KR102047571B1 - 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 - Google Patents
폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 Download PDFInfo
- Publication number
- KR102047571B1 KR102047571B1 KR1020147027958A KR20147027958A KR102047571B1 KR 102047571 B1 KR102047571 B1 KR 102047571B1 KR 1020147027958 A KR1020147027958 A KR 1020147027958A KR 20147027958 A KR20147027958 A KR 20147027958A KR 102047571 B1 KR102047571 B1 KR 102047571B1
- Authority
- KR
- South Korea
- Prior art keywords
- compound
- polythiol
- minutes
- composition
- peak area
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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Classifications
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
- C07C321/02—Thiols having mercapto groups bound to acyclic carbon atoms
- C07C321/04—Thiols having mercapto groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
- C07C321/12—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms
- C07C321/14—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/10—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton
- C07C323/11—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/12—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C335/00—Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C335/30—Isothioureas
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
- C08G18/3855—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur
- C08G18/3876—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur containing mercapto groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
- C08G18/7628—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group
- C08G18/7642—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group containing at least two isocyanate or isothiocyanate groups linked to the aromatic ring by means of an aliphatic group having a primary carbon atom next to the isocyanate or isothiocyanate groups, e.g. xylylene diisocyanate or homologues substituted on the aromatic ring
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
- G02B1/041—Lenses
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Polyurethanes Or Polyureas (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012179899 | 2012-08-14 | ||
| JPJP-P-2012-179899 | 2012-08-14 | ||
| JP2013001201 | 2013-02-28 | ||
| JPPCT/JP2013/001201 | 2013-02-28 | ||
| PCT/JP2013/071891 WO2014027665A1 (ja) | 2012-08-14 | 2013-08-13 | ポリチオール組成物、光学材料用重合性組成物およびその用途 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020147027835A Division KR101533207B1 (ko) | 2012-08-14 | 2013-08-13 | 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020187021526A Division KR102074091B1 (ko) | 2012-08-14 | 2013-08-13 | 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20150032250A KR20150032250A (ko) | 2015-03-25 |
| KR102047571B1 true KR102047571B1 (ko) | 2019-11-21 |
Family
ID=49954940
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020147027835A Active KR101533207B1 (ko) | 2012-08-14 | 2013-08-13 | 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 |
| KR1020147027958A Active KR102047571B1 (ko) | 2012-08-14 | 2013-08-13 | 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 |
