KR960022689A - 수계 유기 폴리실록산 함유 조성물, 이의 제조방법 및 용도 - Google Patents

수계 유기 폴리실록산 함유 조성물, 이의 제조방법 및 용도 Download PDF

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KR960022689A
KR960022689A KR1019950047254A KR19950047254A KR960022689A KR 960022689 A KR960022689 A KR 960022689A KR 1019950047254 A KR1019950047254 A KR 1019950047254A KR 19950047254 A KR19950047254 A KR 19950047254A KR 960022689 A KR960022689 A KR 960022689A
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슈탄트케 부르크하르트
프링스 알베르트
호른 미카엘
퀘츠쉬 한스-요하임
크로프강스 프랑크
몽키에비츠 야로슬라프
자일러 클라우스-디트리히
스타인메츠 짐
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우베 페터스 · 한스-요하임 슈베르트페거
휠스 아크티엔게젤샤프트
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    • C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
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Abstract

본 발명은 필수적으로 유기 용매를 함유하지 않고, 인화점이 70℃ 이상이며, 특히 물로 희석된 상태에서의 가수분해로 인해 알콜이 유리되지 않는 수계 유리 폴리실록산 함유 조성물에 관한 것이다.
본 발명에 따르는 유기 폴리실록산 함유 조성물은 수불용성 유기 트리알콕시실란 M몰과 수용성 아미노알킬 알콕시실란 Q몰을 M/Q가 0보다 크고 2 이하인 몰 비로 혼합하고, 몰은 당해 혼합물에 가한 다음, 반응 혼합물의 pH를 1 내지 8로 조절하고, 이어서 이미 존재하고/하거나 반응 도중에 생성되는 알콜을 제거함으로써 수득할 수 있다.
본 발명에 따르는 유기 폴리실록산 함유 조성물의 제조방법 및 이의 용도에 대해서도 또한 기술되어 있다.

Description

수계 유기 폴리실록산 함유 조성물, 이의 제조방법 및 용도
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (17)

