칠란트 아게 니트로벤젠의 제조 방법
WO2020011817A1 (fr) 2018-07-12 2020-01-16 Covestro Deutschland Ag Procédé de production de nitrobenzène par nitrification adiabatique de benzène
DE102018217955B4 (de) * 2018-10-19 2020-06-04 Plinke Gmbh Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens
CN111393299A (zh) * 2020-05-06 2020-07-10 沈阳感光化工研究院有限公司 一种使用微通道连续流反应器对硝基苯进行硝化的方法
WO2024003050A1 (fr) 2022-06-28 2024-01-04 Basf Se Procédé de production de nitrobenzène

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3087971A (en) * 1953-12-07 1963-04-30 Samuelsen Eirik Method for trinitrotoluene manufacture
GB1081091A (en) * 1964-01-08 1967-08-31 Ici Ltd Improvements in or relating to the preparation of dinitrotoluenes
US3928475A (en) * 1974-08-09 1975-12-23 Du Pont Azeotropic nitration of benzene
US4021498A (en) * 1975-12-09 1977-05-03 American Cyanamid Company Adiabatic process for nitration of nitratable aromatic compounds

Also Published As

Publication number Publication date
JPS5432424A (en) 1979-03-09
CS207645B2 (en) 1981-08-31
PT68105A (en) 1978-06-01
IT1103488B (it) 1985-10-14
FR2400501B1 (fr) 1984-01-27
TR19875A (tr) 1980-04-03
MX148692A (es) 1983-06-02
DD136960A5 (de) 1979-08-08
FR2400501A1 (fr) 1979-03-16
EG13569A (en) 1981-12-31
NL7805409A (nl) 1979-02-21
BR7803249A (pt) 1979-03-27
IN147796B (fr) 1980-06-28
AT357140B (de) 1980-06-25
CA1083608A (fr) 1980-08-12
DE2821571A1 (de) 1979-03-01
US4091042A (en) 1978-05-23
GB1597433A (en) 1981-09-09
NL189757C (nl) 1993-07-16
IT7849331A0 (it) 1978-05-12
AU518647B2 (en) 1981-10-15
CH639936A5 (de) 1983-12-15
PL113312B1 (en) 1980-12-31
ATA369978A (de) 1979-11-15
AU3529978A (en) 1979-10-25
NL189757B (nl) 1993-02-16
PL207037A1 (pl) 1979-05-07

Similar Documents

Publication Publication Date Title
BE867355A (fr) Procede adiabatique continu de mononitration du benzene
FR2334653A1 (fr) Procede adiabatique pour la nitration de composes aromatiques nitrables
BE862052A (fr) Procede de deshydrocyclodimerisation
RO76054A (fr) Procede pour la preparation des tetradecapeptides
BE862420A (fr) Procede de production de structures cylindriques creuses
RO75870A (fr) Procede pour la preparation des alkylendiamines
BE857244A (fr) Procede de preparation de 3-chlorocephalosporines
BE857607A (fr) Procede de preparation de carotenoides symetriques
RO79398A (fr) Procede pour la preparation des 1-oxa-dethiacephalosporines
RO74429A (fr) Procede pour la preparation du nitrobenzene
FR2345454A1 (fr) Procede de preparation de 3-halomethylcephemes
BE842583A (fr) Procede de preparation d'azomethines
BE860267R (fr) Procede de preparation de para-alkylphenols
RO83446A (fr) Procede pour la preparation des cyclopropylmethoxyanilides
RO77935A (fr) Procede pour la preparation des cis-4a-arylo tahydro-1h-2-pyrinidine s
BE856615A (fr) Procede de production de colorants oxazeniques
FR2342968A1 (fr) Procede de preparation de 3-desoxyanthocyanidines
PT66890A (fr) Procede pour la preparation des aryloxy-1 amino-3 propanols-2
BE870104A (fr) Procede de preparation de 2-chlorosulfinyl-azetidin-4-ones
RO76031A (fr) Procede pour la preparation du n-1,1,2,2-tetrachlore-2-fluore-ethylthiobenzanilide
BE850632R (fr) Procede de preparation de para-alkylphenols
RO74444A (fr) Procede de preparation de l-asphargil-o-sulphato-l-tyrozyle-l-methionyleglicyle 1- triptofyle-l-methionyle-l-asparagyle-l-fenylamides
FR2318166A1 (fr) Procede de preparation continue de 2,5-dioxo-1-oxa-2-phospholanes
BE865432A (fr) Procede de preparation continue de polyesters insatures
BE866904A (fr) Procede de preparation de 3-bromophtalide

Legal Events

Date Code Title Description
RE20 Patent expired

Owner name: AMERICAN CYANAMID CY

Effective date: 19980523