| KR1020187021526A Active KR102074091B1 (ko) | 2012-08-14 | 2013-08-13 | 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020147027835A Active KR101533207B1 (ko) | 2012-08-14 | 2013-08-13 | 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020187021526A Active KR102074091B1 (ko) | 2012-08-14 | 2013-08-13 | 폴리티올 조성물, 광학재료용 중합성 조성물 및 그 용도 |
Country Status (8)
| Country | Link |
|---|---|
| US (4) | US9777103B2 (enExample) |
| EP (2) | EP2960266B1 (enExample) |
| JP (2) | JP5373226B1 (enExample) |
| KR (3) | KR101533207B1 (enExample) |
| CN (4) | CN108623773B (enExample) |
| BR (1) | BR112014025570B1 (enExample) |
| IN (1) | IN2014DN08100A (enExample) |
| WO (1) | WO2014027665A1 (enExample) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5373226B1 (ja) | 2012-08-14 | 2013-12-18 | 三井化学株式会社 | ポリチオール組成物、光学材料用重合性組成物およびその用途 |
| TW201506083A (zh) * | 2013-06-18 | 2015-02-16 | Mitsubishi Gas Chemical Co | 光學材料用組成物 |
| TWI699389B (zh) | 2014-07-18 | 2020-07-21 | 日商三菱瓦斯化學股份有限公司 | 聚硫醇組成物及其製造方法 |
| US10132961B2 (en) | 2015-03-31 | 2018-11-20 | Mitsubishi Gas Chemical Company, Inc. | Episulfide compound and optical material composition including same |
| KR101831892B1 (ko) * | 2016-06-30 | 2018-02-26 | 에스케이씨 주식회사 | 폴리티오우레탄계 광학 재료용 중합성 조성물 |
| CN108884204A (zh) * | 2016-06-30 | 2018-11-23 | 豪雅镜片泰国有限公司 | 固化物的制造方法、固化物及眼镜镜片基材 |
| CN108884028B (zh) * | 2016-06-30 | 2020-10-09 | 豪雅镜片泰国有限公司 | 多硫醇化合物的制造方法、固化性组合物的制造方法、及固化物的制造方法 |
| JPWO2018003058A1 (ja) * | 2016-06-30 | 2019-01-17 | ホヤ レンズ タイランド リミテッドHOYA Lens Thailand Ltd | 硬化物の製造方法、硬化物および眼鏡レンズ基材 |
| WO2018012803A1 (ko) | 2016-07-14 | 2018-01-18 | 에스케이씨 주식회사 | 광학 재료용 방향족 폴리티올 화합물 |
| JP6306102B2 (ja) | 2016-07-29 | 2018-04-04 | ホヤ レンズ タイランド リミテッドHOYA Lens Thailand Ltd | 樹脂組成物 |
| KR101971110B1 (ko) * | 2016-08-30 | 2019-04-22 | 에스케이씨 주식회사 | 광학 재료용 폴리티올 화합물 |
| CN113372250B (zh) | 2017-02-15 | 2023-12-08 | Ks试验研究株式会社 | 多硫醇化合物、其制备方法、由其制备的透明氨基甲酸酯类树脂以及光学体 |
| CN110446696A (zh) * | 2017-03-24 | 2019-11-12 | 三井化学株式会社 | 多元硫醇化合物的制造方法、聚合性组合物及其用途 |
| KR101894921B1 (ko) * | 2018-01-19 | 2018-09-04 | 에스케이씨 주식회사 | 플라스틱 광학 렌즈용 폴리티올 조성물 |
| CN111868025B (zh) * | 2018-03-30 | 2023-12-12 | 三井化学株式会社 | 有机巯基化合物或其中间体的制造方法、(多)硫醇成分、光学材料用聚合性组合物、成型体、光学材料及透镜 |
| KR20190138145A (ko) | 2018-06-04 | 2019-12-12 | 에스케이씨 주식회사 | 폴리티올 조성물 및 이의 제조방법 |
| EP3841134A1 (en) * | 2018-08-20 | 2021-06-30 | PPG Industries Ohio Inc. | Polythiol composition |
| CN109651214A (zh) * | 2018-12-17 | 2019-04-19 | 锦西化工研究院有限公司 | 一种去除二巯乙基硫醚中絮状物,提高产品纯度、收率的方法 |
| JP7296754B2 (ja) * | 2019-03-28 | 2023-06-23 | ホヤ レンズ タイランド リミテッド | 光学部材用重合性組成物、光学部材、及び眼鏡レンズ |
| JP7296755B2 (ja) * | 2019-03-28 | 2023-06-23 | ホヤ レンズ タイランド リミテッド | 光学部材用樹脂組成物、光学部材、及び眼鏡レンズ |
| JP7273156B2 (ja) * | 2019-07-17 | 2023-05-12 | 三井化学株式会社 | ポリチオール組成物及びその応用 |
| JP7437932B2 (ja) * | 2019-12-27 | 2024-02-26 | 三井化学株式会社 | 廃水処理方法 |
| EP3916470B1 (en) | 2020-01-27 | 2023-12-27 | Mitsui Chemicals, Inc. | Polymerizable composition for optical material, polymerizable prepolymer composition for optical material, cured product, and method of producing optical material |
| MX2021013149A (es) | 2020-01-27 | 2021-12-10 | Mitsui Chemicals Inc | Composicion polimerizable para material optico, composicion polimerizable de prepolimero para material optico, producto curado y metodo para producir el material optico. |
