KR101410844B1 - 알칼리 금속 티타네이트 및 그 합성방법 - Google Patents

알칼리 금속 티타네이트 및 그 합성방법 Download PDF

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KR101410844B1
KR101410844B1 KR1020087031175A KR20087031175A KR101410844B1 KR 101410844 B1 KR101410844 B1 KR 101410844B1 KR 1020087031175 A KR1020087031175 A KR 1020087031175A KR 20087031175 A KR20087031175 A KR 20087031175A KR 101410844 B1 KR101410844 B1 KR 101410844B1
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alkali metal
lithium
dopant
lithium titanate
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KR20090015131A (ko
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푸 장
슈레쉬 마니
마이클 알. 위그좀
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에이일이삼 시스템즈 인코포레이티드
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/003—Titanates
    • C01G23/005—Alkali titanates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/04—Processes of manufacture in general
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
KR1020087031175A 2006-06-05 2007-06-05 알칼리 금속 티타네이트 및 그 합성방법 Active KR101410844B1 (ko)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US81094206P 2006-06-05 2006-06-05
US60/810,942 2006-06-05
US82267506P 2006-08-17 2006-08-17
US60/822,675 2006-08-17
US11/757,658 2007-06-04
US11/757,658 US7879493B2 (en) 2006-06-05 2007-06-04 Alkali metal titanates and methods for their synthesis
PCT/US2007/070387 WO2007143640A2 (en) 2006-06-05 2007-06-05 Alkali metal titanates and methods for their synthesis

Publications (2)

Publication Number Publication Date
KR20090015131A KR20090015131A (ko) 2009-02-11
KR101410844B1 true KR101410844B1 (ko) 2014-06-23

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Country Status (6)

Country Link
US (1) US7879493B2 (enExample)
JP (1) JP5362555B2 (enExample)
KR (1) KR101410844B1 (enExample)
CA (1) CA2654605A1 (enExample)
DE (1) DE112007001382T5 (enExample)
WO (1) WO2007143640A2 (enExample)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102008026580A1 (de) * 2008-06-03 2009-12-10 Süd-Chemie AG Verfahren zur Herstellung von Lithiumtitan-Spinell und dessen Verwendung
DE102009049470A1 (de) * 2009-10-15 2011-04-28 Süd-Chemie AG Verfahren zur Herstellung von feinteiligen Lithiumtitan-Spinellen und deren Verwendung
DE102009049693A1 (de) 2009-10-16 2011-04-21 Süd-Chemie AG Phasenreines Lithiumaluminiumtitanphosphat und Verfahren zur Herstellung und dessen Verwendung
JP5553110B2 (ja) * 2010-05-18 2014-07-16 株式会社村田製作所 電極活物質およびその製造方法、ならびにそれを備えた非水電解質二次電池
JP5672859B2 (ja) 2010-08-26 2015-02-18 宇部興産株式会社 微細な炭素繊維と複合化されたリチウムチタン複合酸化物電極材料
WO2012111294A1 (ja) * 2011-02-15 2012-08-23 パナソニック株式会社 リチウムイオン二次電池用負極活物質材料およびその製造方法
EP2677575B1 (en) * 2011-02-15 2017-06-28 Panasonic Intellectual Property Management Co., Ltd. Negative electrode active material for lithium ion secondary battery, and manufacturing method for same
KR101262054B1 (ko) 2011-02-17 2013-05-09 이화여자대학교 산학협력단 2차원 나노구조 리튬 티타늄 산화물, 그 제조방법 및 상기 2차원 나노구조 리튬 티타늄 산화물을 포함한 전극 물질
EP2701231A4 (en) * 2011-04-20 2014-11-19 Panasonic Corp SECONDARY BATTERY WITH NON-WATER ELECTROLYTE
CN102842706B (zh) * 2011-06-22 2015-05-13 比亚迪股份有限公司 一种钛酸锂材料的制备方法及钛酸锂材料、锂离子电池
JP5897444B2 (ja) * 2011-10-28 2016-03-30 富士フイルム株式会社 非水二次電池用電解液及び二次電池
WO2013081231A1 (ko) * 2011-11-30 2013-06-06 주식회사 휘닉스소재 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
DE102012208608A1 (de) * 2012-05-23 2013-11-28 Robert Bosch Gmbh Verfahren zum Herstellen einer Elektrode für einen elektrochemischen Energiespeicher und Elektrode
CN102780005B (zh) * 2012-08-20 2015-11-11 山东大学 一种钇改性的钛酸锂负极材料及其制备方法
CN103771500B (zh) * 2012-10-18 2015-06-24 上海纳米技术及应用国家工程研究中心有限公司 锂离子二次电池a、b位同时掺杂纳米钛酸锂的制备方法
GB201306814D0 (en) * 2013-04-15 2013-05-29 Johnson Matthey Plc Improvements in lithium-containing materials
KR101796233B1 (ko) * 2013-05-23 2017-12-01 주식회사 포스코 이종 금속이 도핑된 리튬 티탄 복합 산화물의 제조 방법, 및 이에 의하여 제조된 이종 금속이 도핑된 리튬 티탄 복합 산화물
RU2558140C1 (ru) * 2014-02-18 2015-07-27 Общество с ограниченной ответственностью "Научный центр "Автономные источники тока" (ООО "Научный центр "АИТ") АНОДНЫЙ МАТЕРИАЛ ЛИТИЙ-ИОННОГО АККУМУЛЯТОРА НА ОСНОВЕ LiCrTiO4 СО СТРУКТУРОЙ ШПИНЕЛИ И СПОСОБ ЕГО ПОЛУЧЕНИЯ
WO2015138019A1 (en) * 2014-03-12 2015-09-17 Imra America,Inc. Negative electrode active material for energy storage devices and method for making the same
WO2017111566A1 (ko) 2015-12-24 2017-06-29 주식회사 엘지화학 출력 특성이 향상된 음극 활물질 상기 음극 활물질을 포함하는 전기화학소자용 전극
CN108417823B (zh) * 2018-02-28 2021-03-30 华南理工大学 一种利用重复球磨法制备的Li2FeTi1-yMoyO4材料及其制备方法与应用
JP7771597B2 (ja) * 2020-09-28 2025-11-18 Ｕｂｅ株式会社 チタン酸リチウム粉末、それを用いた電極、及び蓄電デバイス