  1. 필수적으로 유기 용매를 함유하지 않고, 인화점이 70℃이상이며, 필수적으로 물로 희석된 상태에서의 가수분해로 인해 알콜이 유리되지 않는 수제 유기 폴리실록산 함유 조성물.
  2. 제1항에 있어서, 일반식(I)의 수용성 아미노알킬알콜시 실란 Q몰과 일반식(II)의 수불용성 알킬알콕시실란 M몰을 M/Q가 0보다 크고 2 이하인 몰 비로 혼합하고, 물을 당해 혼합물에 가한 다음, 반응 혼합물의 pH를 1 내지 8로 조절하고, 이어서 이미 존재하고/하거나 반응 도중에 생성되는 알콜을 제거함으로써 수득할 수 있는 유기 폴리실록산 함유 조성물.
    R-Si(R1)y(OR1*)3-y(I)
    R2-Si(R1**)3(II)
    상기 식에서, R은 일반식
    [Z(f+c·f*)](f+c·f*)-[AdNH(2+f-d)-[(CH2)a-NA1 eH(1-e+f*)-]c(CH2)b-](f+c·f*)+(III)
    의 아미노 작용성 유기 그룹[여기서, a 및 b는 각각 1 내지 6이고, c는 0 내지 6이며, d는 0 내지 2이고, e, f 및 f*은 각각 0 내지 1이며, A 및 A1은 벤질 또는 비닐벤질 라디칼이고, N은 질소원자이며, 또는 Z는1가의 무기산 또는 유기산 라디칼을 나타낸다]이고, R1, R1*및 R1**는 메틸 또는 에틸 라디칼이며, R2는 탄소수 1 내지 6의 직쇄, 사이클릭 또는 측쇄 알킬 라디칼 또는 일반식 NH2-CO-NH-(CH2)b-(IV)의 우레이도-알킬 그룹[여기서, b는 1 내지 6이다]이고, y는 0 내지 1이다.
  3. 제1항 또는 제2항에 있어서, pH가 1 내지 8임을 특징으로 하는 유기 폴리실록산 함유 조성물.
  4. 제1항 내지 제3항 중의 어느 한 항에 있어서, 1염기성 무기산 및/또는 유기산 및/또는 이들의 2차 생성물을 포함함을 특징으로 하는 유기 폴리실록산 함유 조성물.
  5. 제1항 내지 제4항 중의 어느 한 항에 있어서, 알콜 함량이 5중량% 미만임을 특징으로 하는 폴리실록산 함유 조성물.
  6. 제1항 내지 제5항 중의 어느 한 항에 있어서, 실리콘 수지 현탁액을 포함함을 특징으로 하는 유기 폴리실록산 함유 조성물.
  7. 제1항 내지 제6항 중의 어느 한 항에 있어서, 일반식 (I)의 수용성 아미노알킬알록시실란 Q몰과 일반식(II)의 수불용성 알킬알콕시실란 M몰을 M/Q가 0보다 크고 2 이하인 몰 비로 혼합하고, 물을 당해 혼합물에 가한 다음, 반응 혼합물의 pH를 1 내지 8로 조절하고, 이어서 이미 존재하고/하거나 반응 도중에 생성되는 알콜을 제거함을 특징으로 하는, 유기 폴리실록산 함유 조성물의 제조방법.
    R-Si(R1)y(OR1*)3-y(I)
    R2-Si(R1**)3(II)
    상기 식에서, R은 일반식
    [Z(f+c·f*)](f+c·f*)-[AdNH(2+f-d)-[(CH2)a-NA1 eH(1-e+f*)-]c(CH2)b-](f+c·f*)+(III)
    의 아미노 작용성 유기 그룹[여기서, a 및 b는 각각 1 내지 6이고, c는 0 내지 6이며, d는 0 내지 2이고, e, f 및 f*은 각각 0 내지 1이며, A 및 A1은 벤질 또는 비닐벤질 라디칼이고, N은 질소원자이며, Z는 1가의 무기산 또는 유기산 라디칼을 나타낸다]이고, R1, R1*및 R1**는 메틸 또는 에틸 라디칼이며, R2는 탄소수 1 내지 6의 직쇄, 사이클릭 또는 측쇄 알킬 라디칼 또는 일반식 NH2-CO-NH-(CH2)b-(IV)의 우레이도-알킬 그룹[여기서, b는 1 내지 6이다]이고, y는 0 내지 1이다.
  8. 제7항에 있어서, 사용되는 일반식(I)의 아미노알킬알콕시 실란과 일반식(II)의 알킬알콕시실란 1몰당 0.5 내지 30몰의 물이 반응 혼합물에 첨가됨을 특징으로 하는 방법.
  9. 제7항 또는 제8항에 있어서, 1염기성 산이 반응 혼합물에 첨가됨을 특징으로 하는 방법.
  10. 제7항 내지 제9항 중 어느 한 항에 있어서, 반응이 0℃ 내지 100℃의 온도 범위에서 수행됨을 특징으로 하는 방법.
  11. 제7항 내지 제10항 중의 어느 한 항에 있어서, 이미 존재하고/하거나 반응 도중에 생성되는 알콜이 반응 매질로부터 제거되는 비율로 물이 동시에 첨가됨을 특징으로 하는 방법.
  12. 제7항 내지 제11항 중의 어느 한 항에 있어서, 증류에 의한 알콜의 제거가 감압하에서 수행됨을 특징으로 하는 방법.
  13. 제7항 내지 제12항 중의 어느 한 항에 있어서, 증류에 의한 알콜의 제거가, 컬럼의 상부 온도가 물의 비점에 상응하는 온도에 도달할 때까지 계속됨을 특징으로 하는 방법.
  14. 제7항 내지 제13항 중의 어느 한 항에 있어서, 증류에 의해 알콜을 제거하기 전 및/또는 제거하는 동안 탈포제를 가하여 발포를 감소시킴을 특징으로 하는 방법.
  15. 제7항 내지 제14항 중의 어느 한 항에 있어서, 유기 폴리실록산 함유 조성물 중의 알콜 잔여량이 5중량% 미만으로 조절됨을 특징으로 하는 방법.
  16. 제7항 내지 제15항 중의 어느 한 항에 있어서, 증류에 의해 알콜을 제거한 후, 생성물이 침전 및/또는 여과에 의해 후정제됨을 특징으로 하는 방법.
  17. 표면을 소수성화하고, 무기 건촉 자재를 소수성화하며, 건축물 및 건축물의 외관을 보호하고, 유리 섬유를 피복시키며, 충전제를 실란화하고, 중합체 분산액과 에멀젼의 레올로지 특성(rheological property)을 개선 시키며, 직물, 피혁, 셀룰로오즈 및 녹말 제품을 소수성화하기 위해, 접착 증진제, 이형제, 가교결합제 및, 페인트 및 니스장 첨가제로서 사용하기 위한, 제1항 내지 제16항 중의 어느 한 항에 따르는 수계 유기 폴리실록산 함유 조성물의 용도.
    ※ 참고사항 :최초출원 내용에 의하여 공개하는 것임.
KR1019950047254A 1994-12-09 1995-12-07 수계 유기 폴리실록산 함유 조성물, 이의 제조방법 및 용도 KR960022689A (ko)

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DEP4443824.9 1994-12-09
DE4443824A DE4443824A1 (de) 1994-12-09 1994-12-09 Organopolysiloxan-haltige Zusammensetzungen auf Wasserbasis, Verfahren zu deren Herstellung sowie deren Verwendung

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Cited By (1)

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KR101222936B1 (ko) * 2010-09-29 2013-01-17 (주)디오 아미노실란을 이용한 수계 자외선 및 적외선 차단 코팅제 및 이를 사용하여 제조된 코팅막

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FR2737214B1 (fr) 1995-07-25 1997-10-24 Rhone Poulenc Chimie Polyorganosiloxanes perhalogenes polyfonctionnels et leurs procedes d'obtention
DE19624032A1 (de) * 1996-06-17 1997-12-18 Huels Chemische Werke Ag Oligomerengemisch kondensierter Alkylalkoxysilane
JP3419242B2 (ja) * 1996-07-18 2003-06-23 信越化学工業株式会社 バインダー組成物及び水系コーティング剤
DE19639782A1 (de) * 1996-09-27 1998-04-02 Huels Chemische Werke Ag Glycidether-, Acryl- und/oder Methacryl-funktionelle Organopolysiloxan-haltige Zusammensetzungen auf Wasser-Basis, Verfahren zu deren Herstellung sowie deren Verwendung
DE19639783A1 (de) * 1996-09-27 1998-04-02 Merck Patent Gmbh Modifizierte Perlglanzpigmente für Wasserlacksysteme
DE19649955A1 (de) 1996-12-03 1998-06-04 Huels Chemische Werke Ag Fluoralkyl-funktionelle Organopolysiloxan-haltige Zusammensetzungen auf Wasser/Alkohol-Basis, Verfahren zu deren Herstellung sowie deren Verwendung
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