| KR20200026853A (ko) | 2020-02-28 | 2020-03-11 | 에스케이씨 주식회사 | 폴리티올 조성물 및 이의 제조방법 |
| JP7434526B2 (ja) | 2020-03-10 | 2024-02-20 | 三井化学株式会社 | 光学材料用重合性組成物、光学材料用重合性プレポリマー組成物、硬化物及び光学材料の製造方法 |
| MX2022012244A (es) | 2020-03-30 | 2022-10-27 | Ppg Ind Ohio Inc | Metodo para preparar composiciones de polimeros de baja turbidez para su uso en materiales opticos con indice de refraccion alto. |
| KR20210121873A (ko) | 2020-03-31 | 2021-10-08 | 주식회사 엠엘텍 | 티오우레탄계 광학재료용 수지 조성물과 티오우레탄계 광학재료용 수지의 제조방법 |
| KR20220033890A (ko) * | 2020-09-10 | 2022-03-17 | 에스케이씨 주식회사 | 폴리티올 조성물 및 이를 포함하는 광학용 중합성 조성물 |
| KR102448166B1 (ko) * | 2020-09-22 | 2022-09-27 | 에스케이씨 주식회사 | 폴리티올 조성물 및 이를 포함하는 광학용 중합성 조성물 |
| CN114765982B (zh) * | 2020-11-13 | 2024-06-28 | 三井化学株式会社 | 多硫醇组合物、聚合性组合物、树脂、成型体、光学材料及透镜 |
| CN116601200A (zh) * | 2020-11-27 | 2023-08-15 | Skc株式会社 | 多硫醇组合物、光学组合物和光学产品 |
| CN116457385A (zh) * | 2020-11-27 | 2023-07-18 | Skc株式会社 | 多硫醇组合物、光学组合物和光学产品 |
| EP4455740A1 (en) | 2021-12-24 | 2024-10-30 | Mitsui Chemicals, Inc. | Method for manufacturing optical member and cured product |
| JPWO2024080383A1 (enExample) * | 2022-10-14 | 2024-04-18 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US5087758A (en) | 1988-12-22 | 1992-02-11 | Mitsui Toatsu Chemicals, Inc. | Mercapto compound, a high refractive index resin and lens and a process for preparing them |
| JP2621991B2 (ja) * | 1988-12-22 | 1997-06-18 | 三井東圧化学株式会社 | メルカプト化合物及びその製造方法 |
| JP2989787B2 (ja) * | 1991-08-08 | 1999-12-13 | 三井化学株式会社 | 含硫ウレタン系樹脂及びレンズ |
| JP2740714B2 (ja) * | 1991-08-08 | 1998-04-15 | 三井東圧化学株式会社 | メルカプト化合物及びその製造方法 |
| AU634932B1 (en) | 1991-08-08 | 1993-03-04 | Mitsui Chemicals, Inc. | Mercapto compound, its preparation process, and sulfur- containing urethane resins and lenses using the same |
| US5608115A (en) * | 1994-01-26 | 1997-03-04 | Mitsui Toatsu Chemicals, Inc. | Polythiol useful for preparing sulfur-containing urethane-based resin and process for producing the same |
| US5736609A (en) * | 1995-06-30 | 1998-04-07 | Mitsui Toatsu Chemicals, Inc. | Sulfur-containing urethane-based resin composition, its resin, and optical element and lens comprising resin |
| JP3229781B2 (ja) * | 1995-08-14 | 2001-11-19 | 三井化学株式会社 | 新規なポリチオールを用いた含硫ウレタン系プラスチックレンズ |
| JPH09194558A (ja) * | 1996-01-23 | 1997-07-29 | Mitsui Toatsu Chem Inc | 含硫ウレタン系プラスチックレンズ |
| JP3794651B2 (ja) * | 1996-03-28 | 2006-07-05 | 住友精化株式会社 | メルカプト化合物、メルカプト化合物の製造方法、テトラオール化合物およびテトラオール化合物の製造方法 |
| JP3910232B2 (ja) * | 1996-04-19 | 2007-04-25 | 住友精化株式会社 | メルカプト化合物、トリオール化合物、およびそれらの製造方法 |
| US5932681A (en) * | 1998-03-09 | 1999-08-03 | Ppg Industries Ohio, Inc. | Method of preparing an optical polymerizate |
| JP4426017B2 (ja) * | 1999-07-27 | 2010-03-03 | 三井化学株式会社 | 有機メルカプト化合物の製造方法 |
| JP2002270859A (ja) * | 2000-11-27 | 2002-09-20 | Mitsui Chemicals Inc | 光電素子用パッケージおよびその製造方法 |
| JP2007129450A (ja) | 2005-11-02 | 2007-05-24 | Canon Inc | 画像処理装置 |
| JP2007129449A (ja) | 2005-11-02 | 2007-05-24 | Canon Inc | 画像処理装置 |
| CN101421232A (zh) * | 2006-04-19 | 2009-04-29 | 三井化学株式会社 | 光学材料用(多)硫醇化合物的制造方法及含有该化合物的聚合性组合物 |
| WO2007129449A1 (ja) | 2006-04-20 | 2007-11-15 | Mitsui Chemicals, Inc. | 光学材料用ポリチオール化合物の製造方法およびそれを含む重合性組成物 |