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10251020A (ja) * 1997-03-11 1998-09-22 Ishihara Sangyo Kaisha Ltd 金属置換チタン酸リチウムおよびその製造方法ならびにそれを用いてなるリチウム電池
JP2000277116A (ja) * 1999-03-25 2000-10-06 Sanyo Electric Co Ltd リチウム二次電池
US20030073001A1 (en) * 2001-10-02 2003-04-17 Jeremy Barker Synthesis of lithiated transition metal titanates for lithium cells

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3502118B2 (ja) * 1993-03-17 2004-03-02 松下電器産業株式会社 リチウム二次電池およびその負極の製造法
US6379843B1 (en) * 1996-06-14 2002-04-30 Hitachi Maxwell, Ltd. Nonaqueous secondary battery with lithium titanium cathode
US6221531B1 (en) * 1998-07-09 2001-04-24 The University Of Chicago Lithium-titanium-oxide anodes for lithium batteries
US6645673B2 (en) * 1999-02-16 2003-11-11 Toho Titanium Co., Ltd. Process for producing lithium titanate and lithium ion battery and negative electrode therein
JP4540167B2 (ja) * 1999-02-16 2010-09-08 東邦チタニウム株式会社 チタン酸リチウムの製造方法
JP2001354421A (ja) * 2000-06-08 2001-12-25 Toyota Central Res & Dev Lab Inc リチウム二次電池電極活物質用リチウムチタン複合酸化物およびその製造方法
US7211350B2 (en) * 2001-01-29 2007-05-01 Rutgers University Foundation Nanostructure lithium titanate electrode for high cycle rate rechargeable electrochemical cell
US6827921B1 (en) * 2001-02-01 2004-12-07 Nanopowder Enterprises Inc. Nanostructured Li4Ti5O12 powders and method of making the same
US6890510B2 (en) * 2001-07-20 2005-05-10 Altair Nanomaterials Inc. Process for making lithium titanate
US6881393B2 (en) * 2002-03-08 2005-04-19 Altair Nanomaterials Inc. Process for making nano-sized and sub-micron-sized lithium-transition metal oxides
DE10319464A1 (de) * 2003-04-29 2004-11-18 Basf Ag Verfahren zur Herstellung von nanokristallinen Lithiumtitanat-Spinellen

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10251020A (ja) * 1997-03-11 1998-09-22 Ishihara Sangyo Kaisha Ltd 金属置換チタン酸リチウムおよびその製造方法ならびにそれを用いてなるリチウム電池
JP2000277116A (ja) * 1999-03-25 2000-10-06 Sanyo Electric Co Ltd リチウム二次電池
US20030073001A1 (en) * 2001-10-02 2003-04-17 Jeremy Barker Synthesis of lithiated transition metal titanates for lithium cells

Also Published As

Publication number Publication date
JP2009542562A (ja) 2009-12-03
CA2654605A1 (en) 2007-12-13
US7879493B2 (en) 2011-02-01
WO2007143640A2 (en) 2007-12-13
DE112007001382T5 (de) 2009-05-07
JP5362555B2 (ja) 2013-12-11
WO2007143640A3 (en) 2008-10-09
US20070281211A1 (en) 2007-12-06
KR20090015131A (ko) 2009-02-11

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