KR102364285B1 - 2-메틸알릴 프로파네이트 알코올 용액의 연속 제조 방법 - Google Patents

2-메틸알릴 프로파네이트 알코올 용액의 연속 제조 방법 Download PDF

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KR102364285B1
KR102364285B1 KR1020207010735A KR20207010735A KR102364285B1 KR 102364285 B1 KR102364285 B1 KR 102364285B1 KR 1020207010735 A KR1020207010735 A KR 1020207010735A KR 20207010735 A KR20207010735 A KR 20207010735A KR 102364285 B1 KR102364285 B1 KR 102364285B1
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methylallyl
tower
alcohol
solution
propanate
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KR1020207010735A
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Korean (ko)
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KR20200047717A (ko
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즈롱 천
홍 인
웨이송 왕
이펑 진
성리 왕
칭메이 완
홍쥔 가오
딩리엔 마
즈미아오 량
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저지앙 대학
저지앙 황마 테크놀로지 컴퍼니 리미티드
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/68Preparation of metal alcoholates
    • C07C29/70Preparation of metal alcoholates by converting hydroxy groups to O-metal groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C08G65/2609Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020207010735A 2018-03-01 2018-10-10 2-메틸알릴 프로파네이트 알코올 용액의 연속 제조 방법 KR102364285B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN201810170183.X 2018-03-01
CN201810170183.XA CN108299159B (zh) 2018-03-01 2018-03-01 一种连续制备2-甲基烯丙醇盐醇溶液的方法
PCT/CN2018/109599 WO2019165783A1 (zh) 2018-03-01 2018-10-10 一种连续制备2-甲基烯丙醇盐醇溶液的方法

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KR20200047717A KR20200047717A (ko) 2020-05-07
KR102364285B1 true KR102364285B1 (ko) 2022-02-17

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JP (1) JP6977211B2 (ja)
KR (1) KR102364285B1 (ja)
CN (1) CN108299159B (ja)
DE (1) DE112018004253T5 (ja)
WO (1) WO2019165783A1 (ja)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108299159B (zh) * 2018-03-01 2020-06-12 浙江大学 一种连续制备2-甲基烯丙醇盐醇溶液的方法
CN112495315A (zh) * 2020-12-22 2021-03-16 赞宇科技集团股份有限公司 一种低杂质的脂肪酰胺丙基叔胺的生产工艺与装置
CN114591143B (zh) * 2022-03-16 2024-06-21 齐翔华利新材料有限公司 一种甲基烯丙醇钠的制备方法
CN115353441B (zh) * 2022-08-25 2024-01-30 江苏瑞恒新材料科技有限公司 一种提高回收甲醇纯度的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101314557A (zh) * 2007-06-01 2008-12-03 赢创德固赛有限责任公司 制备碱金属醇盐的方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2877274A (en) * 1958-01-21 1959-03-10 Du Pont Production of sodium methoxide
DE1254612C2 (de) 1965-11-10 1973-05-17 Dynamit Nobel Ag Verfahren zur kontinuierlichen Herstellung von Alkalialkoholaten
DE3413212C1 (de) * 1984-04-07 1985-09-12 Dynamit Nobel Ag, 5210 Troisdorf Verfahren zur Herstellung von wasserfreiem Kalium-tert.-butoxid
DE3701268C1 (de) * 1987-01-17 1988-04-14 Dynamit Nobel Ag Verfahren zur kontinuierlichen Herstellung von Kalium-tert.-butoxid
JPH0977730A (ja) 1995-09-14 1997-03-25 Mitsui Toatsu Chem Inc ジアセトニトリル類の製造方法
JPH09309849A (ja) * 1996-05-22 1997-12-02 Tokuyama Corp アルコキシド化合物の製造方法
DE19900073A1 (de) 1999-01-05 2000-07-06 Degussa Verfahren zur Herstellung von Alkalialkoholaten höherer Alkohole
DE19959153A1 (de) * 1999-12-08 2001-06-21 Basf Ag Verfahren zur Herstellung von Alkalimethylaten
DE10050015A1 (de) 2000-10-06 2002-04-11 Basf Ag Verfahren zur katalytischen Herstellung von Alkalialkoholaten
DE10158354A1 (de) 2001-11-28 2003-06-12 Degussa Verfahren zur Herstellung und Reinigung von Alkalimetall- und Erdalkalimetall-Alkoholaten
DE10352877A1 (de) 2003-11-10 2005-06-16 Basf Ag Verfahren zur katalytischen Herstellung von Alkalialkoholaten
CN102504239A (zh) * 2011-11-03 2012-06-20 山西合盛邦砼建材有限公司 用于制备聚羧酸盐减水剂大单体的催化剂及其制备方法
CN106831334A (zh) * 2017-01-22 2017-06-13 青岛科技大学 一种碱法合成异丙醇钾的连续生产工艺
CN108299159B (zh) * 2018-03-01 2020-06-12 浙江大学 一种连续制备2-甲基烯丙醇盐醇溶液的方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101314557A (zh) * 2007-06-01 2008-12-03 赢创德固赛有限责任公司 制备碱金属醇盐的方法

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JP2021512931A (ja) 2021-05-20
CN108299159A (zh) 2018-07-20
WO2019165783A1 (zh) 2019-09-06
CN108299159B (zh) 2020-06-12
DE112018004253T5 (de) 2020-05-14
KR20200047717A (ko) 2020-05-07
JP6977211B2 (ja) 2021-12-08

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