| JP5026432B2 (ja) | 2006-10-16 | 2012-09-12 | 三井化学株式会社 | 光学材料用樹脂の製造方法 |
| CN101614831B (zh) * | 2009-08-11 | 2010-10-27 | 杭州新顺化工有限公司 | 高折射率树脂镜片及其制备方法 |
| IT1400108B1 (it) | 2010-05-20 | 2013-05-17 | Acomon Ag | Catalizzatore di polimerizzazione per politiouretani, composizione liquida polimerizzabile e procedimento per la produzione di vetri organici politiouretanici ad alto indice di rifrazione |
| KR20120058635A (ko) * | 2010-08-13 | 2012-06-08 | 주식회사 케이오씨솔루션 | 광학렌즈용 폴리티올 화합물의 제조법 및 이를 포함하는 수지 조성물 |
| CN104321306B (zh) * | 2012-08-14 | 2016-10-19 | 三井化学株式会社 | 多硫醇化合物的制造方法、光学材料用聚合性组合物及其用途 |
| JP5373226B1 (ja) | 2012-08-14 | 2013-12-18 | 三井化学株式会社 | ポリチオール組成物、光学材料用重合性組成物およびその用途 |
-
2013
- 2013-02-28 JP JP2013511439A patent/JP5373226B1/ja active Active
- 2013-08-13 KR KR1020147027835A patent/KR101533207B1/ko active Active
- 2013-08-13 CN CN201810335752.1A patent/CN108623773B/zh active Active
- 2013-08-13 CN CN201380023522.7A patent/CN104271629B/zh active Active
- 2013-08-13 KR KR1020147027958A patent/KR102047571B1/ko active Active
- 2013-08-13 KR KR1020187021526A patent/KR102074091B1/ko active Active
- 2013-08-13 IN IN8100DEN2014 patent/IN2014DN08100A/en unknown
- 2013-08-13 JP JP2013557683A patent/JP5613847B2/ja active Active
- 2013-08-13 EP EP15176601.1A patent/EP2960266B1/en active Active
- 2013-08-13 CN CN201810336442.1A patent/CN108727559B/zh active Active
- 2013-08-13 US US14/395,146 patent/US9777103B2/en active Active
- 2013-08-13 CN CN201810336616.4A patent/CN108559043B/zh active Active
- 2013-08-13 WO PCT/JP2013/071891 patent/WO2014027665A1/ja not_active Ceased
- 2013-08-13 BR BR112014025570-9A patent/BR112014025570B1/pt not_active IP Right Cessation
- 2013-08-13 EP EP13830142.9A patent/EP2824126B1/en active Active
-
2017
- 2017-08-25 US US15/686,970 patent/US20170349692A1/en not_active Abandoned
-
2018
- 2018-07-31 US US16/050,106 patent/US10858472B2/en active Active
- 2018-07-31 US US16/050,186 patent/US10858473B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN104271629B (zh) | 2018-05-11 |
| EP2824126B1 (en) | 2015-09-30 |
| US10858473B2 (en) | 2020-12-08 |
| US10858472B2 (en) | 2020-12-08 |
| WO2014027665A1 (ja) | 2014-02-20 |
| KR20140125457A (ko) | 2014-10-28 |
| CN108727559B (zh) | 2021-07-23 |
| US20170349692A1 (en) | 2017-12-07 |
| CN108559043B (zh) | 2021-11-02 |
| US20150094443A1 (en) | 2015-04-02 |
| BR112014025570B1 (pt) | 2020-12-22 |
| KR20180090898A (ko) | 2018-08-13 |
| CN108559043A (zh) | 2018-09-21 |
| US20180334527A1 (en) | 2018-11-22 |
| CN108727559A (zh) | 2018-11-02 |
| US9777103B2 (en) | 2017-10-03 |
| EP2824126A1 (en) | 2015-01-14 |
| US20180334528A1 (en) | 2018-11-22 |
| JPWO2014027665A1 (ja) | 2016-07-28 |
| IN2014DN08100A (enExample) | 2015-05-01 |
| EP2960266A1 (en) | 2015-12-30 |
| CN108623773B (zh) | 2021-04-16 |
| KR20150032250A (ko) | 2015-03-25 |
| KR101533207B1 (ko) | 2015-07-01 |
| EP2824126A4 (en) | 2015-03-04 |
| EP2960266B1 (en) | 2017-04-19 |
| CN108623773A (zh) | 2018-10-09 |
| JP5373226B1 (ja) | 2013-12-18 |
| CN104271629A (zh) | 2015-01-07 |
| JP5613847B2 (ja) | 2014-10-29 |
| KR102074091B1 (ko) | 2020-02-05 |
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